• Title/Summary/Keyword: slurry stability

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Preparation of Porous Inorganic Materials by Foaming Slurry (슬러리 발포에 의한 연속성 무기질 다공체의 제조)

  • 박재구;이정식
    • Journal of the Korean Ceramic Society
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    • v.35 no.12
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    • pp.1280-1285
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    • 1998
  • Foaming method is presented the preparation of porous materials from high-concentrated kaolin silica and flyash slurries. The slurries were foamed dried and sintered respectively. The porosity of sintered ma-terials was about 70-75% Mean pore-size was the range of 70-150$\mu\textrm{m}$ and pore structure was continuous Sodium lauryl sulfate anionic surfactant was used as a foaming agent. The foaming ability and the froth sta-bility were increased with increasing the concentration of the foaming agent. But the size of the constituent bubble of froth after foaming process was not affected by the concentration of the foaming agent. These results showed that the mean pore-size of sintered materials was closely related to the froth stability which is related to the change of bubble-size during the drying process.

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COLOR STABILITY AND SURFACE TEXTURE TO TEMPERATURE AT STASHING OF PORCELAIN RESTORATION (도재수복물의 표면첨색시 온도에 따른 색조안정성과 표면조도의 평가)

  • Beak Eun-Ju;Bae Tae-Seong;Song Kwang-Yeob;Park Charn-Woon
    • The Journal of Korean Academy of Prosthodontics
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    • v.29 no.3
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    • pp.87-99
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    • 1991
  • The effect of oven firing on the color stability and surface texture of extrinsic stains used characterization and color modification of metal cermic restoration were studied by comparing different temperatures and techniques. They were autoglaze technique, applied glaze technique, two step low-fusing glaze technique and one step low-fusing glaze technique. Autoglaze technique and applied glaze technique were air-fired to manufacturer's recommended temperature. Two step low-fusing glaze technique is separated staining and overglazing. Thin slurry of stain powder were air-fired to $1500^{\circ}F$, Overglaze powder powder was then mixed with seam medium and air-fired to $170^{\circ}F$. One step low-fusing glaze technique is combined staining and overglazing. Thin slurry of stain and glaze powder were air-fired to $170^{\circ}F$. The obtained results were as fellows. 1. Slightly significant color differences by colorimeter were found between different stain application and fusion techniques(P<0.05). 2. Two step low-fusing glaze method showed the most rough surface, especially ceramco orage stain(P<0.05). 3. Surface roughness increased gradually in order of autoglaze, applied glaze, one step low-fusing glaze but they were not significantly different(P<0.05). 4. When two step low-fusing glaze was applied, both color measurement and surface texture were sinificantly different from other groups(P<0.05).

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Reclamation and Soil Improvement on Ultra Soft Soil (I) - Reclamation (초연약지반의 매립 및 지반개량 사례 연구 (I) - 매립)

  • Na, Yung-Mook;Hong, Eui;Han, Jung-Soo
    • Journal of the Korean GEO-environmental Society
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    • v.6 no.1
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    • pp.23-31
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    • 2005
  • The "Silt Pond" is 180 hectares in size and contained ultra soft slurry-like soil varying between 3 to 20 meters in thickness. Reclamation works in the Silt Pond commenced in the mid of 1990s. A considerable amount of subsurface investigation inclusive of sampling, field vane and density logging tests were carried out prior to the reclamation of the Silt Pond. Since material in the Silt Pond is extremely soft, filling was done by spreading sand with high water content in thin and equal thickness lifts, allowing the stability of the slurry-like foundation. Despite the extreme care taken, failures occurred during the sand spreading phase. A large piece of high strength geotextile measuring $900m{\times}700m$ was placed to strengthen the slurry like soil foundation at locations where the ultra-soft soil was found to be exposed. Following the remedial works, the Silt Pond was again reclaimed by sand spreading up to +4.0m CD. The success of the reclamation was confirmed by marine CPT profiling.

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Li4SiO4 slurry conditions and sintering temperature for fabricating Li4SiO4 pebbles as tritium breeders for nuclear-fusion reactors

  • Young Ah Park;Ji Won Yoo;Yi-Hyun Park;Young Soo Yoon
    • Nuclear Engineering and Technology
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    • v.55 no.8
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    • pp.2966-2976
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    • 2023
  • A tritium breeder is a lithium-based material capable of producing tritium. Many researchers designing nuclear-fusion energy are studying tritium production using pebbles, which are solid-type breeders. The sphericity and size of the pebbles are critical in obtaining pebbles with good tritium-breeding efficiency. Furthermore, tritium-release efficiency can be increased by using pebbles with appropriate porosities. Promising raw materials for tritium-breeding materials include Li4SiO4 and Li2TiO3. Li4SiO4 has a higher lithium density than Li2TiO3 and exhibits excellent tritium-breeding efficiency. However, it has the disadvantage of being easily decomposed during the Li4SiO4-green-pebble sintering process because of its low structural stability at high temperatures and high lithium density. In this study, we attempted to determine the optimal conditions for manufacturing Li4SiO4 pebbles using the droplet-freeze-drying method. The optimal Li4SiO4 slurry conditions and sintering temperatures were determined. The optimal Li4SiO4 slurry-fabrication conditions were 3 wt% polyvinyl alcohol and 75 wt% Li4SiO4 based on the deionized-water weight content. The sintering temperature at which Li4SiO4 did not decompose and exhibited the optimum porosity of 10.8% was 900 ℃.

Influence of Foaming Agents on the Properties of Foamed Concretes Having Various Densities

  • Kim, Jin-Man;Jeong, Ji-Yong
    • Journal of the Korea Institute of Building Construction
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    • v.12 no.1
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    • pp.22-30
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    • 2012
  • Four types of foaming agents, including Alcohol Ethoxy Sulfate (AES), Alpha Olefin Sulfonate (AOS), Vegetable Soap (VS), and Fe-Protein (FP), are widely used in the construction field. These have different surface tensions and viscosities in water of the same concentration, affecting the flow speed of liquid, size and distribution of foam, and foam stability. However, there is a lack of data regarding the properties of foam concrete using various foam agents. The purpose of this study is to investigate influence of foaming agents on the properties of foamed concretes with various densities. We find that the foaming agent type has little effect on the density, compressive strength, and thermal conductivity of foam concrete, but considerably affects the unit weight of foam, flow and flexural strength of foamed concrete. While almost all properties of foam concrete are affected by density in fresh or hardened state, the potential energy changed by slurry density and the viscosity of foam are dominant factors in the flowability of foam slurry.

Fabrication of Porous Ceramic Materials for Biomedical and Environmental Applications

  • Lee, Byong-Taek
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.11a
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    • pp.18.2-18.2
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    • 2009
  • Ceramics have some properties that are unmatched by other kind of materials like metals or polymers. The ability of high thermal and chemical resistance and in case of being superior in specific mechanical properties makes the ceramic materials suitable for arange of applications. The microstructure and morphology of a material arguably permit the use of many advanced application otherwise difficult to achieve.Porous structures have some important applications in biomedical and environmental field. For human hard tissue reconstruction and augmentation procedure suitable biomaterials are used with a desirable porosity. A range of porous bioceramics were fabricated with tailored design to meet the demand of specific applications. Channeled and interconnected porosity was introduced in alumina, zirconia, and hydroxyapatite or tri calcium phosphate ceramics by different methods like multi-pass extrusion process, bubble formation in viscous slurry,slurry dripping in immiscible liquid, sponge replica method etc. The detailed microstructural and morphological investigations were carried out to establish the unique features of each method and the developed systems. For environmental filters the porous structures were also very important. We investigated a range of channeled and randomly porous silicon based ceramic composites to enhance the material stability and filtration efficiency by taking advantage of the material chemistry of the element. Detailed microstructural and mechanical characterizations were carried out for the fabricated porous filtration systems.

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Effect of Increasing Amounts of Ammonium Nitrogen Induced by Consecutive Mixture of Poultry Manure and Cattle Slurry on the Microbial Community during Thermophilic Anaerobic Digestion

  • Alsouleman, Khulud
    • Journal of Microbiology and Biotechnology
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    • v.29 no.12
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    • pp.1993-2005
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    • 2019
  • Thermophilic anaerobic digestion (TAD) is characterized by higher biogas production rates as a result of assumedly faster microbial metabolic conversion rates compared to mesophilic AD. It was hypothesized that the thermophilic microbiome with its lower diversity than the mesophilic one is more susceptible to disturbances introduced by alterations in the operating factors, as an example, the supply of nitrogen-rich feedstock such as poultry manure (PM). Laboratory scaled TAD experiments using cattle slurry and increasing amounts of PM were carried out to investigate the (in-) stability of the process performance caused by the accumulation of ammonium and ammonia with special emphasis on the microbial community structure and its dynamic variation. The results revealed that the moderate PM addition, i.e., 25% (vol/vol based on volatile substances) PM, resulted in a reorganization of the microbial community structure which was still working sufficiently. With 50% PM application, the microbial community was further stepwise re-organized and was able to compensate for the high cytotoxic ammonia contents only for a short time resulting in consequent process disturbance and final process failure. This study demonstrated the ability of the acclimated thermophilic microbial community to tolerate a certain amount of nitrogen-rich substrate.

Optimization of CMP Process parameter using DOE(Design of Experiment) Technique (DOE(Design of Experiment)기법을 통한 CMP 공정 변수의 최적화)

  • Lee, Kyoung-Jin;Park, Sung-Woo;Park, Chang-Jun;Kim, Ki-Wook;Jeong, So-Young;Kim, Chul-Bok;Choi, Woon-Shik;Kim, Sang-Yong;Seo, Yong-Jin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.05c
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    • pp.228-232
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    • 2002
  • The rise throughput and the stability in the device fabrication can be obtained by applying chemical mechanical polishing(CMP) process in 0.18 ${\mu}m$ semiconductor device. However it does have various problems due to the CMP equipment. Especially, among the CMP components, process variables are very important parameters in determining removal rate and non-uniformity. In this paper, We studied the DOE(design of experiment) method for the optimized CMP process. Various process variations, such as table and head speed, slurry flow rate and down force, have investigated in the viewpoint of removal rate and non-uniformity. Through the above DOE results, we could set-up the optimal process parameters.

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Preparation and Characterization of a Layered Organic-inorganic Composite by the Electrophoretic Deposition of Plate-shaped Al2O3 Particles and Electrophoretic Resin (전기영동적층법을 통한 판상 알루미나 입자와 전기영동 수지의 배향 유무기 복합체 제조 및 물성평가)

  • Park, Hee Jeong;Lim, Hyung Mi;Choi, Sung-Churl;Kim, Younghee
    • Journal of the Korean Ceramic Society
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    • v.50 no.6
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    • pp.460-465
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    • 2013
  • Plate-shaped inorganic particles are coated onto a stainless steel substrate by the electrophoretic deposition of a precursor slurry which includes the inorganic particles of $Al_2O_3$ and polymer resin in mixed solvents to mimic the abalone shell structure, which is a composite of plate-shaped inorganic particles and organic interlayer binding materials with a layered orientation. The process parameters of the electrophoretic deposition include the voltage, coating time, and conductivity of the substrate. In addition, the suspension parameters are the particle size, concentration, viscosity, conductivity, and stability. We prepared an organic-inorganic composite coating with a high inorganic solid content by arraying the plate-shaped $Al_2O_3$ particles and electrophoretic resin via an electrophoretic deposition method. We analyzed the effect of the slurry composition and the electrophoretic deposition process parameters on the physical, mechanical and thermal properties of the coating layer, i.e., the thickness, density, particle orientation, Young's modulus and thermogravimetric analysis results.

A Study of End Point Detection Measurement for STI-CMP Applications (STI-CMP 공정 적용을 위한 연마 정지점 고찰)

  • 이경태;김상용;김창일;서용진;장의구
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.07a
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    • pp.90-93
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    • 2000
  • In this study, the rise throughput and the stability in fabrication of device can be obtained by applying of CMP process to STI structure in 0.18um semiconductor device. To employ in STI CMP, the reverse moat process has been added thus the process became complex and the defects were seriously increased. Removal rates of each thin films in STI CMP was not equal hence the devices must to be effected, that is, the damage was occured in the device dimension in the case of excessive CMP process and the nitride film was remained on the device dimension in the case of insufficient CMP process than these defects affect the device characteristics. To resolve these problems, the development of slurry for CMP with high removal rate and high selectivity between each thin films was studied then it can be prevent the reasons of many defects by reasons of many defects by simplification of process that directly apply CMP process to STI structure without the reverse moat pattern process.

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