• 제목/요약/키워드: sigma phase

검색결과 264건 처리시간 0.032초

천체망원경용 비구면 반사경 표면조도 향상을 위한 최적연삭변수 수치결정모델 (GRINDING OPTIMIZATION MODEL FOR NANOMETRIC SURFACE ROUGHNESS FOR ASPHERIC ASTRONOMICAL OPTICAL SURFACES)

  • 한정열;김석환;김건희;한인우;양순철
    • Journal of Astronomy and Space Sciences
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    • 제22권1호
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    • pp.13-20
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    • 2005
  • 지상 및 우주 천체 망원경용 비구면 반사경면 초기 제작공정에는 고정입자 휠을 사용하는 연삭이 있다. 본 연구에서는 매 연삭 가공 이전에 설정한 목표 표면조도를 달성할 수 있도록 입력 연삭변수들을 결정하고, 표면 가공오차를 추적하며 , 가공 경과시간을 최소화하는 새로운 연삭공정을 개발하였다. 특별히 이 공정 기법은 이전 연삭 가공 작업시 까지 수집된 입력 변수 및 가공 결과 표면조도 자료를 다 변수 회귀분석 방법에 대입하여 목표 표면조도에 따른 최적 연삭가공 입력변수를 매 가공 작업 시 진화적으로 제시하는 지능형 공정 조절 능력을 갖추고 있다. 개발된 공정기법과 초정밀 컴퓨터 수치제어 연삭기를 사용하여 $96.1\~65.0nm(Ra)$ 범위 의 목표 표면조도를 갖는 제로듀어 소재에 대하여 10회 가공 실험을 수행 한 결과 $=-0.906{\pm}3.38(\sigma)nm(Ra)$의 가공 정밀도를 달성하여, 지능형 연삭공정의 효율을 입증하였다. 이러한 연구결과는 천체망원경용 반사경면 연삭 가공 시 정성적 경험에 의존하여 가공하는 기존 기술을 극복하고 정량적 수치 모형에 의하여 가공소요시간 최소화 및 나노미터 급 표면조도를 달성하는 진화형 공정 최적화 기술의 확립이라는 의의를 가지고 있다.

기체 분리막의 투과 특성 예측 모델식 개발 (Predictive Thermodynamic Model for Gas Permeability of Gas Separation Membrane)

  • 김종환;홍성규;박상진
    • Korean Chemical Engineering Research
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    • 제45권6호
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    • pp.619-626
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    • 2007
  • 막을 이용한 분리 공정은 상(phase) 변화가 없고 낮은 에너지 소비, 장치의 간소화, 큰 선택성, 가공의 용이성, 낮은투자 및 운용비용 등 여러 가지 장점으로 인하여 다른 방법들에 비해 분리가 간단하다는 장점 때문에 여러 분야에서 광범위하게 응용되고 있다. 여러 가지 기체 분리 방법 중 막을 이용한 기체 분리는 막 층 내에서의 기체 분자의 투과성의 차이를 이용하여 기체 분리를 할 수 있다. 이러한 기체 투과 특성을 예측하기 위해서 본 연구에서는 PDMS, ${\gamma}-radiated$ PDMS, PTFE, PTFE-X 기체 분리막을 선택하였다. 네 가지 분리막의 기체 투과 실험의 결과를 이용하여 열역학적으로 고찰, 분석 후 실험데이터의 reduction 및 regression을 통하여 온도, 압력등의 외부 조건과 기체 분자의 열역학적 특성값에 따른 기체 투과특성 예측식을 개발하였다. 이렇게 개발된 예측식으로 구한 값과 실험데이터를 비교하여 객관적 신뢰성을 확인하였다. 이로 인하여 분리막이 분리 조건과 각각의 기체의 열역학적 특성값($\sigma$, $\varepsilon/k$)으로 기체 투과특성을 알 수 있으므로 예측식을 여러 분야에서 활용할 수 있다 하겠다.

Growth of Hexagonal Boron Nitride Thin Films on Silicon Using a Single Source Precursors

  • Boo, Jin-Hyo;Lee, Soon-Bo;Casten Rohr;Wilson Ho
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 1998년도 제14회 학술발표회 논문개요집
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    • pp.120-120
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    • 1998
  • Boron nitride (BN) films have attracted a growing interest for a variety of t technological applications due to their excellent characteristics, namely hardness, c chemical inertness, and dielectrical behavior, etc. There are two crystalline phases 1551; of BN that are analogous to phases of carbon. Hexagonal boron nitride (h-BN) has a a layered s$\sigma$ucture which is spz-bonded structure similar to that of graphite, and is t the stable ordered phase at ambient conditions. Cubic boron nitride (c-BN) has a z zinc blende structure with sp3-bonding like as diamond, 따ld is the metastable phase a at ambient conditions. Among of their prototypes, especially 삼Ie c-BN is an i interesting material because it has almost the same hardness and thermal c conductivity as di없nond. C Conventionally, significant progress has been made in the experimental t techniques for synthesizing BN films using various of the physical vapor deposition 밍ld chemical vapor deposition. But, the major disadvantage of c-BN films is that t they are much more difficult to synthesize than h-BN films due to its narrow s stability phase region, high compression stress, and problem of nitrogen source c control. Recent studies of the metalorganic chemical vapor deposition (MOCVD) of I III - V compound have established that a molecular level understanding of the d deposition process is mandatory in controlling the selectivity parameters. This led t to the concept of using a single source organometallic precursor, having the c constituent elements in stoichiometric ratio, for MOCVD growth of 삼Ie required b binary compound. I In this study, therefore, we have been carried out the growth of h-BN thin f films on silicon substrates using a single source precursors. Polycrystalline h-BN t thin films were deposited on silicon in the temperature range of $\alpha$)() - 900 $^{\circ}$C from t the organometallic precursors of Boron-Triethylamine complex, (CZHs)3N:BRJ, and T Tris(dimethylamino)Borane, [CH3}zNhB, by supersonic molecular jet and remote p plasma assisted MOCVD. Hydrogen was used as carrier gas, and additional nitrogen w was supplied by either aDlIDonia through a nozzle, or nitrogen via a remote plasma. T The as-grown films were characterized by Fourier transform infrared spectroscopy, x x-ray pthotoelectron spectroscopy, Auger electron spectroscopy, x-ray diffraction, t transmission electron diffraction, optical transmission, and atomic force microscopy.roscopy.

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방사선조사 후 타액선 세포와 혈관 내피세포의 DNA합성에 관한 면역조직학적 연구 (AN IMMUNOHISTOCHEMICAL STUDY ON DNA SYNTHESIS OF SALIVARY GLAND TISSUE CEllS AND ENDOTHELIAL CELL AFTER IRRADIATION)

  • 신종섭;유동수
    • 치과방사선
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    • 제21권2호
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    • pp.183-197
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    • 1991
  • After single fraction of 2, 5, 10 Gy irradiation on submandibular gland of 40 male rats, weighing 150gm, respectively, these animal were sacrificed two hours after 0.1㎎/g bromodeoxyuridine (Sigma) peritoneal injection in 1, 3, 7, 15 hours, 1, 3, 7 days after irradiation. And excised submandibular gland were fixed in Carnoy's and Bouin's solution for 2 hours. Paraffin sections were stained with H&E, and PAS for the observation of the change of salivary gland tissue, and with Feulgen for the study of the DNA distribution, and immunohistochemically stained with anti-bromodeoxyuridine (Sanbyo Co.) for detection of DNA synthetic cells in order to study the distribution of DNA synthetic cells of salivary gland tissue and endothelium after irradiation in 5 different sites of 6 slides on X 200 high power field. The results were as followings. 1. In PAS staining 3 days after 5Gy irradiation, decreased mucine secretion of serous cells were found, and 7 days after l0Gy irradiation, decreased mucine secretion of mucous cells were found. 2. In histopathologic features, degeneration of serous cells were found in 3 days after 2 Gy irradiation and there was little change in mucous cells and excretory duct cells. 3. In Feugen staining, 3 days after 2 Gy, 5 Gy irradiation, more high percentage of DNA synthetic cells were found in intercalated duct cells, striated duct cells and excretory duct cells than in BrdU staining. 4. In immunohistochemical features, DNA synethsis of serous cells and granular convoluted tubular cells abruptly decreased in early period after irradiation and showed no recovery in 7 days after irradiation but there was an increase in DNA synthesis of intercalated duct cells, striated duct cells and excretory duct cells, which have less S-phase cells comparatively, in 7 days after 2 Gy, 5 Gy irradiation. 5. In immunohistochemical features, the DNA synthesis of endothelial cells was continuously decreased after irradiation but showed slight increase in 7 days after 2 Gy and S Gy irradiation.

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전력증폭기의 효율 및 선형성 개선을 위한 포락선 제거 및 복원 송신기 (Envelope Elimination and Restoration Transmitter for Efficiency and Linearity Improvement of Power Amplifier)

  • 조영균;김창완;박봉혁
    • 한국전자파학회논문지
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    • 제26권3호
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    • pp.292-299
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    • 2015
  • 본 논문에서는 3-레벨 인코딩 기법을 적용하여 시스템의 효율과 선형성을 개선할 수 있는 새로운 구조의 EER 송신기를 제안하였다. 제안된 송신기는 첨두 전력 대 평균 전력비에 상관없이 동일한 크기의 신호만을 증폭하고, 채널대역 내의 양자화 노이즈를 감소시켜 높은 효율을 얻을 수 있으며, 포락선 신호와 위상 신호 간 시간 부정합 특성을 개선하여 높은 선형성을 가질 수 있도록 하였다. 130 nm CMOS 공정으로 제작된 송신기 칩은 8.5 dB의 첨두 전력 대 평균전력비를 갖는 LTE 20 MHz 신호에 대해 2.13 GHz의 반송주파수에서 3.7 %의 오류 벡터 크기와 37.5 dBc의 인접 채널 누설비 특성을 보인다.

0.2% N을 첨가한 수퍼 2상 스테인리스강의 열처리 조건에 따른 특성 평가 - 제3보: 부식특성 (Characteristic Evaluation according to Heat Treatment Conditions of Super Duplex Stainless Steel with Additive 0.2% N - Part 3: Corrosion Characteristic)

  • 안석환;강흥주;서현수;남기우;이건찬
    • 한국해양공학회지
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    • 제23권5호
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    • pp.85-91
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    • 2009
  • A stainless steel that contains aggressive negative ion was known to decrease the corrosion resistance. Stainless steel with super corrosion resistance was developed for improvement of corrosion resistance. Super duplex stainless steel is widely used under sever environment because of good mechanical properties and corrosion resistance. Also, Super duplex stainless steel has long life in severe environments by showing the enough strength and corrosion resistance. But duplex stainless steel is not stabilized compared to austenite stainless steel in corrosion resistance. In this study, corrosion characteristic were investigated to super duplex stainless steel with additive 0.2% nitrogen with $SiO_2$ thin films coated or no coated by sol-gel method in 3.5% NaCl. From test results, corrosion current density in the heat-treated specimen for ${\sigma}$ phase precipitation was higher than that of different heat-treated specimen. Also, $SiO_2$ colloidal-coated specimen had not occurred almost corrosion.

고출력 펄스응용을 위한 고전압 펄스변압기 최적설계 (Design Optimization of High-Voltage Pulse Transformer for High-Power Pulsed Application)

  • 장성덕;강흥식;박성주;한영진;조무현;남궁원
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2008년도 제39회 하계학술대회
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    • pp.1297-1300
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    • 2008
  • A conventional linear accelerator system requires a flat-topped pulse with less than ${\pm}$ 0.5% ripple to meet the beam energy spread requirements and to improve pulse efficiency of RF systems. A pulse transformer is one of main determinants on the output pulse voltage shape. The pulse transformer was investigated and analyzed with the pulse response characteristics using a simplified equivalent circuit model. The damping factor ${\sigma}$ must be >0.86 to limit the overshoot to less than 0.5% during the flat-top phase. The low leakage inductance and distributed capacitance are often limiting factors to obtain a fast rise time. These parameters are largely controlled by the physical geometry and winding configuration of the transformer. A rise time can be improved by reducing the number of turns, but it produces larger pulse droop and requires a larger core size. By tradeoffs among these parameters, the high-voltage pulse transformer with a pulse width of 10 ${\mu}s$, a rise time of 0.84 ${\mu}s$, and a pulse droop of 2.9% has been designed and fabricated to drive a klystron which has an output voltage of 284 kV, 30-MW peak and 60-kW average RF output power. This paper describes design optimization of a high-voltage pulse transformer for high-power pulsed applications. The experimental results were analyzed and compared with the design. The design and optimal tuning parameter of the system was identified using the model simulation.

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Molecular Characterization of Regulatory Genes Associated with Biofilm Variation in a Staphylococcus aureus Strain

  • Kim, Jong-Hyun;Kim, Cheorl-Ho;Hacker, Jorg;Ziebuhr, Wilma;Lee, Bok-Kwon;Cho, Seung-Hak
    • Journal of Microbiology and Biotechnology
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    • 제18권1호
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    • pp.28-34
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    • 2008
  • Biofilm formation in association with the intercellular adhesion (icaADBC) gene cluster is a serious problem in nosocomial infections of Staphylococcus aureus. In all 112 S. aureus strains tested, the ica genes were present, and none of these strains formed biofilms. The biofilm formation is known to be changeable by environmental factors. We have found about 30% of phase variation in these strains with treatment of tetracycline, pristinamycin, and natrium chloride. However, this phenotype disappeared without these substances. Therefore, we have constructed stable biofilm-producing variants through a passage culture method. To explain the mechanism of this variation, nucleotide changes of ica genes were tested in strain S. aureus 483 and the biofilm-producing variants. No differences of DNA sequence in ica genes were found between the strains. Additionally, molecular analysis of three regulatory genes, the accessory gene regulator (agr) and the staphylococcal accessory regulator (sarA), and in addition, alternative transcription factor ${\sigma}^B$ (sigB), was performed. The data of Northern blot and complementation showed that SigB plays an important role for this biofilm variation in S. aureus 483 and the biofilm-producing variants. Sequence analysis of the sigB operon indicated three point mutations in the rsbU gene, especially in the stop codon, and two point mutations in the rsbW gene. This study shows that this variation of biofilm formation in S. aureus is deduced by the role of sigB, not agr and sarA.

Effect of Carbon on the Coefficient of Thermal Expansion of As-Cast Fe-3 0 wt.%Ni-12.5wt.% Co-xC Invar Alloys

  • 김봉서;유경재;김병걸;이희웅
    • 소성∙가공
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    • 제8권3호
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    • pp.247-247
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    • 1999
  • The segregation (distribution) of nickel and the composition of its constituents influence the low thermal expansion characteristics (Invar effect) in Fe-30 wt.% Ni-12.5 wt.% Co-xC Invar alloy. The change of coefficient of the thermal expansion and magnetic properties were studied as an aspect of carbon addition causing the segregation of Ni in primary austenite of as-cast Fe-30 wt.% Ni-12.5 wt.% Co Invar alloy. The coefficient of thermal expansion of Fe-30 wt.% Ni-12.5 wt.% Co-xC Invar alloy showed its lowest value at 0.08 wt.% carbon, increased with increasing carbon content in the range of 0.08-1.0 wt.%C, kept constant at 1.0-2.0 wt.%C and decreased at carbon higher than 2.0 wt.%. The effective distribution of the coefficient of nickel in as-cast Fe-30 wt.% Ni-12.5 wt.% Co-xC Invar alloy increased with increasing carbon content. The volume fraction of they phase of Fe-30 wt.% Ni-12.5 wt.% Co-xC alloy increased with increasing carbon content. The microstructure of Fe-30 wt.% Ni-12.5 wt.% Co-xC alloy changed with the carbon content was independent of the coefficient of thermal expansion. The Curie temperature changed linearly with the carbon content and was similar to the change of the coefficient of thermal expansion. Moreover, the coefficient of thermal expansion decreased when the ratio of saturation magnetization to Curie temperature ($\sigma_s/T_c$) increased, decreasing the Curie temperature and showed a specific relationship with the magnetic properties of the Fe-30 wt.% Ni-12.5 wt.% Co-xCInvar alloy.

합류식 하수관거의 유출 특성 분석 조사 (Characteristics and Combined Sewer Overflows)

  • 안기선;장성용;권영호
    • 한국환경과학회지
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    • 제19권6호
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    • pp.747-753
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    • 2010
  • It follows in quality and sewage exclusion method of the investigation objective sector and the Combined Sewer Overflows which is suitable in regional characteristics and the confluence area against the rainfall initially a flow and the medulla and measurement - it analyzes the initial rainfall outflow possibility control plan which is suitable in the domestic actual condition and it proposes the monitor ring plan for the long-term flow and pollution load data accumulation. From the research which it sees the Infiltration water/Influent water and CSOs investigation it passes by the phase of hazard chain and Namwon right time 4 it does not hold reverse under selecting, Measurement it used the hazard automatic flow joint seal Sigma 910 machine and in case 15 minute interval of the I/I, it measured a flow at case 5, 15 minute standing of the CSOs. The water quality investigation for the water leakage investigation of the I/I and the sewage from the point which is identical with flow measurement during on-the-spot inspection duration against 6 items which include the BOD sampling and an analysis, when the rainfall analysis for CSOs fundamental investigation analyzed against 18 items which include the BOD sampling. Consequently, for the optimum interpretation invasion water / inflow water of the this investigation area day average the lowest flow - water quality assessment veterinarian optimum interpretation hazard average per day - lowest flow - it averages a medulla evaluation law department one lowest flow evaluation technique and it selects, it presentation collectively from here it gets, position result with base flow analysis of invasion water / inflow water.