• Title/Summary/Keyword: silicon Carbide

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Effect of Grain Boundary Composition on Microstructure and Mechanical Properties of Silicon Carbide (입계상 조성이 탄화규소의 미세구조와 기계적 특성에 미치는 영향)

  • 김재연;김영욱;이준근
    • Journal of the Korean Ceramic Society
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    • v.35 no.9
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    • pp.911-916
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    • 1998
  • By using {{{{ { { {Y }_{3 }Al }_{5 }O }_{12 } }} (YAG) and SiO2 as sintering additives the effect of the composition of sintering ad-ditives on microstructure and mechanical properties of the hog-pressed and subsequently annealed SiC ma-terials were investigated. Microstructures of sintered and annealed materials were strongly dependent onthe composition of sintering additives. The average diameter and volume fraction of elongated grains in an-nealed materials increased with the SiO2/YAg ratio while the fracture toughness increased with the SiO2/YAg ratio. The average MPa.{{{{ { m}^{1/2 } }} respectively. Typical strength and fracture toughness of an annealed material with SiO2/YAg ra-tionof 0.67 were 371 MPa and 5.6 MPa.{{{{ { m}^{1/2 } }} respectively.

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Effect of Additive Composition on Mechanical Properties of Silicon Carbide Sintered with Aluminum Nitride and Erbium Oxide

  • Lee, Sung-Hee;Kim, Young-Wook
    • Journal of the Korean Ceramic Society
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    • v.42 no.1
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    • pp.16-21
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    • 2005
  • The effect of additive composition, using AlN and $Er_{2}O_{3}$ as sintering additives, on the mechanical properties of liquid-phase-sintered, and subsequently annealed SiC ceramics was investigated. The microstructures developed were quantitatively analyzed by image analysis. The average thickness of SiC grains increased with increasing the $Er_{2}O_{3}/(AlN + Er_{2}O_{3})$ ratio in the additives whereas the aspect ratio decreased with increasing the ratio. The mechanical properties versus $Er_{2}O_{3}/(AlN + Er_{2}O_{3})$ ratio curve had a maximum; i.e., there was a small composition range at which optimum mechanical properties were realized. The best results were obtained when the ratio ranged from 0.4 to 0.6. The flexural strength and fracture toughness of the SiC ceramics were $550\~650\;MPa$ and $5.5\~6.5$ MPa${\cdot}m^{1/2}$, respectively.

Influence of Liquid-Phase Amount on the Microstructure and Phase Transformation of Liquid-phase Sintered Silicon Carbide (액상량이 탄화규소 소결체의 미세구조 및 상변태에 미치는 영향)

  • 이종국;강현희;박종곤;이은구
    • Journal of the Korean Ceramic Society
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    • v.35 no.4
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    • pp.413-419
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    • 1998
  • ${\beta}$-silicon carbides with yttrium aluminum garnet of 2,5,10 mol% were prepared by a liquid--phase sint-ering and the microstructural evolution and phase transformation were investigated during sintering as functions of liquid-phase amount and sintering time. The rate of grain growth decreases with the addition of the amount of yttrium aluminum garnet (YAG) in the SiC starting powder however the apparent density and the aspect ratio of grains in sintered body increase. The phase transformation from ${\beta}$-SiC to ${\alpha}$-SiC were dependent on the liquid-phase amount and sintering time.

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Comparison of cutting performance of an AWJ with several types of abrasives (Water jet 절단에서의 연마재 종류별 성능 비교 시험)

  • Choon Sunwoo;;Ryu Chang ha;Kwng soo Kwon
    • Tunnel and Underground Space
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    • v.6 no.2
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    • pp.175-183
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    • 1996
  • Linear cutting tests on granite were conducted to evaluated the cutting performance of abrasive water jet(AWJ) using several types of abrasives. The abrasives used in the tests were grarnet, alumimum oxide, and silicon carbide. And one type of granite which is comercially known as "KeuchangSuk" was used as workpiece throughout the tests. The results from the tests were described in terms of cutting depth and abrasive productivity. Authors tried to confirm the effects of the operational parameters of abrasive mass flow rate, water pressure, and traverse speed of nozzle on cutting depth and presented almost all the data obtained in the tests. Abrasive productivity can be defined as the area of kerf wall cut by unit weight of abrasive and is an important factor to evaluated the cutting ability of abrasive and assess the cost effectiveness of an AWJ system. In the tests the maximum abrasive productivities of garnet, alumina, and silicon carbide were about 0.21, 0.24, and 0.20 $\textrm{cm}^2$ respectively under similar operational conditions.onditions.

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INVESTIGATIONS ON THREE-BODY ABRASIVE WEAR BEHAVIOUR OF SILICON CARBIDE AND GRAPHITE FILLED GLASS-VINYL ESTER COMPOSITES

  • Suresha, B.;Chandramohan, G.;Siddaramaiah, Siddaramaiah;Lee, Joong- Hee
    • Proceedings of the KSME Conference
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    • 2007.05a
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    • pp.148-153
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    • 2007
  • The effect of silicon carbide (SiC) and graphite fillers incorporation on the abrasive wear behaviour of glass-vinyl ester (G-V) composites have been investigated. The three-body abrasive wear behaviour was assessed by rubber wheel abrasion tests (RWAT). The worn surfaces were examined using scanning electron microscopy (SEM). The addition of SiC and graphite fillers in G-V composite improves the abrasion resistance under different loads/abrading distances. The SEM studies indicate the reasons for failure of composites and influencing parameters.

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R-curve, erosion and wear of silicon carbide ceramics (탄화규소의 R-curve, 침식 및 마모 특성)

  • 채준혁;조성재;김석삼
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1998.04a
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    • pp.139-145
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    • 1998
  • This paper addresses the R-curve properties, wear resistance, and erosion resistance of the two silicon carbide ceramics with different microstructures, i.e. , fine grained SiC and in situ-toughened SiC(IST SIC). Fine grained SiC exhibits a relatively flat R-curve behavior whereas the IST SiC exhibits a increasing R-curve behavior. The increasing R-curve behavior in IST SiC is attributed to relatively weak grain boundaries. The rate of material removal during wear tests and erosion tests was higher for IST SiC than that for fine grained SiC. This is attributed to the weaker grain boundaries in IST SiC than that in fine grained SiC. It is implied that fracture toughness in short crack regime should be taken into consideration in the interpretation of the microscopical material removal process. We show that the higher the strength of grain boundaries is, the higher wear and erosion resistances are.

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Possible Strategies for Microstructure Control of Liquid-Phase-Sintered Silicon Carbide Ceramics

  • Chun, Yong-Seong;Kim, Young-Wook
    • Journal of the Korean Ceramic Society
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    • v.42 no.8 s.279
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    • pp.542-547
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    • 2005
  • Keys to the attainment of tailored properties in SiC ceramics are microstructure control and judicious selection of the sintering additives. In this study, three different strategies for controlling microstructure of liquid-phase-sintered SiC ceramics (LPS-SiC) have been suggested: control of the initial $\alpha-SiC$ content in the starting powder, a seeding technique, and a post-sintering heat treatment. The strategies suggested offer substantial flexibility for producing toughened SiC ceramics whereby grain size, grain size distribution, and aspect ratio can be effectively controlled. The present results suggest that the proposed strategies are suitable for the manufacture of toughened SiC ceramics with improved toughness.

Texture Development in Liquid-Phase-Sintered β -SiC by Seeding with β -SiC Whiskers

  • Kim, Won-Joong;Roh, Myong-Hoon
    • Journal of the Korean Ceramic Society
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    • v.43 no.3 s.286
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    • pp.152-155
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    • 2006
  • Silicon carbide ceramics seeded with 10-30 wt% SiC whiskers are fabricated by hot pressing and annealing. A quantitative texture analysis including calculation of the Orientation Distribution Function (ODF) is used for obtaining the degrees of preferred orientation of the fabricated samples. The microstructure and crystallographic texture are discussed with respect to the effect of ${\beta}-SiC$ whisker seeds on the resulting fracture toughness values. The SEM microstructures and the texture data reveal a correlation between texture and fracture toughness anisotropy.

Texture in hot-pressed silicon carbide (고온가압소결한 탄화규소의 집합조직)

  • 김영욱;김원중
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.5 no.4
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    • pp.343-350
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    • 1995
  • A Abstract Systematic studies of the effects of crystalline forms of starting powders and p processing variables on the texture of hot - pressed silicon carbide are described. The results I indicate that hot - pressing of $\beta$ - SiC can produce strong textures and composite type duplex microstructure due to the ${\beta} {\rightarrow} {\alpha}$ phase transformation of SiC. The texture variations d during post - annealing have been observed. In the case of using a - SiC as starting pow¬d ders, the degree of preferred orientation by hot - pressing is relatively weak.

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Synthesis of Silicon Carbide Nanowhiskers from Coconut Fibres and Sol-Gel Derived Silica

  • Raman, V.;Bhatia, G.;Mishra, A.;Saha, M.;Sengupta, P.R.;Srivastava, A.K.
    • Carbon letters
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    • v.7 no.3
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    • pp.166-170
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    • 2006
  • Silicon carbide whiskers ($SiC_w$) having the diameter in the range of 20-80 nm were synthesised from coconut fibres through sol-gel process. The coconut fibres were impregnated with tetraethoxysilane and methyltriethoxysilane derived sol and pyrolyzed at $1400^{\circ}C$ in argon. X-ray of the pyrolyzed samples showed the formation of ${\beta}$-SiC.

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