• Title/Summary/Keyword: secondary crack

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Ni Electroplating in the Emulsions of Supercritical $CO_2$ Formed by Ultrasonar (초음파를 이용한 초임계 이산화탄소 에멀젼내 Ni 전해도금)

  • Koh M. S.;Joo M. S.;Park K. H.;Kim H. D.;Kim H. W.;Han S. H.;Sato Nobuaki
    • Journal of the Korean institute of surface engineering
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    • v.37 no.6
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    • pp.344-349
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    • 2004
  • Emulsions were formed through putting small quantity of nickel electroplating solution into supercritical carbon dioxide, and then electroplating in the $sc-CO_2$ emulsions was conducted. It is an environmental-friendly technology that can solve the treatment of a large quantity of toxic plating wastewater, which is a big problem in the existing wet plating, and also can reduce secondary waste generation fundamentally. Supercritical carbon dioxide emulsions enhanced by ultrasonic horn were formed by non-ionic surfactant and nickel solution. Plating condition within emulsions was set up as 120bar and $55^{\circ}C$ through measurement of electrical conductivity following the pressure change. Experiments were conducted respectively against supercritical carbon dioxide emulsions electroplating and general chemical electroplating, and then their results were compared and analyzed. As the experiment result utilizing emulsions, plating surface was formed very evenly even with a small quantity of electroplating solution, and fine particles were plated compactly without any pinhole or crack due to hydrogenation, which occurs in general electroplating. Used electroplating solution can be reused through recovery process. Therefore, this technology will be able to be applied as new clean technology in electro-plating.

Microstructure and Toughness of Weld Heat-Affected Zone in Cu-containing HSLA-100 steel (Cu를 함유한 HSLA-100강 용접 열영향부의 미세 조직 및 인성)

  • Park, T.W.;Shim, I.O.;Kim, Y.W.;Kang, C.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.8 no.1
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    • pp.53-64
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    • 1995
  • A study was made to characterize the microstructures and mechanical properties of the base metal and the heat-affected zone(HAZ) in Cu-bearing HSLA-100 steel. The Gleeble thermal/mechanical simulator was used to simulated the weld HAZ. The relationship between microstructure and toughness of HAZ was studied by impact test, O. M, SEM, TEM, and DSC. The toughness requirement of military specification value was met in all test temperatures for the base metal. The decrease of HAZ toughness comparing to base plate is ascribed to the coarsed-grain and the formation of bainite. Obliquely sectioned Charpy specimens show that secondary crack propagate easily along bainite lath. Improved toughness(240J) at HAZ of $Tp_2=950^{\circ}C$ is due to the fine grain, and reasonable toughness(160~00J) in the intercritical reheated HZA is achieved by the addition of small amount of carbon which affects the formation of "M-A". Cu precipitated during ageing for increasing the strength of base metal is dissolved during single thermal cycle to $1,350^{\circ}C$ and is precipitated little on cooling and heating during subsequent weld thermal cycle. Thus, the decrease of toughness does not occur owing to the precipitation of Cu.

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The Effect of Die Cooling on the Surface Defects of the Aluminum 7075 Extrudates (알루미늄 7075 합금의 압출에서 금형 냉각이 압출재의 표면 결함에 미치는 영향)

  • S.Y., Lee
    • Journal of the Korean Society for Heat Treatment
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    • v.35 no.6
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    • pp.319-326
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    • 2022
  • Direct extrusions of an aluminum 7075 alloy were carried out using 1500 ton machine with and without die cooling system. Cooling of extrusion die has been performed by the flow of liquid nitrogen and controlled by laser thermometer. Billet was 180 mm in diameter and 500 mm in length. The preheating temperatures of billet, container and die were 390℃, 400℃ and 450℃, respectively. Ram speed was kept with 1.25 mm/sec first. The change of ram speed was carried out during extrusion according to the observation of surface defects such as crack or tearing. Extrudates of 8.3 m in length, 100 mm in width and 15 mm in thickness were obtained to observe and analyze surface defects by optical microscopy and EBSD (Electron BackScattered Diffraction). In case of extrusion without die cooling cracks on the surface and tearing in the corner of extrudate occurred in the middle stage and developed in size and frequency during the late stage of extrusion. At the extrusion with die cooling the occurrence of defects could be suppressed on the most part of extrudate. EBSD micrographs showed that cracks and tearings have been resulted from the same origin. Surface defects were generated at the boundaries of grains formed by secondary recrystallization due to surface overheating during extrusion.

Fabrication of YBCO films in MOD processing using F-free Y & Cu precursor solution (F-free Y & Cu 전구용액을 이용한 YBCO 박막 제조)

  • Kim, Young-Kuk;Yoo, Jai-Moo;Ko, Jae-Woong;Chung, Kook-Chae;Kim, Young-Jun;Han, Bong-Soo;Wang, X.L.;Dou, S.X.
    • Progress in Superconductivity and Cryogenics
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    • v.8 no.1
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    • pp.15-18
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    • 2006
  • A new precursor solution wilt low fluorine content was synthesized for MOD processing of coated conductors. In this study, the precursor solution for MOD processing was synthesized using F-free yttrium and copper precursor. It was shown that crack-free and uniform precursor films were formed after calcination in humidified oxygen atmosphere. Less than 2 hours were required to finish the calcination process. The relatively gradual weight loss during the calcination process is attributed to the feasibility of fast calcination profile. The calcined precursor film was converted to a YBCO film without any secondary phases after annealing in wet $Ar/O_2$ atmosphere. Fully converted film shows uniform microstructure and high critical current density. $(Jc=2.7MA/cm^2) $.

Applicability of SRSL(Self-Recovering Sustainable Liner) to the Landfill Final Cover System (SRSL(Self Recovering Sustainable Liner)재의 매립지 최종복토층에 대한 활용성 검토)

  • Kwon, Oh-Jung;Seo, Min-Woo;Hong, Soo-Jung;Park, Jun-Boum;Park, Soo-Young
    • Proceedings of the Korean Geotechical Society Conference
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    • 2004.03b
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    • pp.453-460
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    • 2004
  • To prevent penetration of rainwater into the landfill site is the main purpose of the final cover in landfill sites. Conventional designs of landfill covers uses geotextiles such as geomembrane and GCL, and clay liners to lower the permeability of final covers of landfill sites. However, differential settlement and the variation of temperature in landfill sites cause the development of cracks or structural damage inside the final cover and it is also difficult to obtain clay - the main material of the compacted clay liner in Korea. Thus the former final cover system that suggests geomembrane and GCL or compacted clay liner has several limitations. Therefore, an alternative method is necessary and one of them is the application of SRSL(self-Recovering Sustainable Liner) material. SRSL is two different layers consist of individual materials that react with each other and form precipitates, and with this process lowers the permeability of the landfill final cover. SRSL generally is made up of two layers, so that when a internal crack occurs the reactants of the two layers migrate towards the crack and heal it by forming another liner. In this study the applicability of SRSL material for landfill final cover was examined by performing; (1) jar test to verify the formation of precipitate in the mixture of each reactants, (2) falling head test considering the field stress in order to confirm the decrease of permeability or prove that the hydraulic condctivity is lower than the regulations, (3) compression tests to judge weather if the strength satisfies the restricts for landfills, (4) freeze/thaw test to check the applicability of SRSL for domestic climate. In addition, the application of waste materials in the environmental and economical aspect was inspected, and finally the possibility of secondary contamination due to the waste materials was examined by performing elution tests.

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Numerical Analysis Study for Optimal Design Method on Intersection between Longitudinal and Transversal Rib in Orthotropic Steel Deck Bridge (강바닥판교의 종리브-횡리브 교차연결 상세변화에 따른 최적설계방안의 수치해석 연구)

  • 배두병;공병승
    • Journal of the Computational Structural Engineering Institute of Korea
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    • v.17 no.3
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    • pp.333-340
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    • 2004
  • The use of the othotropic steel deck is steadily increased due to the advance of the technology in the steel bridges which recently have been longer. But the othotropic steel deck bridge is the structure that is very fragile to the fatigue, especially, the fatigue crack at the cross of the longitudinal rib and transversal rib is one of the biggest problems that othotropic steel deck bridges have. The causes of these fatigue cracks come from the secondary stress on out-plane behavior of transversal rib. In this study, we conducted the experiment to find the optimal details to improve fatigue strength on intersection between longitudinal rib and transversal rib in the othotropic steel deck bridge through numerical analysis using the experiment of the fatigue in the 3-dimensional real structure and program LUSAS. As a result of study, it is showed that the details of the korean standard section attached with a curved bulkhead plate is the most profitable. And, it is indicated that the stress which is generated when the reform improved section by parametic study can be reduced by about 50% at most or more. Along with the reduced stress and the longer interval between transversal ribs(G=400), the decreased steel amount by 4% and the shortened welding length by 34% make it possible to produce the othotropic steel deck bridge which is strong against fatigue.

Secondary Growth of Sodium Type Faujasite Zeolite Layers on a Porous $\alpha-Al_2O_3$ Tube and the $CO_2/N_2$ Separation (Na형 Faujasite 제올라이트 분리막 형성 및 $CO_2/N_2$ 분리)

  • Cho, Churl-Hee;Yeo, Jeong-Gu;Ahn, Young-Soo;Han, Moon-Hee;Kim, Yong-Ha;Hyun, Sang-Hoon
    • Membrane Journal
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    • v.17 no.3
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    • pp.254-268
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    • 2007
  • Sodium type faujasite(FAU) zeolite layers with diverse materials characteristics(Si/Al ratio, thickness, and structural discontinuity) were hydrothermally grown on a porous $\alpha-Al_2O_3$ tube, and then the $CO_2/N_2$ separation was evaluated at $30^{\circ}C$ for an equimolar mixture of $CO_2$ and $N_2$. Among hydrothermal conditions, $SiO_2$ content in hydrothermal solution seriously affected materials characteristics: with an increment in the $SiO_2$ content, Si/Al ratio, thickness, and structural discontinuity of grown FAU zeolite layer simultaneously increased. The present study reveals that structural discontinuity(intercrystalline voids due to an incomplete densification and cracks induced by GIS Na-P1 phase) is the most important variable affecting the $CO_2/N_2$ separation. Also, it was suggested that the $CO_2$ desorption in permeate side be the rate-determining(slowest) step in the overall $CO_2$ permeation.

Corrosion effects on mechanical behavior of steel fiber reinforced concrete, including fibers from recycled tires

  • Ansari, Mokhtar;Safiey, Amir
    • Computers and Concrete
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    • v.26 no.4
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    • pp.367-375
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    • 2020
  • Today, the use of special technologies in the admixture of concrete has made tremendous progress, but the problem that has always existed in the construction of concrete members is the brittleness and lack of loading bearing after cracking, which leads to reduced strength and energy absorption. One of the best ways to fix this is to reinforce the concrete with steel fibers. Steel fibers also control cracks due to dry shrinkage, reduce structural crack width, and improve impact resistance. In this study, recycled steel fibers from worn tires have been used in the manufacture of concrete samples, the secondary benefits of which are the reduction of environmental pollution. One of the disadvantages of steel fiber reinforced concrete is the corrosion of steel fibers and their deterioration in harsh environments such as coastal areas. Corrosion caused by chlorine ions in metal fibers causes deterioration and early decommissioning of structures in corrosive environments. In this study, the effect of the dosage of steel fibers (dosages of 15, 30, and 45 kg of fibers per cubic meter of concrete) and aspect ratio of fibers (aspect ratio of 25 and 50) on compressive and flexural strength of concrete samples are investigated. In the following, the effect of fiber corrosion on the results of the mechanical properties of concrete samples is examined. The results show that the increase in fiber causes a relative increase in compressive strength, and a significant increase in flexural strength, and corrosion of steel fibers without reducing workability reduces compressive strength and flexural strength by up to 6 to 11%, respectively.

Research Strategy on Columnar Joint in South Korea (우리나라 주상절리에 대한 연구 전략)

  • Ahn, Kun Sang
    • Journal of the Korean earth science society
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    • v.35 no.7
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    • pp.501-517
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    • 2014
  • Based on a summary of the previous studies on columnar joints, this study presents research strategies and subjects to understand a formation of columnar joints, and its application in South Korea as follows; geometry of colonnade and entablature, formation mechanism and pattern change, surface morphology and internal structure, platy joint at the top and the bottom of columnar joints, crack patterns in drying starch-water slurries, using numerical models and computer graphics on joint formation, scale and geometry concerned with occurrence of volcanic rock, petrological and mineralogical study of the host rock. Additionally, more research is needed, such as deformation of column pattern during the hot state, secondary landform by alteration and weathering on the Earth's surface such as rock stream, tor and tafoni. This study will take an active role in research of columnar joint and the Cenozoic lava flow of South Korea. Results of this study will be useful to the activation of geotourism and geological field study.

Experimental Study on the Shear Behavior of Reinforced Hooked-Steel-Fiver Concrete Beams (훅트강섬유보강 철근콘크리트보의 전단거동에 대한 실험적 연구)

  • 심종성;이차돈;김규선;오홍섭
    • Magazine of the Korea Concrete Institute
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    • v.7 no.5
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    • pp.179-188
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    • 1995
  • SFRC overcomes brittleness of concrete and has increases strength due to the action of confmement, crack arrestmg mechan~sm and pull out resistances of steel f~bers ~ n s ~ d e the concrete. These lead also to the increased strength and ductility under the shear stress. It has been reported that the secondary remforcement effect of steel fibers IS more pronounced In shear than flexure. Addition of hooked stee!, fibers into the cementitious materials enhanced shear resistance and consequently improves structural behavior and shear strength of Reinforced Hooked-Steel-Fiber Concrete Ream(RHSFCI3) under the shear forces. Experimental observations were made on the main parameters effecting structural behavior of RHSFCB in this study. The volume fractions of fibers, shear span to depth ratios, and spaclngs of stlrrups were taken into account as the mam parameters. Some eyuatlons reported in the literatures, regardmg the predict~ons of the shear strength of RHSFCB have been evaluated stdtlst~cdlly based on the tot a1 number of 95 test results on RHSFCB faded In shear on shear flexu~al mode.