• 한국표면공학회지
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• 제19권3호
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• pp.92-108
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• 1986

An electroplating on the lead frame fabricated from domestic copper plate was studied experimentally. In this study, nickel was plated on the thin copper lead frame and silver layer was coated on the nickel film in the cyanide electrolyte. The effect of process variables such as current density, plating time, coating thickness and flow rate of electrolytic solution on the properties of coating was investigated. Some samples on each step were fabricated during electroplating. The results obtained from polarization measurement, observation of SEM photograph, adhesion test of coating and microhardness test are as follows. On silver plating, polarization resistance of potentiostatic cathodic polarization curve is reduced as the flow rate of Ag electrolytic solution increases. And above resistance is also reduced when the minor chemicals of sodium cyanide and sodium carbonate are added in potassium silver cyanide bath. The reduced polarization resistance makes silver deposition on the cathode easy. An increase in the current density and the coating thickness causes the particle size of deposit to coarsen, and consequently the Knoop microhardness of the coating decreases. On selective plating an increase in the flow rate of plating solution lead to do high speed plating with high current density. In this case, the surface morphology of deposit is of fine microstructure with high Knoop hardness. An increasing trend of the adhesion of coating was shown with increasing the current density and flow rate of electrolytic solution.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 1998년도 제28회 추계학술대회
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• pp.49-58
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• 1998

An experimental study was performed to discover the effect of adsorbed moisture on the rolling resistance behavior of pure silver coated 52100 bearing steel. Plasma surface modifications were performed on the silver coated specimen to change the wetting characteristics. Experiments using a thrust ball beating-typed roiling test-rig were performed under vacuum, dry air and various tmmidity conditions. Results showed that the changes in the wetting characteristics influenced remarkably on the silver particle agglomeration and resulted in the different behavior of rolling resistance with humidity.

• 마이크로전자및패키징학회지
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• 제29권2호
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• pp.107-112
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• 2022

본 연구에서는 용제를 전혀 사용하지않고 UV경화가 가능한 실버 페이스트를 개발하였다. 무용제(solvent-free) 타입으로 개발한 실버 페이스트의 점도 및 점탄성 측정하였다. 그리고 스크린인쇄로 패턴을 인쇄한 후에 UV경화로 전극도막을 형성시켰다. 형성된 전극도막의 전도성, 연필경도, 접착력에 대해서 평가하였다. 마지막으로 전극도막의 경화특성은 TGA 및 FT-IR로 평가하였다. 이러한 결과를 정리하면 전도성, 접착력, 경화특성에 대해서는 Paste(4), 즉 1.2 ㎛의 구형 실버 파우더와 50 nm 실버 파우더를 72:8%로 혼합한 실버 페이스트가 가장 우수한 물성이 얻어짐을 알 수 있었다.

• Tribology and Lubricants
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• 제18권6호
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• pp.377-383
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• 2002

The tribological role of mass transfer layer was studied with silver coatings under various ranges of load and sliding speed. Silver coating was performed with a functionally gradient coating method. Tests were per-formed in dry sliding conditions, using a ball-on-disk contact configuration, at the load of 0.0196-17.64 N and the sliding speed of 20-1,000 mm/s in ambient air. Optical microscope and EPMA analyses showed that contact surfaces were covered with the mass transfer layers of agglomerated wear particles depending upon the contact conditions, and they greatly influenced the tribological characteristics of the surfaces. However, the formation of mass transfer layer was suppressed as the sliding speed increased, and above a critical sliding speed, no mass transfer layer was able to form. For building up a general framework of triboiogical behavior of the coated silver films, all test data were summarized on a map whose axes are contact pressure and sliding speed.

• 방사선산업학회지
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• 제6권3호
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• pp.273-279
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• 2012

Silica hybrid silver nanoparticles showing the strong antimicrobial activity, in which nano-silver is bound to silica molecules, has been synthesized using ${\gamma}-irradiation$ at room temperature. The present study relates to an antimicrobial composition for coating fiber products comprising silica hybrid silver nanoparticles. In this study, we describe antimicrobial fiber products coated with the silica hybrid silver nanoparticles and a method of antimicrobially treating fiber products by coating the fiber products with the silica hybrid silver nanoparticles. The antimicrobial fiber products exhibited excellent antimicrobial effects. In detailed practice, when the present composition comprising nanosized silica-silver was applied to a cloth (fabric) in a concentration of $6.4mg\;yard^{-1}$, the viable cell number decreased to less than 10 cells before and after laundering, resulting in a reduction of 99.9% or greater in the viable cell number. The present composition displays long-lasting potent disinfecting effects on bacteria. Also, we investigated the toxicity of silica hybrid silver nanoparticles in rats. The skin of rats was treated with a 30 ppm nanoparticles solution ($2ml\;Kg^{-1}$) for 8 days. No toxicity was detected in the treatment. These results suggest that the fiber products coated with the silica hybrid silver nanoparticles can be used to inhibit the growth of various microorganisms.

• 한국인터넷방송통신학회논문지
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• 제18권6호
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• pp.107-112
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• 2018

콘포멀 스프레이 코팅으로 형성한 EMI 차단막으로 차폐효과(SE)를 얼마나 개선할 수 있는지 연구하였다. 차단막을 형성하는데 사용한 재료는 도체 분말을 아크릴계 바인더에 혼합한 금속-레진 복합재료이며, 금속분말로는 은(Ag)과 니켈(Ni)을 비교하였다. 재료의 점도는 400 cPs와 100 cPs에서 차폐성능을 비교하였다. 차단막의 두께는, 은의 경우 20 um에서 50 um, 니켈의 경우 60 um에서 120 um로 만들어 비교하였다. 차폐효과의 측정은 동축형 표준 측정기를 이용하여 ASTM D4935 방법으로 수행하였다. 니켈 시료보다 은 시료의 차폐효과가 우수했다. 차폐효과는 차단막 두께와 비례해 증가하지만 35 um 이상에서 더 이상 증가하지 않는다는 사실도 관찰하였다. 가장 차폐효과가 좋은 경우는 35 um 두께 은 시료 차단막으로, 63 dB의 차폐효과가 측정되었다.

• 한국표면공학회지
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• 제49권1호
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• pp.87-91
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• 2016

The development of high performance transparent electrode with flexibility have been required for flexible electronics. Here, we demonstrate the silver nanowire and reduced graphene oxide hybrid transparent electrode for replacing brittle indium-tin-oxide electrode by spray coating technique and plasma reduction. The spray coating system is applied to deposit silver nanowire and over coated graphene oxide films and it has a great potential to scale-up. The resistance of silver nanowire transparent electrode is reduced by 10% and the surface roughness is decreased after graphene oxide coating. The over-coated graphene oxide is successfully reduced by $H_2$ plasma treatment and it is effective in increasing the environmental stability of electrode. The lifetime of silver nanowire and reduced graphene oxide hybrid electrode at $85^{\circ}C$ of Celsius degree of temperature and 85% of relative humidity has much increased.

• Tribology and Lubricants
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• 제15권4호
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• pp.321-327
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• 1999

An experimental study was performed to discover the effect of adsorbed moisture on the rolling resistance behavior of pure silver-coated 52100 bearing steel. Plasma surface modifications were performed on the silver-coated specimen to change the wetting characteristics. Experiments using a thrust ball bearing-type rolling test-rig were performed under vacuum, dry air and various humidity conditions. Results showed that the changes in the wetting characteristics influenced remarkably on the silver particle agglomeration and resulted in the different behavior of rolling resistance with humidity.

• 한국전기전자재료학회논문지
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• 제28권12호
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• pp.813-820
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• 2015

We have studied commercialization and process optimization of protective film on transparent conductive coated substrate, nano silver on flexible PET (poly ethylene terephthalate), by means of roll-to-roll micro-gravure coater. Nanosilver on flexible PET substrate is potential materials to replace ITO (indium tin oxide). Protective film is most important to maintain unique silver pattern on top of transparent PET. PSA pressure sensitive adhesives) was developed solely for nano silver on PET and protective film was successfully laminated. We have optimized all process conditions such as coating thickness, line speed and aging time & temperature via experimental design. Transparent conductive film and its protective film developed in this research are commercially available at this moment.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 2001년도 제33회 춘계학술대회 개최
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• pp.127-134
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• 2001

Nano adhesion and friction between a Sj$_3$N$_4$ AFM tip and thin silver films were experimentally studied. Tests were performed to measure the nano adhesion and friction in both AFM(atomic force microscope) and LFM(lateral force microscope) modes in various ranges of normal load. Thin silver films deposited by IBAD (ion beam assisted deposition) on Si-wafer (100) and Si-wafer of different surface roughness were used. Results showed that nano adhesion and friction decreased as the surface roughness increased. When the Si surfaces were coated by pure silver, the adhesion and friction decreased. But the adhesion and friction were not affected by the thickness of IBAD silver coating. As the normal force increased, the adhesion forces of bare Si-wafer and IBAD silver coating film remained constant, but the friction forces increased linearly. Test results suggested that the friction was mainly governed by the adhesion as long as the normal load was low.