• Title/Summary/Keyword: separate solution method

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Analysis of Transient Electromagnetic Scattering from 3-Dimensional Dielectric Objects by using Time-Domain PMCHW Integral Equation (시간영역 PMCHW 적분식을 이용한 3차원 유전체의 전자파 과도 산란 해석)

  • 정백호;서정훈;한상호
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.14 no.10
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    • pp.1096-1103
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    • 2003
  • In this paper, we analyze the transient electromagnetic response from three-dimensional(3-D) dielectric bodies using a time-domain PMCHW(Poggio, Miller, Chang, Harrington, Wu) formulation. The solution method in this paper is based on the Galerkin's method that involves separate spatial and temporal testing procedures. Triangular patch basis functions are used for spatial expansion and testing functions for arbitrarily shaped 3-D dielectric structures. The time-domain unknown coefficients of the equivalent currents are approximated by a set of orthonormal basis functions that are derived from the Laguerre polynomials. These basis functions are also used as the temporal testing. Numerical results involving equivalent currents and far fields computed by the proposed method are presented.

Flame Atomic Absorption Spectrometric Determination of Ultra Traces of Thallium(I) ion after Solid Phase Extraction by Octadecyl Silica Membrane Disk Modified by a New Schiff Base

  • Mashhadizadeh, Mohammad Hossein;Moatafavi, Ali;Allah-Abadi, Hossein;Zadmehr, Mohammad Reza
    • Bulletin of the Korean Chemical Society
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    • v.25 no.9
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    • pp.1309-1313
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    • 2004
  • A simple and reliable method has been developed to selectively separate and concentrate trace amounts of thallium ion from real samples for the subsequent measurement by flame atomic absorption spectrometry (FAAS). Thallium ions are absorbed quantitatively during passage of aqueous real samples through an octadecyl bonded silica membrane disk modified by 4-(4-Chloro-phenylazo)-2-[(4-hydroxy-phenylamino)-methyl]-phenol. The retained $Tl^+$ ions are then stripped from the disk quantitatively with a minimal amount of thiosulfate solution as eluent. The proposed method permitted large enrichment factors of about 130 and higher. The relative standard deviation for ten replicate extraction of thallium from 1 L samples containing 5 ${\mu}g$ thallium is 1.2%. The break through volume for 5 ${\mu}g$ thallium is 1000 mL. The limit of detection of the proposed method is 11.2 ng of $Tl^+$ per 1000 mL. The effects of various cationic interferences on the recovery of thallium in binary mixtures were studied. The method was applied to the recovery of $Tl^+$ ions from natural water and human hair samples.

Separation of Phosvitin from Egg Yolk without Using Organic Solvents

  • Jung, Samooel;Ahn, Dong Uk;Nam, Ki Chang;Kim, Hyun Joo;Jo, Cheorun
    • Asian-Australasian Journal of Animal Sciences
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    • v.26 no.11
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    • pp.1622-1629
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    • 2013
  • The objective of this study was to develop a new method to separate phosvitin from egg yolk without using organic solvents. Phosvitin was extracted from yolk granules using 10% NaCl or 10% $(NH_4)_2SO_4$ (final concentration) and then treated with heat to precipitate the lipoproteins from the extracted solution. The optimal pH for the phosvitin extraction from yolk granules was determined, and the iron-binding ability of the extracted phosvitin (final product) was tested. Adding 10% $(NH_4)_2SO_4$ disrupted the granules, and the subsequent thermal treatment at $90^{\circ}C$ for 1 h precipitated low density and high density lipoproteins, which enabled separation of phosvitin by centrifugation. The phosvitin concentration in the extract was significantly higher when the pH of the solution was adjusted to pH ${\geq}9$. The purity and recovery rate of phosvitin at the end of the separation process were approximately 78% and 56%, respectively. The separated phosvitin was confirmed to have ferrous and ferric iron binding ability. The advantages of this new method compared with the traditional methods include no organic solvents and high-priced equipment are needed for the separation. Also, this method is more environment and consumer friendly than that of the traditional methods.

Synthesis of Yttria Stabilized Zirconia by Sol-gel Precipitation Using PEG and PVA as Stabilizing Agent

  • Bramhe, Sachin N.;Lee, Young Pil;Nguyen, Tuan Dung;Kim, Taik-Nam
    • Korean Journal of Materials Research
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    • v.23 no.8
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    • pp.441-446
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    • 2013
  • There is increasing interest in zirconia as a dental material due to its aesthetics, as well as the exceptionally high fracture toughness and high strength that are on offer when it is alloyed with certain oxides like yttria. In recent years, many solution based chemical synthesis methods have been reported for synthesis of zirconia, of which the sol-gel method is considered to be best. Here, we synthesize zirconia by a sol gel assisted precipitation method using either PEG or PVA as a stabilizing agent. Zirconia sol is first synthesized using the hydrothermal method. We used NaOH as the precipitating agent in this method because it is easy to remove from the final solution. Zirconium and yttrium salts are used as precursors and PEG or PVA are used as stabilizers to separate the metal ions. The resulting amorphous zirconia powder is calcined at $900^{\circ}C$ for 2 h to get crystallized zirconia. XRD analysis confirmed the partially stabilized zirconia synthesis in all the synthesized powders. SEM was taken to check the morphology of the powder synthesized using either PEG or PVA as a stabilizing agent and finally the transparency was calculated. The results confirmed that the powder synthesized with 10 % PVA as the stabilizing agent had highest percentage of transparency among all the synthesized powder.

Nonlinear Deblurring Algorithm on Convex-Mirror Image for Reducing Occlusion (볼록거울 영상에서 일어나는 영상 겹침 극복을 위한 비선형적 디블러링 알고리즘)

  • Lee, In-Jung
    • The KIPS Transactions:PartA
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    • v.13A no.5 s.102
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    • pp.429-434
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    • 2006
  • A CCTV system reduces some number of cameras if we use convex-mirror. In this case, convex-mirror Image distorted, we need transformation to flat images. In the center of mirror images, a transformed image has no distortion, but at near boundary image has plentiful distortion. This distortion is caused by occlusion of angled ray and diffraction. We know that the linear filtering approach cannot separate noise from signal where their Fourier spectra overlap. But using a non-linear discretization method, we shall reduce blurred noise. In this paper, we introduce the backward solution of nonlinear wave equation for reducing blurred noise and biased expansion of equilibrium contour. We propose, after applying the introduced method, and calculate with discretization method. To analysis the experimental result, we investigate to PSNR and get about 4dB better than current method.

An Implementation of Integrated System for Topographic and Cadastral Data (지형 및 지적자료의 통합체계 구축)

  • 유복모;김갑진
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.18 no.2
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    • pp.143-155
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    • 2000
  • With the increasing needs for the integrated use of topographic and cadastral data in order to build an efficient geo-spatial information system. it is urgently necessary to research into its solution. The intention of this study is to detect error types of data and to propose adjustment methods for solving the problems caused by integrating topographic and cadastral data. For this purpose a primary integrated data model is created to link attribute data(land management system) and graphic data within cadastral information in the first step. In next, a secondary integrated data model based on the improved method is formed to coincide the graphic data of cadastral map with that of topographic map. At the first, because a numerous error types md sources caused by separate management of graphic and attribute data are easily checked, it is possible to suggest an improved method to correct these errors using the primary integrated data model. In addition, the accuracy in position and area with coordinate transformation method based on multi-block adjustment is more efficient than rubber-sheeting method. As a result, the secondary integrated data model could be built by harmonizing cadastral map with topographic map using the improved solution.

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Separation of Single-Walled Carbon Nanotubes by Length and Diameter (단일벽 탄소 나노튜브의 길이와 지름에 따른 분류)

  • Oh Young-Seok;Lee Dock-Jin;Chang Yyun-Seok;Choi Jae-Boong;Kim Young-Jin;Baik Seung-Hyun
    • Journal of the Korean Society for Precision Engineering
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    • v.23 no.3 s.180
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    • pp.171-178
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    • 2006
  • The sonication mettled is widely used with surfactants to suspend individual single-walled carbon nanotubes in solution, and it is well known that sonication-induced tube cutting occurs. Recently, it is found out that ultrasonicated nanotubes yield simultaneous separation by tube length and diameter. Nanotubes that have been cut shortest possess the greatest enrichments of large-diameter species. In this study, single-walled carbon nanotubes are cut using a ball milling method. Similar fracture behavior is observed fur the ball milled nanotubes: i.e., large diameter tubes are cut shorter. The ability to separate carbon nanotubes by diameter and length will contribute to tile development of nanotube-based applications.

Recycling Process of WC Fine Powder Contained by Cemented Carbides Parts in JAPAN

  • Mitsuru Nakamura;Kim, Ha-Young;Hwang, Sun-Hyo
    • Proceedings of the KWS Conference
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    • 1999.10a
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    • pp.297-298
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    • 1999
  • Cemented carbides material (WC-Co hard alloy) were recognized very important and expensive tool or die assembly parts because of compose for the main elements of rare metal (W and Co etc). This research was developed to separate and recover of WC fine powder contained by WC-Co materials. Recycling process was a new method named by the Tin impregnation for decobaltification on cemented carbides. This reaction occurred to product a brittle Co-Sn intermetallic compounds, thereafter it carried out by acid cleaning solution and physical milling or powdering. New process was able to recover about 60% WC fine powder from 1 to 5 ${\mu}{\textrm}{m}$.

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Bifurcation Analysis of a Non-linear Hysteretic Oscillating System (비선형 히스테리시스 진동시스템의 분기해석)

  • 송덕근;최진권;장서일
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2001.05a
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    • pp.289-294
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    • 2001
  • Three kinds of viscoelastic damper model, which has a non-linear spring as an element is studied analytically and numerically. The behavior of the damper model shows non-linear hysteresis curves which is qualitatively similar to those of real viscoelastic materials. The motion is governed by a non-linear constitutive equation and an additional equation of motion. Harmonic balance method is applied to get analytic solutions of the system. The frequency-response curves show that multiple solutions co-exist and that the jump phenomena can occur. In addition, it is shown that separate solution branch exists and that it can merge with the primary response curve. Saddle-node bifurcation sets explain the occurrences of such non-linear phenomena.

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Bifurcation Analysis of a Non-linear Hysteretic Oscillating System (비선형 히스테리시스 진동시스템의 분기해석)

  • 장서일;송덕근;최진권
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.12 no.1
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    • pp.57-64
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    • 2002
  • Three kinds of viscoelastic damper model, which has a non-linear spring as an element is studied analytically and numerically The behavior of the damper model shows non-linear hysteresis curves which is qualitatively similar to those of real viscoelastic materials. The motion is governed by a non-linear constitutive equation and an additional equation of motion. Harmonic balance method is applied to get analytical solutions of the system. The frequency-response curves sallow that multiple solutions co-exist and that the jump phenomena can occur. In addition, it is shown that separate solution branch exists and that it can merge with the primary response curve. Saddle-node bifurcation sets explain the occurrences of such non-linear Phenomena.