• 대한치과교정학회지
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• 제22권2호
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• pp.327-343
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• 1992

Metal brackets and ceramic brackets were bonded to natural teeth, porcelain crowns and gold crowns After stored in artificial saliva solution for 72 hours at $37^{\circ}C$, the shear bond strengths were measured by Instron and compared with them, the bonding sites and bracket bases were examined by scanning electron microscope and light optical stereomicroscope. The results were as follows: 1. The shear bond strengths of the group which metal brackets were bonded to natural teeth and the groups which ceramic brackets were bonded to natural teeth and porcelain crowns were comparable to each other, the shear bond strength of the group which metal brackets were bonded to gold crowns was significantly low. 2. The bond failed predominantly at the bracket base/adhesive interface with the bulk of adhesive remaining on enamel in the group which metal brackets were bonded to natural teeth. 3. The bond failed consistently at the crown/adhesive interface with all of adhesive remaining on the bracket babes in the group which metal brackets were bonded to gold crowns. 4. The bond failed at the enamel or crown/adhesive interface with the bulk of adhesive remaining on the bracket bases in the groups which cramic brackets were bonded to natural teeth and porcelain crowns. 5. The shear bond strengths of the groups which ceramic brackets were bonded to porcelain crowns were not affected by etching time.

• The Journal of Advanced Prosthodontics
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• 제7권1호
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• pp.47-50
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• 2015

PURPOSE. This study aimed to discover a way to increase the bond strength between bis-acryl resins, using a comparison of the shear bond strengths attained from bis-acryl resins treated with light curing, pressure, oxygen inhibition, and heat. MATERIALS AND METHODS. Self-cured bis-acryl resin was used as both a base material and as a repair material. Seventy specimens were distributed into seven groups according to treatment methods: pressure - stored in a pressure cooker at 0.2 Mpa; oxygen inhibition- applied an oxygen inhibitor around the repaired material,; heat treatment - performed heat treatment in a dry oven at $60^{\circ}C$, $100^{\circ}C$, or $140^{\circ}C$. The shear bond strength was measured with a universal testing machine, and the shear bond strength (MPa) was calculated from the peak load of failure. A comparison of the bond strength between the repaired specimens was conducted using one-way ANOVA and Tukey multiple comparison tests (${\alpha}$=.05). RESULTS. There were no statistically significant differences in the shear bond strength between the control group and the light curing, pressure, and oxygen inhibition groups. However, the heat treatment groups showed statistically higher bond strengths than the groups treated without heat, and the groups treated at a higher temperature resulted in higher bond strengths. Statistically significant differences were seen between groups after different degrees of heat treatment, except in groups heated at $100^{\circ}C$ and $140^{\circ}C$. CONCLUSION. Strong bonding can be achieved between a bis-acryl base and bis-acryl repair material after heat treatment.

• Restorative Dentistry and Endodontics
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• 제43권1호
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• pp.7.1-7.7
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• 2018

Objectives: The aim of this study is to compare the shear bond strengths of ceramic brackets bonded to zirconia surfaces using different zirconia primers and universal adhesive. Materials and Methods: Fifty zirconia blocks ($15{\times}15{\times}10mm$, Zpex, Tosoh Corporation) were polished with 1,000 grit sand paper and air-abraded with $50{\mu}m$ $Al_2O_3$ for 10 seconds (40 psi). They were divided into 5 groups: control (CO), Metal/Zirconia primer (MZ, Ivoclar Vivadent), Z-PRIME Plus (ZP, Bisco), Zirconia Liner (ZL, Sun Medical), and Scotchbond Universal adhesive (SU, 3M ESPE). Transbond XT Primer (used for CO, MZ, ZP, and ZL) and Transbond XT Paste was used for bracket bonding (Gemini clear ceramic brackets, 3M Unitek). After 24 hours at $37^{\circ}C$ storage, specimens underwent 2,000 thermocycles, and then, shear bond strengths were measured (1 mm/min). An adhesive remnant index (ARI) score was calculated. The data were analyzed using one-way analysis of variance and the Bonferroni test (p = 0.05). Results: Surface treatment with primers resulted in increased shear bond strength. The SU group showed the highest shear bond strength followed by the ZP, ZL, MZ, and CO groups, in that order. The median ARI scores were as follows: CO = 0, MZ = 0, ZP = 0, ZL = 0, and SU = 3 (p < 0.05). Conclusions: Within this experiment, zirconia primer can increase the shear bond strength of bracket bonding. The highest shear bond strength is observed in SU group, even when no primer is used.

• Restorative Dentistry and Endodontics
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• 제22권2호
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• pp.680-692
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• 1997

New bonding agent systems have been supplied which operators can simply apply to conditioned tooth surfaces. The purpose of this study was to evaluate the shear bond strengths and the microleakages of three bonding agents and composite resins to dentin. Seventy-five extracted human maxillary and mandibular molar teeth were used in this study. For the shear bond strength test, the entire occlusal dentin surfaces of thirty teeth were exposed with Diamond Wheel Saw and smoothed with Lapping and Polishing Machine (South Bay Technology Co., U.S.A). For the microleakage test, Class V cavities were prepared in the buccal surfaces of fourtyfive teeth. They were randomly assigned into 3 groups according to dentin bonding agents ($Scotchbond^{TM}$ Multi-Purpose plus, ONE-$STEP^{TM}$ and Prime & $Bond^{TM}$)and composite resins (Z-100, $Aelitefil^{TM}$ and TPH $Spectrum^{TM}$) to be used. Bonding agents and composite resins were bonded to exposed dentin surfaces of the tooth crown and to Class V cavities on the buccal surfaces respectively according to manufacturer's directions. The shear bond strengths were measured by universal testing machine($U^{TM}$ AGS-100, Japan). In addition, the degree of micro leakage at the occlusal and gingival margin was examined by 2 % methylene blue and stereomicroscope(Olymous SZH 10, Japan). The results were as follows: 1. The shear bond strength to dentin was the highest value in SBMP-Plus group($16.68{\pm}7.38$ MPa) and the lowest value in Prime & Bond group($11.61{\pm}5.82$ MPa), but there was no significant difference of shear bond strength among three groups. 2. The degree of microleakage at both occlusal and gingival margin was showed the lowest in SBMP-Plus group and the highest in ONE-STEP group. 3. At both occlusal and gingival margin, there was significant difference of microleakage between SBMP-Plus and ONE-STEP/ Prime & Bond groups(p<0.05), but no significant difference of microleakage between ONE-STEP and Prime & Bond group(p>0.05).

• Restorative Dentistry and Endodontics
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• 제15권1호
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• pp.201-216
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• 1990

A variety of surface pre-treatments have been advocated to prepare the dentin prior to placement of a bonding agent. The purpose of this study was to evaluate the effect of various dentin conditioners upon the degree of resin impregnation to the dentinal tubules and the shear bond strength of a new dentinal bonding agent (Scotchbond 2) used in conjunction with a visible light cured composite (Silux). The healthy eighty human molars extracted due to periodontal or orthodontic reasons were used and randomly divided into five groups. All the grinded dentin surfaces were conditioned with 3% $H_2O_2$, Cavity Cleanser (Columbus/Bayer), Dentin Conditioner (GC Inter. Corp.), Scotchprep (3M Co.) according to the manufacturer's directions. The specimens were then demineralized in 10% HCl for 20 sec. and 24 hrs. in order to observe the resin tags in Hitachi X-450 scanning electron microscope at 25KV. Also, shear strengths were obtained using an Instron Testing Machine with a cross head speed of 1 mm/min. The following results were obtained ; 1. In group treating with Dentin Conditioner and Scotchprep, the resin strings were formed on most of the surfaces and penetrated more than $50{\mu}m$ into the tubules. 2. The inner surface of resin treated with Cavity Cleanser, indicating the resin strings formed partly and penetrated about in depth of $30{\mu}m$. 3. In control and experimental group treated with 3% $H_2O_2$, the resin tags were not formed, if any, penetrated shortly. 4. Shear bond strengths in groups treating with Dentin Conditioner and Scotchprep were statistically significant increase than with 3% $H_2O_2$. (P<0.01). 5. The Scotchprep treatment group was significantly higher in shear strength than groups treated with no conditioning and Cavity Cleanser.(P<0.01) 6. Shear bond strengths evaluated were gradually increase in proportion to the tag length of resin impregnation.

• 한국지반신소재학회논문집
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• 제16권2호
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• pp.55-66
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• 2017

본 연구에서는 지반 특성에 관계없이 일률적으로 적용되는 피에조콘 관입속도 2cm/s 조건 하에서, 저소성 실트 지반의 경우 부분배수 내지는 완전 배수 현상이 발생된다는 관점에서 저소성 실트 지반의 비배수전단강도선과 완전배수 전단강도선 사이에서의 피에조콘계수($N_{kt}$)에 의한 전단강도 분포 경향을 기준으로 부분배수 전단강도를 평가하였다. 그 결과, 인천, 화성 및 군산 저소성 실트 지반의 부분배수 내부마찰각(${\varphi}^{\prime}$)은 $3{\sim}15^{\circ}$에서 분포하는 것으로 분석되었다. 한편, 강제치환 역해석 결과 및 비압밀비배수 삼축시험으로부터 얻어진 내부마찰각(${\varphi}^{\prime}$)은 소성지수 감소에 따라 $2{\sim}14^{\circ}$의 범위에서 분포되어, CPTU 데이터에 의한 부분배수 내부마찰각(${\varphi}^{\prime}$)과 유사한 경향을 나타내어 이에 대한 적용성을 확인할 수 있었다.

• The Journal of Advanced Prosthodontics
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• 제12권6호
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• pp.376-382
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• 2020

PURPOSE. To determine the shear bond strengths of different denture base resins to different types of prefabricated teeth (acrylic, nanohybrid composite, and cross-linked) and denture teeth produced by computer-aided design/computer-aided manufacturing (CAD/CAM) technology. MATERIALS AND METHODS. Prefabricated teeth and CAD/CAM (milled) denture teeth were divided into 10 groups and bonded to different denture base materials. Groups 1-3 comprised of different types of prefabricated teeth and cold-polymerized denture base resin; groups 4-6 comprised of different types of prefabricated teeth and heat-polymerized denture base resin; groups 7-9 comprised of different types of prefabricated teeth and CAD/CAM (milled) denture base resin; and group 10 comprised of milled denture teeth produced by CAD/CAM technology and CAD/CAM (milled) denture base resin. A universal testing machine was used to evaluate the shear bond strength for all specimens. One-way ANOVA and Tukey post-hoc test were used for analyzing the data (α=.05). RESULTS. The shear bond strengths of different groups ranged from 3.37 ± 2.14 MPa to 18.10 ± 2.68 MPa. Statistical analysis showed significant differences among the tested groups (P<.0001). Among different polymerization methods, the lowest values were determined in cold-polymerized resin.There was no significant difference between the shear bond strength values of heat-polymerized and CAD/CAM (milled) denture base resins. CONCLUSION. Different combinations of materials for removable denture base and denture teeth can affect their bond strength. Cold-polymerized resin should be avoided for attaching prefabricated teeth to a denture base. CAD/CAM (milled) and heat-polymerized denture base resins bonded to different types of prefabricated teeth show similar shear bond strength values.

• 한국지반공학회논문집
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• 제30권5호
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• pp.37-46
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• 2014

다양한 지반조건을 갖고 있는 지반구조물들은 공사 설계에 대한 특성에 따라 안정성 해석을 하여 설계와 시공이 되어야 한다. 일반적으로 지반의 강도정수들은 삼축압축시험으로 분석한 결과를 설계시공에 적용하여 안정성을 해석한다. 띠하중과 같은 응력을 받고 있는 댐, 제방, 옹벽 등은 한방향의 변형이 구속되어 있는 평면변형 조건의 지반구조물들이다. 지반 조건에 맞는 안정성 해석은 적절한 강도정수들의 적용에 의해서 이루어져야 한다. 삼축압축시험에 의한 강도정수 적용은 이러한 지반구조물들을 설계할 때, 안전율이 과소평가되어 시공성과 경제성에 불리하게 작용한다. 본 연구는 화강풍화토를 대상으로 삼축압축시험과 평면변형시험을 통하여 강도정수를 산정하고 상대밀도에 따른 강도 증가에 대한 경향을 분석하고자 한다. 삼축압축시험은 응력경화가 지속적으로 발생하기 때문에 최대 변형률 15%에서 한계파괴응력을 결정짓는 반면에, 평면변형 조건에서 수행되는 시험은 강도가 증가하면서 2번의 뚜렷한 응력경화를 나타내었고, 강도정수를 결정할 수 있는 항복응력을 구분할 수 있었다.

• 대한소아치과학회지
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• 제34권1호
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• pp.81-90
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• 2007

본 연구에서는 세 가지 서로 다른 광원(할로겐 램프 :. Elipar Trilight ; 3M ESPE, Seefeld, Germany, Light Emitting Diode (LED) ; Elipar Freelight2 ; 3M ESPE, Seefeld, Germany, 플라즈마 광 : Flipo ; LOKKI, France)을 사용하여 브라켓과 광원사이의 거리에 따른 광중합형 글라스 아이오노머 시멘트(Fuji ORTHO LC : GC, Japan)의 전단 결합 강도를 알아보고자 하였다. 1. 광중합기에 따른 전단 결합 강도는 광중합기로부터 브라켓까지의 거리가 0mm일 때 3가지 광원에 유의할 만한 차이는 보이지 않았고 광중합기로부터 브라켓까지의 거리가 3mm, 6mm일 때, 할로겐 광과 플라즈마 광 사이에는 유의할 만한 차이가 없었으나 LED 광은 유의성 있게 낮은 전단 결합 강도를 나타냈다. 2. 할로겐 광과 플라즈마 광으로 광중합시 거리에 따른 전단 결합 강도에 유의한 차 없었고 LED광을 사용하여 광중합시에는 거리가 증가할수록 전단 결합 강도가 감소하였다. 특히 0mm에서 3mm로 거리가 증가시 유의할 만한 감소를 나타내었다.

• 한국지반공학회논문집
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• 제33권12호
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• pp.7-20
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• 2017

본 연구에서는 전단특성 및 유변학적 정수를 모두 산정할 수 있는 직접전단실험 장비를 이용하여 조립토와 세립토에 대하여 전단강도 및 유변학적 특성에 대한 입도분포의 영향을 조사하고자 하였다. 최대입경 0.075mm의 세립토와 최대입경이 0.425mm이고, 세립분 함량이 17%인 조립토를 건조상태와 액성한계상태로 조성하여, 산사태 분류기준에 따라 재활성 산사태(reactivated landslide) 혹은 붕괴직후 토석류 속도에 해당하는 전단속도에 대하여 전단강도를 산정하였다. 또한, 유변학적 특성 평가를 위해 액성한계상태로 조성된 조립토와 세립토에 대하여 서로 다른 세 가지의 전단변형률속도로 반복적으로 전단하며 잔류전단강도를 측정하였다. 측정된 잔류전단강도와 전단변형률속도와의 관계를 통해 빙햄모델의 소성 점도와 항복응력을 산정하였다. 건조 및 액성한계상태에서 조성된 시료에 대하여 첨두전단강도에서 산정한 점착력의 경우, 세립토에서 조립토보다 더 크게 산정되었으며, 내부마찰각은 조립토에서 더 크게 산정되었다. 유변학 정수의 경우, 소성 점도와 항복응력이 조립토보다 세립토에서 더 큰 것으로 나타났다. 본 연구는 재활성 산사태 혹은 붕괴직후 토석류의 거동예측에 효과적으로 활용될 것으로 기대된다.