• Journal of Internet of Things and Convergence
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• v.6 no.4
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• pp.33-38
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• 2020

It was reported that a mobile application was designed to easily provide natural dyeing information such as natural dye related resources, colors and dyed fabrics in 2007. Since studies on the linkage, application, etc. between natural dye dyeing and IoT are still lacking, diversity of information on the change of dyeing pattern by natural dye dyeing is required. In this study, it was to construct dyeing information by natural dyes, e.g., Lithospermum erythrorhizon, on silk, which has been traditionally used as many fibers in Korea. The extraction of the dye from L. erythrorhizon was carried out under pH4. The dried root of L. erythrorhizon showed dark brownish purple. Silk fabric by a without a mordant typically showed a purple dyed pattern. In the staining by sodium tartrate plus citric acid, silk fabric was stained clear brown. Interestingly, the mordant of iron (II) sulfate, the silk fabric was dyed in a light gray color rather than black. When the mordant of aluminum potassium sulfate was treated with L. erythrorhizon-extracted dye, the results were almost the same as when the mordant was not treated. When the degree of dyeing was evaluated numerically, the treatment of the mordant of potassium dichromate was about 50% darker, and the dyeing by iron (II) sulfate was about 75% darker. These results will be helpful in the study of applying various dye colors using L. erythrorhizon, and it will provide information on dyeing controller and database system construction by dyeing parameters such as dyeing degree, pH concentration, and chromaticity change.

• Textile Coloration and Finishing
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• v.28 no.3
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• pp.219-229
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• 2016

The purpose of this study was to investigate the dyeability of silk fabrics with sweet potato stem leaf extract. To obtain the optimal dyeing conditions it was examined at various dyeing conditions(temperature, pH, time and bath ratio). The dyeability and the depths of shade which were evaluated in terms of K/S and CIELAB color difference values of the dyed and mordanted fabrics were also investigated. After dyeing, various color fastness(wash fastness, dry cleaning fastness, light fastness, rub fastness, and perspiration fastness) was measured and reviewed for UV protective, deodorant and antimicrobial functionality. The optimun output, as a result, was shown at 100% of dye concentration, $90^{\circ}C$ of dyeing temperature and 80 minutes of dyeing time while in terms of dye uptake depending on the kind of mordants and mordanting, it was found that among four mordants of $Alk(SO_4)_2$, $CuSO_4$, $SnCl_2$, and $FeSO_4$, post-mordanting with $SnCl_2$ showed the best results. Color fastness to dry cleaning, washing and rubbing was found strong at grade 4-5 and the grade to perspiration was as good as 3 while to light fastness was good at 4 as well. In aspects of functional properties, it showed excellent results of 98.3% UV protection rate and 88% deodorization rate. Antibacterial activity was 99.9% against staphylococcus aureus and 73.3% against klebisella pneumoniae. In conclusion, we validated that the dyestuffs from the disused sweet potato stem leaf extract would be useful as a natural dye material using the optimized conditions and dyeability for silk dyeing.

• Journal of Sericultural and Entomological Science
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• v.38 no.2
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• pp.175-179
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• 1996

The sappan wood dyeing conditions and mordanting methods suitable for ramie as well as silk were investigated. The HVC values of dyed silk ramie fabrics were varied by the amount of sappan wood in the dyeing bath, while the optimum weight of sappan wood for the extraction of dye was around 15g/l. The K/S value of dyed silk fabric showed no significant difference in the pH range of 3.5 to 6.5. However, the K/S values of dyed ramie fabric was increased proportion to the pH value of dye bath. The K/S value of dyed silk and ramie fabrics were most increased at the highest dyeing temperature in the range of 30 to 9$0^{\circ}C$. By various mordantings, the HVC values of dyed silk and ramie fabrics were differentiated and it's color fastness could be improved.

• Journal of the Korea Fashion and Costume Design Association
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• v.19 no.1
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• pp.135-145
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• 2017

In order to analysis on color difference of yellow natural dyes, I have dyed cellulose and protein fabrics. The results of experiment have been analysed by wavelength of maximum absorption, amounts of dye uptake, color difference, Hunter's value and Munsell's value. The results from these analyses are as follows : Bud of pagoda tree, Amur cork, and Curcuma showed greenish yellow color, Gardenia Jasminoides showed reddish yellow color. Barberry root showed reddish yellow color with post-mordanting method on cellulose fabric. Moreover, Dupioni silk was dyed in reddish yellow color by Barberry root and Rhubarb. In addition to Chroma index, Gardenia Jasminoides and Curcuma showed clear color overall. However, dyeing rayon and silk by Barberry root, and dyeing silk by Rhubarb showed clear color. Comparing all the results to actual dyed materials, Bud of pagoda tree had small dye uptake, and both ${\Delta}a$ and ${\Delta}b$ value were short which can't recognized the yellow color easily. Dye uptake of Amur cork and Gardenia Jasminoides was small just like Bud of pagoda tree. However, ${\Delta}b$ value order was Gardenia Jasminoides>Amur cork>Bud of pagoda tree. Therefore, Gardenia Jasminoides recognized reddish yellow because of big value of red color and yellow color. In case of Barberry root and Rhubarb which have larger dye uptake, Baberry root recognized yellow color on rayon only, and couldn't recognized yellow color on bleached cotton fabric, ramie, silk, and dupioni silk. Rhubarb recognized yellow color on rayon with pre-mordanting method only, but recognized silk and dupioni silk as brown like color. Moreover, we could not analyze color by dye uptake, Lab, and H(v/c) for Barberry root and Rhubarb. As a result, I think we need to attach color table for the research paper which handled the color of dyeing materials.

• Textile Coloration and Finishing
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• v.20 no.6
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• pp.35-41
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• 2008

This study investigated the dyeing properties of silk fabrics with Annatto. The dye stuff was extracted by distilled water at $60^{\circ}C$, 10minutes, 1:100 of bath ratio. Dyeability(K/S) and color fastness of silk fabrics were tested under conditions of various concentrations, time, temperature, repeat-numbers of dyeing, pH, mordants variables and methods of mordanting. The highest absorbance was found in methanol extract of Annatto. The optimum dyeing concentration, time and temperature of silk fabrics with Annatto were 25%(o.w.f.), 60min and $60^{\circ}C$ respectively. The K/S value showed higher in post-mordanting than in pre-mordanting, and especially post-Fe mordant showed highest K/S value. In the case of colorfastness, Cu-mordanted fabrics were good washing fastness. Dry cleaning fastness appeared 4-5 grades and light fastness showed lowest grade.

• Journal of the Korean Society of Clothing and Textiles
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• v.26 no.1
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• pp.124-132
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• 2002

Dyeing properties of silk fabric on gromwell roof colorants were studied for the effect of dyeing conditions, such as methanol ratio, colorants concentration, pH, temperature and time etc. on the dye uptake and effect of mordants and mordanting methods on color change and dye uptake. And various colorfastnesses of dyed fabrics were evaluated far practical use. Gromwell colorants showed high affinity to silk and its isotherm adsorption curve was Freundlich type close to Nernst type. Therefore, it is considered that hydrogen bonding and Van der Waals force were involved in the adsorption of cromwell colorants to silk fabric. Post-mordanting method gave higher K/S value than other methods, but it was not significantly different color values from unmordanted one. Gromwell colorants produced mainly R and RP color depending on mordants and mordanting method. Dyed fabrics showed high colorfastness irrespective of mordanting treatment. Light colorfastness was increased for repeatedly dyed and Fe mordanted dyed fabrics.

• Journal of Fashion Business
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• v.9 no.1
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• pp.113-119
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• 2005

In our previous study, the color development characteristics in the dyeing of silk fibers and PET fibers using Rhusjara ica and related properties were meticulously reviewed. At the same time, the fabric specimens were endowed with chitosan treatment prior to the dyeing procedure in order to investigate the effect of chitosan on the dyeing behavior. The analysis of the colors only, however, would not give us complete elucidation of the effect of fiber characteristics and the mordanting characteristics. In this study, the effect of chitosan and metal mordant treatment in dyeing of silk and PET fabrics using Rhusjara ica has been studied. The change of air-permeability, wash fastness, and light fastness were also investigated.

• Textile Coloration and Finishing
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• v.13 no.2
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• pp.114-119
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• 2001

Four kinds of neutral sodium salts with different anions, NaF, NaCl, NaBr, and NaI, were added to the dye bath to accurately understand the effect of anions on the reactive dyeing of silk with C. I. Reactive Black 5. The sodium cation towered the negative surface potential of the silk and increased the dye-uptake on fille fabric as reported previously. However, because of the discrepancy in the anions'inhibition power from cation's lowering: the surface negative potential the amount of the dye on the silk fiber was different from each other in the order of $F^->Cl^-> Br^-I^-$. The activation energy(E$_{a}$) lot the dyeing was in the order of $F^->Cl^-> Br^-I^-$ but the dye-uptake on the fabric and the activation free energy$(\Delta{G}^*)$, the real energy barrier fort the reaction, were in the order of $F^->Cl^-> Br^-I^-$ because the strength of the interaction of the anions with sodium cations was the salute as the order of the latter. In other words F$^{[-1000]}$ exerted the weakest electrostatic force on $Na^+$ and competed with the dyestuff anions least of all. The decrease in $\Delta{S}^*$ may be due to the looesly bonded activated complex of dyestuff anions, sodium cations and fiber molecules at transition state. It was clarified from the Brёnsted equation that sodium salts with different anions also had fille ionic strength effect and the specific salt effect on the reactive dyeing.g.

• Journal of Fashion Business
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• v.9 no.6
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• pp.29-38
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• 2005

Natural dyes have attracted the worldwide attention because of its environmental advantage over synthetic dyes. However, most of natural dyes are expensive for mass production, strongly season and source dependent, and hard to store. In this study, coffee waste were used as natural dye to create beautiful colors. Coffee waste is inexpensive and easy to store, and provides a comparatively regular quality regardless of seasonand source. The effects of mordant agent concentration and mordanting temperature on dyeing efficiency of silk fabrics were investigated. Coffee extract dyed silk showed brilliant colors, and the colors were different with the kind of mordants. Cu, Sn, and Al mordanted silks showed golden yellow with subtle change of hue and value, while Fe mordanted silk showed a brownish green color. The increase in mordant concentration did not always increase the dyeability, and 0.5% o.w.f. mordant concentration was enough to get a satifactory result. Mordanting temperature also had little effect on the dyeability in case of Al, Cu, and Sn mordanted fabrics. Only Fe mordanted fabrics showed a better dyeability in the increase in mordating temperature. Coffee extract dyeing is an effective way using waste as resource and can create brilliant colors with minimal amount of mordant and under mild mordanting condition.

• Textile Coloration and Finishing
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• v.12 no.6
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• pp.396-403
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• 2000

The purpose of this study was to investigate the dyeing properties of silk, wool, nylon and poly(ethylene teraphtlate)〔PET〕 fabrics dyed with Tumeric(Curcuma longa) extracts. The dyeing property and color fastness were investigated by using the extracts and the post mordanting with Aluminum, Copper and Iron salts. In the UV-visible spectra, the maximum absorption of wavelength of the extract with methyl alcohol appeared at 420nm, and that of the extract with distilled water was at 415nm. Increasing the dyeing temperature, the K/S values of dyed fabrics were increased. The optimum dyeing condition was 30∼60 minute of dyeing time at pH 5∼5.6. Surface colors of silk and wool became dark by using mordants compared to those of nylon and PET fabrics. The drycleaning fastness of fabrics dyed with the extracts was good. The laundering and light fastness were improved by using mordants.