• Restorative Dentistry and Endodontics
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• v.23 no.1
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• pp.247-256
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• 1998

To evalutate the change in shear bond strength according to dentin surface treatment, 4 materials were divided into control group(A) and experimental group(B). Group A was treated according to the instruction of manufacture. Group B was treated with 32% phosphoric acid. After dentin surface treatment, each material was bonded and stored in 100% humidity during 7 days, and then, the shear bond strength was evaluated. The results were as follows: 1. In the case of treatment according to the instruction of manufacture, the shear bond strength according to material showed Z-100 to be highest with 12.42 MPa, Compoglass had the lowest shear bond strength with 4.23 MPa and there was significant difference between Compoglass and Z-100, Dyract (p<0.01). 2. The group treated with 32% phosphoric acid showed lower shear bond strength than that of the group treated according to the instruction of manufacture but there was no statistical significance. 3. As a result of observation under SEM, the fracture pattern was a mixture of cohesive and adhesive failure in group 1, and there was more adhesive failure in group 2, and in group 3 and 4 there was cohesive failure of material or tooth structure. From the results above Dyract showed shear bond strength levels between resin and resin -modified glass ionomer but Compoglass showed much lower shear bond strength than that of resin-modified glass ionomer thus indicating that even though they are the same type of material they show evident differences in physical properties. And it is thought that the treatment of dentin surface with phosphoric acid did not increase the shear bond strength, unlike enamel.

• Computers and Concrete
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• v.24 no.1
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• pp.37-49
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• 2019

In this study, the shear behaviour of reinforced concrete (RC) beams that were retrofitted using precast panels of ultra-high performance fiber reinforced concrete (UHPFRC) is presented. The precast UHPFRC panels were glued to the side surfaces of RC beams using epoxy adhesive in two different configurations: (i) retrofitting two sides, and (ii) retrofitting three sides. Experimental tests on the adhesive bond were conducted to estimate the bond capacity between the UHPFRC and normal concrete. All the specimens were tested in shear under varying levels of shear span-to-depth ratio (a/d=1.0; 1.5). For both types of configuration, the retrofitted specimens exhibited a significant improvement in terms of stiffness, load carrying capacity and failure mode. In addition, the UHPFRC retrofitting panels glued in three-sides shifted the failure from brittle shear to a more ductile flexural failure with enhancing the shear capacity up to 70%. This was more noticeable in beams that were tested with a/d=1.5. An approach for the approximation of the failure capacity of the retrofitted RC beams was evolved using a multi-level regression of the data obtained from the experimental work. The predicted values of strength have been validated by comparing them with the available test data. In addition, a 3-D finite element model (FEM) was developed to estimate the failure load and overall behaviour of the retrofitted beams. The FEM of the retrofitted beams was conducted using the non-linear finite element software ABAQUS.

• Steel and Composite Structures
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• v.13 no.5
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• pp.473-487
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• 2012

An experimental study was performed to investigate the seismic performance of steel reinforced concrete (SRC) special-shaped columns. For this purpose, 17 steel reinforced concrete special-shaped column specimens under low-cyclic reversed load were tested, load process and failure patterns of the specimens with different steel reinforcement were observed. The test results showed that the failure patterns of these columns include shear-diagonal compression failure, shear-bond failure, shear-flexure failure and flexural failure. The failure mechanisms and characteristics of SRC special-shaped columns were also analyzed. For different SRC special-shaped columns, based on the failure characteristics and mechanism observed from the test, formulas for calculating ultimate shear capacity in shear-diagonal compression failure and shear-bond failure under horizontal axis and oblique load were derived. The calculated results were compared with the test results. Both the theoretical analysis and the experimental results showed that, the shear capacity of T, L shaped columns under oblique load are larger than that under horizontal axis load, whereas the shear capacity of +-shaped columns under oblique load are less than that under horizontal axis load.

• The Journal of Advanced Prosthodontics
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• v.9 no.2
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• pp.130-137
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• 2017

PURPOSE. The purpose of this study was to evaluate the effect of nano-structured alumina surface coating on shear bond strength between Y-TZP ceramic and various dual-cured resin cements. MATERIALS AND METHODS. A total of 90 disk-shaped zirconia specimens (HASS CO., Gangneung, Korea) were divided into three groups by surface treatment method: (1) airborne particle abrasion, (2) tribochemicalsilica coating, and (3) nano-structured alumina coating. Each group was categorized into three subgroups of ten specimens and bonded with three different types of dual-cured resin cements. After thermocycling, shear bond strength was measured and failure modes were observed through FE-SEM. Two-way ANOVA and the Tukey's HSD test were performed to determine the effects of surface treatment method and type of cement on bond strength (P<.05). To confirm the correlation of surface treatment and failure mode, the Chi-square test was used. RESULTS. Groups treated with the nano-structured alumina coating showed significantly higher shear bond strength compared to other groups treated with airborne particle abrasion or tribochemical silica coating. Clearfil SA Luting showed a significantly higher shear bond strength compared to RelyX ARC and RelyX Unicem. The cohesive failure mode was observed to be dominant in the groups treated with nano-structured alumina coating, while the adhesive failure mode was prevalent in the groups treated with either airborne particle abrasion or tribochemical silica coating. CONCLUSION. Nano-structured alumina coating is an effective zirconia surface treatment method for enhancing the bond strength between Y-TZP ceramic and various dual-cured resin cements.

• The Journal of Advanced Prosthodontics
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• v.12 no.5
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• pp.251-258
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• 2020

PURPOSE. The bond strengths between resin denture teeth with various compositions and denture base resins including conventional and CAD/CAM purposed materials were evaluated to find influence of each material. MATERIALS AND METHODS. Cylindrical rods (6.0 mm diameter × 8.0 mm length) prepared from pre-polymerized CAD/CAM denture base resin blocks (PMMA Block-pink; Huge Dental Material, Vipi Block-Pink; Vipi Industria) were bonded to the basal surface of resin teeth from three different companies (VITA MFT^®; VITA Zahnfabrik, Endura Posterio^®; SHOFU Dental, Duracross Physio^®; Nissin Dental Products Inc.) using resin cement (Super-Bond C&B; SUN MEDICAL). As a control group, rods from a conventional heat-polymerizing denture base resin (Vertex™ Rapid Simplified; Vertex-Dental B.V. Co.) were attached to the resin teeth using the conventional flasking and curing method. Furthermore, the effect of air abrasion was studied with the highly cross-linked resin teeth (VITA MFT^®) groups. The shear bond strengths were measured, and then the fractured surfaces were examined to analyze the mode of failure. RESULTS. The shear bond strengths of the conventional heat-polymerizing PMMA denture resin group and the CAD/CAM denture base resin groups were similar. Air abrasion to VITA MFT^® did not improve shear bond strengths. Interfacial failure was the dominant cause of failure for all specimens. CONCLUSION. Shear bond strengths of CAD/CAM denture base materials and resin denture teeth using resin cement are comparable to those of conventional methods.

• Restorative Dentistry and Endodontics
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• v.26 no.2
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• pp.171-179
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• 2001

The purpose of this study was to evaluate the shear bond strength of compomers according to dentin surface treatment. Two materials of compomer were devided into six groups. The compomer used in this study were Dyract AP(D) and F2000(F), Group 1 (DN) and 4(FN) were treated according to manufacturers instructions as control groups. Group 2(DE) and 5(FE) were treated with 37％ phosphoric acid and group 3(DA) and 6(FA) were treated with air abrasion unit (80 psi, 50 m aluminum oxide particles) respectively as experimental groups. After dentin surface treatment, compomers were bonded. Completed samples were stored in 100％ humidity. 37C during 7 days, and then, the shear bond strength of specimens were evaluated. The results were as follows: 1. In the case of Dyract AP, the shear bond strength was showed the highest value of 9.10 MPa in dentin surface treatment with air abrasion unit. but there were no significant differences to the other groups. 2. In the case of F2000. the shear bond strength was showed the highest value of 13.51MPa and there were significant differences to the other groups(p<0.05). 3. The shear bond strength of F2000 was higher than Dyract AP in each dentin surface treatment. and in the case of etching and air abrasion. there were significant differences(p<0.05). 4. As a result of observation of SEM. the most of fracture pattern was adhesive failure in group 1(DN), 2(DE) and 4(FN), and cohesive failure in group 3(DA), S(FE) and 6(FA).

• Journal of Korean Association for Spatial Structures
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• v.18 no.4
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• pp.61-68
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• 2018

Tensile load tests were conducted on High-Shear Ring Anchors (HRAs) after shear load had been applied to the HRAs, which had been developed to reduce the number of the anchors. Test variables include the embedment length of the rod and the width of the specimens and a total of 12 specimens were tested. Test results show that the HRAs pulled out due to bond failure or steel failure occurred in case that the HRAs were installed to the members with 300mm or greater width and the embedment length of 160mm (the actual embedment of rod is 140mm) or deeper. Except 4 HRAs showing steel failure of rod, the minimum and average of test-to-prediction by ACI 318-14 ratios are 1.18 and 1.79, respectively. The tensile strength of HRAs, after shear load was applied to the HRAs, can be safely evaluated by the minimum among the concrete breakout strength and bond strength with the actual embedment length of the rod.

• The Journal of Korean Academy of Prosthodontics
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• v.29 no.3
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• pp.33-41
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• 1991

Cermic has been widely used because of its excellent esthetics and strength. The recently introduced castable ceramic system is regarded as the more esthetic and biocompatible restorative material. The purpose of this study was to compare the shear bond strength of Dicer & G-Cera porcelain laminate veneer according to the type of cement and surface treatment and to observe the surface of bonding failure with SEM. Total forty disks(3.5mm $diam.\times2.0mm$ thickness) were prepared. Forty extracted human maxillary central incisor teeth were stored in saline solution. Ten teeth were bonded to Dicer specimen with Dicer ZPC cement and ten teeth were bonded with Dicer resin cement. Ten silicoated G-Cera specimen and ten non-silicoated G-Cera specimen were bonded to teeth with G-Cera resin cement. Bonded units were mounted in a plastic tube with hard stone and stored in a humidor at $37^{\circ}C$ for 24 hours. Shear bond strength was measured by Instron Universal Testing Machine (Model 1125) and all the specimen were observed with SEM(JEOL, JSM-T2000)and modes of failure were recorded. The obtained results were as follows: 1. The mean shear bond strength of Dicer bonded with Dicer resin cement was 11.62 MPa and that bonded with Dicor ZPC cement was 0.88 MPa : Shear bond strength of Dicer bonded with Dicer resin cement was significantly increased(P<0.05). 2. The mean shear bond strength of silicoated G-Cera was 13.10 MPa and that of non silicoated G-Cera was 10.93 MPa : Shear bond strength of silicoated G-Cera was not significantly increased (P>0.05). 3. Shear bond strength of Dicer and G-Cera porcelain laminate veneer was not significantly different (P>0.05). 4. In observation of bond failure with SEM, Dicer bonded with Dicer ZPC cement exhibited adhesive failure. Dicer bonded with Dicer resin cement and silicoated and non silicoated G-Cera exhibited cohesive failure.

• The Journal of Korean Academy of Prosthodontics
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• v.31 no.2
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• pp.165-179
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• 1993

Dicor has not been prescribed routinely, in spite of many advantages, because of esthetic limitations by excessive translucency and external shading. In an attempt to solve these problems, the technique of veneering Dicor by aluminous poreclain has been used and recently Dicor Plus system was developed. The purpose of this study was to evaluate the compatibility between Dicor and several veneering porcelains by measuring the shear bond strength and observing the failure mode and interface appearance with SEM. Total 55 Dicor disks(10.0mm diam. X 3.0mm thickness) were fabricated by lost wax technique and divided into five groups of 11. Veneering porcelains such as Dicor Plus, Vitadur Alpha, Vitadur N, Vivodent, and Ceramco II were built up over the center of the treated Dicor surface using paper tube(5.0mm diam. X 4.0mm height) and fired according to the manufacturesr’instructions. A representative sample from each group was completely embedded in epoxy resin and crosssectioned, and remaining 50 samples were embedded in epoxy resin with the bonded area perpendicular to table base. The shear bond strengths were measured by applying the shear load parallel to Dicor surface close to the bonded area. Failure modes and interface appearances were observed using SEM at 15 and 1000 magnification respectively. The obtained results were as follows : 1. The mean shear bond strengths showed Dicor-Dicor Plus(10.53 MPa); Dicor-Vitadur Alpha(8.84 MPa); Dicor-Vitadur N(7.37 MPa); Dicor-Vivodent(4.28 MPa); Dicor-Ceramco II(0.89 MPa). 2. The shear bond strength of Dicor-CeramcoII was significantly decreased compared with Dicor-Dicor Plus(p<0.01), but had no significant difference compared with Dicor-Vivodent(p>0.01). 3. The shear bond strengths of Dicor-Vitadur Alpha and Dicor-Vitadur N were not significantly different compared with Dicor-Dicor Plus(p>0.01). 4. SEM examination of bond failure modes revealed that Dicor-Dicor plus, Dicor-Vitadur Alpha, Dicor-Vitadur N exhibited cohesive failure within Dicor and Dicor-Vivodent exhibited adhesive failure. And Dicor-Ceramco III exhibited adhesive failure and cohesive failure within CeramcoIII together. 5. SEM examination of interfaces revealed that Dicor-Dicor Plus exhibited the most tight contact and Dicor-Vitadur Alpha, Dicor-Vitadur N exhibited acceptible contacts. But Vivodent exhibited discontinuous gap and Ceramco II exhibited large continuous gap.

• Journal of the Korea Concrete Institute
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• v.22 no.4
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• pp.527-534
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• 2010

This study presents a simple method to improve the bond performance of reinforced concrete (RC) beams having high-strength shear reinforcement. In general, the yield strength and the ratio of shear reinforcements are the main parameters governing the shear capacity of RC beams. The yield strength of shear reinforcement, however, has little influence on the bond capacity of RC beams. Therefore, a sudden bond failure of the members with high-strength shear reinforcement can occur before flexural failure. To estimate the structural performance of the proposed method, four RC beams were cast and tested. The main test parameters were the yield strength, ratio, and reinforcing types of shear reinforcements. The experimental results indicated that the proposed method was able to effectively improve the bond performance of RC beams with high-strength shear reinforcement.