• Title/Summary/Keyword: separations

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Separation Phenomenon Occurring during Charpy Impact test of API X80 Linepipe Steels (API X80 라인파이프강의 샤르피 충격 시험 시 발생하는 파열 현상 연구)

  • Shin, Sang Yong;Hong, Suckmin;Bae, Jin-ho;Kim, Kisoo;Lee, Sunghak
    • Korean Journal of Metals and Materials
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    • v.47 no.3
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    • pp.155-168
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    • 2009
  • In this study, microstructural investigation was conducted on the separation phenomenon occurring during Charpy impact tests of API X80 linepipe steels. Particular emphasis was placed on the role of microstructural phases present in the API X80 steels such as acicular ferrite, bainite, and hard secondary phases. Detailed microstructural analysis of fractured impact specimens showed that highly elongated bainite worked as prior initiation sites for separations, and that the number and length of separations increased with increasing volume fraction of bainite. In the steels having high work hardenability, tearing-shaped separations were found because the hammer-impacted region was seriously hardened during the impact test, which led to the reduction in the impact toughness. As the test temperature decreased, the tendency of separations increased, but separations were not observed when the cleavage fracture prevailed at very low temperatures. Thus, the minimization of the formation of bainite and secondary phases in the steels would be beneficial for preventing or minimizing separations because separations deteriorated low-temperature impact toughness.

"Getting Used to Each Other": Immigrant Youth's Family Reunification Experiences

  • Suarez-Orozco, Carola;Kim, Ha-Yeon;Bang, Hee-Jin
    • Child Studies in Asia-Pacific Contexts
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    • v.1 no.1
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    • pp.1-23
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    • 2011
  • Many immigrant youth and their families undergo painful separations and complicated reunification experiences. Using data from the Longitudinal Immigrant Student Adaptation (LISA) study, a 5-year longitudinal, mixed-methods study of newcomer youth to the U.S., we examine the impact of lengthy family separations on youth's mental health and their perceived family conflict. Quantitative analyses demonstrate that longer separations positively predict higher psychological symptoms and family conflict, particularly for girls over a sustained period of time. Qualitative analyses of parent and child responses provide insights into the family reunification experiences.

Affinity Separations Using Microfabricated Microfluidic Devices: In Situ Photopolymerization and Use in Protein Separations

  • Chen Li;Lee, Wen-Chien;Lee, Kelvin H.
    • Biotechnology and Bioprocess Engineering:BBE
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    • v.8 no.4
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    • pp.240-245
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    • 2003
  • The use of microfabricated microfluidic devices offers significant advantages over current technologies including fast analysis time and small reagent requirements. In the context of proteomic research, the possibility of using affinity-based separations for prefractionation of samples using microfluidic devices has significant potential. We demonstrate the use of microscale devices to achieve affinity separations of proteins using a device fabricated from borosilicate glass wafers. Photolithography and wet etching are used to pattern individual glass wafers and the wafers are fusion bonded at 650$^{\circ}C$ to obtain enclosed channels. A polymer has been successfully polymerized in situ and used either as a frit for packing beads or, when derivatized with Cibacron Blue 3GA, as a separation matrix. Both of these technologies are based on in situ UV photopolymerization of glycidyl methacrylate (GMA) and trimethylolpropane trimethacrylate (TRIM) in channels.

Effects of Specimen Thickness and Notch Shape on Fracture Mode Appearing in Drop Weight Tear Test (DWTT) Specimens of API X70 and X80 Linepipe Steels (API X70 및 X80 라인파이프강의 DWTT 시편 파괴 형태에 미치는 시편 두께와 노치 형태의 영향)

  • Hong, Seokmin;Shin, Sang Yong;Lee, Sunghak;Kim, Nack J.
    • Korean Journal of Metals and Materials
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    • v.48 no.8
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    • pp.705-716
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    • 2010
  • Effects of specimen thickness and notch shape on fracture mode appearing in drop weight tear test (DWTT) specimens of API X70 and X80 linepipe steels were investigated. Detailed microstructural analysis of fractured DWTT specimens showed that the fractures were initiated in normal cleavage mode near the specimen notch, and that some separations were observed at the center of the fracture surfaces. The Chevron-notch (CN) DWTT specimens had broader normal cleavage surfaces than the pressed-notch (PN) DWTT specimens. Larger inverse fracture surfaces appeared in the PN DWTT specimens because of the higher fracture initiation energy at the notch and the higher strain hardening in the hammer-impacted region. The number and length of separations were larger in the CN DWTT specimens than in the PN DWTT specimens, and increased with increasing specimen thickness due to the plane strain condition effect. As the test temperature decreased, the tendency to separations increased, but separations were not found when the cleavage fracture prevailed at very low temperatures. The DWTT test results, such as upper shelf energy and energy transition temperature, were discussed in relation with microstructures and fracture modes including cleavage fracture, shear fracture, inverse fracture, and separations.

Membrane Separations and Energy Savings

  • Hwang, Sun-Tak
    • Proceedings of the Membrane Society of Korea Conference
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    • 1994.06a
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    • pp.33-43
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    • 1994
  • It is the purpose of this paper to review the recent developments and future trends in various membrane processes, which will result in energy savings. Historically, there was a long period of academic curiosity in membrane research covering from gas separation to reverse osmosis. With advent of asymmetric membrane technology, many membrane processes proved to be energy efficient than the conventional separation methods. Thus, membrane technology has gained wide acceptance from many sectors of industry. The commercial sale of membranes is still modest compared to the major technologies, but it is one of the fastest growing industries. Recently the U.S.Department of Energy conducted a study (1) to evaluate and prioritize research needs in the membrane separation industry in order to foster and better support the deveolpment of energy-efficient new technologies. The National Science Foundation (U.S.A.) did also do a similar investigation. Both agencies have arrived neary at the same conclusion, that is, membrane separations can offer many new and alternative methods of separations that are more energy efficient than existing processes. This paper is largely based on these findings.

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Trends in Polymer Separations: Better and More Information on Polymer Distributions

  • Schoenmakers, Peter
    • Proceedings of the Polymer Society of Korea Conference
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    • 2006.10a
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    • pp.113-113
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    • 2006
  • Polymer separations are used to obtain information on molecular distributions (molecular-weight distribution, chemical-composition distribution, functionality-type distribution, etc.). The existing methods, such as size-exclusion chromatography are reliable, but imperfect. New methods and improvements to existing methods are being studied and some of the results will be discussed. In addition, comprehensive two-dimensional liquid chromatography allows the complete characterization of two mutually dependent distributions. LCxSEC chromatograms provide a very good qualitative impression of the distributions, but calibration is not straightforward. Finally, progress in mass spectrometry allows much better information to be obtained.

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Robust Polymeric Membranes for the Separation of Petrochemicals using Pervaporation

  • Nam, Sang-Yong
    • Proceedings of the Membrane Society of Korea Conference
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    • 2004.05a
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    • pp.51-54
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    • 2004
  • Utilization of membranes offers the promise of extraordinary energy savings if successfully applied to hydrocarbon-hydrocarbon and other organic separations. Membranes are bound to enter into refining and petrochemical operations involving liquid separations once appropriate materials and modules are developed. Hybrid processes such as utilizing membrane modules to break azeotropes formed during distillation are particularly attractive because they offer less process complexity and reduced capital investment[1,2].(omitted)

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All-arthroscopic, Guideless Single Suture-button Fixation of Acute Acromioclavicular Joint Dislocation: A Description of the Technique and Early Treatment Results

  • Altintas, Burak;Yildiz, Fatih;Uzer, Gokcer;Kapicioglu, Mehmet;Bilsel, Kerem
    • Clinics in Shoulder and Elbow
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    • v.20 no.2
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    • pp.59-67
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    • 2017
  • Background: The purpose of this study was to examine the clinical and radiological results of the all-arthroscopic, suture-button fixation technique to treat acute acromioclavicular (AC) joint separations. Methods: All patients with acute AC joint separations received all-arthroscopic, single suture-button (TightRope) procedure without a special guide. Postoperative Constant score (CS), pain level according to visual analogue scale, and range of motion (ROM) were evaluated. For radiological evaluation, coracoclavicular distances were measured bilaterally. Results: Between December 2010 and June 2012, 18 consecutive patients (4 women and 14 men; mean age, 29.3 years) with acute AC joint separations underwent surgical treatment after 6.4 days (range, 2-20 days) following the initial trauma. The average postoperative follow-up was 16.9 months. The mean CS was 92.4 (range, 84-96). The mean external rotation, forward flexion, and abduction were $75.8^{\circ}$ (range, $50^{\circ}-90^{\circ}$), $170^{\circ}$ (range, $150^{\circ}-180^{\circ}$), and $163.8^{\circ}$ (range, $140^{\circ}-180^{\circ}$), respectively. Five patients exhibited coracoclavicular ossifications. In two patients, superficial wound infections were successfully treated with antibiotic therapy. In one patient, a coracoid fracture was observed. No significant differences were found regarding pain, ROM, or strength parameters between both sides. The coracoclavicular distance was discovered to be approximately 2.8 mm greater on the affected side; however, this minimal reduction loss did not affect the functional results. Conclusions: The findings of this study suggests that all-arthroscopic treatment of AC joint separations using the single suture-button technique without a drill guide is safe, yielding good to excellent clinical results.

SPECKLE OBSERVATION OF VISUAL DOUBLE STARS AT BOSSCHA OBSERVATORY: SEPARATION AND MAGNITUDE DIFFERENCE LIMITS

  • HADIPUTRAWAN, I PUTU WIRA;PUTRA, MAHASENA;IRFAN, MOCHAMAD;YUSUF, MUHAMMAD
    • Publications of The Korean Astronomical Society
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    • v.30 no.2
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    • pp.223-224
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    • 2015
  • We present the results of visual double stars speckle observations from 2013 using a Zeiss Double Refractor 60 cm with visual focal length f = 1,078 cm, and CCD SBIG ST-402 MEA. A Bessel V filter with ${\lambda}=550nm$ was placed in front of the CCD camera to reduce the chromatic aberration of the objective lens. The objects selected for this observation were calibration candidates and program stars with separations ranging from 0.9-6 arc second, and were located in both the northern and southern hemispheres. Seeing at Bosscha Observatory is generally 1-2 arc second, imposing a limit on visual double star separation below which the system cannot be resolved by long exposure imaging (longer than ~50 ms). Speckle interferometry methods are used to resolve double stars with separations below the typical size of seeing effects. A series of images were captured in fast short-time exposures (~50 ms) using a CCD camera. The result of our experiment shows that our system can be used to measure separations of 0.9 arc second (for systems with small ${\Delta}m$) and ${\Delta}m{\approx}3.7$ (for wide systems).

Avantor® ACE® UltraCore HPLC and UHPLC Columns (Avantor® ACE® UltraCore HPLC/UHPLC 칼럼 가이드)

  • Peter Bridge;Ian Phillips;Gemma Lo;Cassandra Rusher
    • FOCUS: LIFE SCIENCE
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    • no.1
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    • pp.4.1-4.15
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    • 2024
  • The Avantor® ACE® UltraCore series encompasses High Performance Liquid Chromatography (HPLC) and Ultra High Performance Liquid Chromatography (UHPLC) columns designed to deliver high throughput and high-efficiency ultra-fast separations. Utilizing ultra-inert solid-core silica particles with monodisperse particle distribution, these columns combine the high efficiency of UHPLC with the operability of HPLC instrumentation, yielding lower backpressure and high-resolution separations suitable for a broad spectrum of analytes. The Avantor® ACE® UltraCore range includes three primary product types: • UltraCore BIO: Designed for large biomolecules (≥5 kDa), these columns offer exceptional performance in separating biologically derived compounds. • UltraCore: Ideal for standard small organic molecules, providing rapid separations for both synthetic and natural mixtures. • UltraCore Super: Equipped with encapsulated bonding technology for small organic molecules in extreme pH conditions, optimal for high pH buffer requirements. The Avantor® ACE® UltraCore columns present a versatile and high-efficiency solution for chromatographic separation needs, accommodating a wide range of molecular sizes and providing enhanced resolution and reduced analysis time. Their adaptability to both HPLC and UHPLC systems, combined with the advantages of solid-core technology, makes them an invaluable tool in analytical and preparative chromatography.

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