• 제목/요약/키워드: sample recovery

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Informational Justice and Post-recovery Satisfaction in E-Commerce: The Role of Service Failure Severity on Behavioral Intentions

  • Kussusanti, Susanti;Tjiptoherijanto, Prijono;Halim, Rizal Edy;Furinto, Asnan
    • The Journal of Asian Finance, Economics and Business
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    • 제6권1호
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    • pp.129-139
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    • 2019
  • The purpose of this research is to examine the effect of informational justice on post-recovery satisfaction, and the effect of post-recovery satisfaction on behavioral intentions in e-commerce, including further investigate the moderating effect of service failure severity. Using quantitative method, the population of this research are online customers in Indonesia, with non-probability sampling that will be done by purposive sampling method based on predetermined criterias, which are customers who were doing transactions in the Business to Consumer (B2C) online sites, experienced service failure in the last 6 months, submitted a complaint, and received a response. Sample of 317 online customers were gathered and analyzed using the Structural Equation Modeling. The results of this study indicated that 5 hypothesis are supported with data. As a conclusion, informational justice and post-recovery satisfaction has positive effect, while service failure severity acts as a moderator between post-recovery satisfaction and behavioral intentions. As a managerial implication, online store management needs to ensure the informational justice to make a post-recovery satisfaction. Therefore, online store management needs to ensure the informational justice to make a post-recovery satisfaction, increase repurchase and positive e-word of mouth intention, also work harder to recover services, especially in high service failure severity condition.

Au/YBCO 박막 곡선에서의 회복 분석 (Analysis on Recovery in Au/YBCO thin Film Meander Lines)

  • 김혜림;임성우;오성용;현옥배
    • Progress in Superconductivity
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    • 제9권1호
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    • pp.119-125
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    • 2007
  • We investigated recovery in $Au/YBa_2Cu_3O_7$ (YBCO) thin film meander lines on sapphire substrates. The meander lines were fabricated by patterning YBCO films coated with gold layers. The lines were subjected to simulated AC fault current and then small current was applied for recovery measurements. The samples were immersed in liquid nitrogen during the experiment. After the fault, the resistance decreased linearly, first slowly and then fast to zero. The initial slow decrease was due to the decrease of the meander line temperature, whereas the fast decrease was originated from the transition from the normal state to the superconducting state. The recovery speed depended on the size of samples, and was faster in the smaller samples during the whole period of recovery. The experimental results were analyzed quantitatively with the concept of heat transfer within the sample and to the surrounding liquid nitrogen. A heat balance equation was solved for the initial phase of recovery, and an expression for the time dependence of resistance was obtained. The result agreed with data well.

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충전 솜사를 이용한 Bedspread Jaquard 직물의 물성과 보온성 (The Physical Properties and Warmth retaining of Bedspread Jacquard Fabrics Using Filling Batt Yarn)

  • 박명수
    • 한국의류산업학회지
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    • 제9권4호
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    • pp.445-449
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    • 2007
  • The results of warmth retaining, heat transfer and compressive elastic recovery of the five kinds of bedspread fabrics, which were produced from packing weft of 2700 denier and 3600 denier batt yarn treated with raw material of Polyester $150^D$/48 DTY, are as follows: 1) 3600 denier packing weft showed lover count in compressive elastic recovery than 2700d packing weft, so it took longer time to recover. 2) When packing weft of the same count is used, a sample of packing weft with higher density showed lower recovery. 3) It took 2700d packing weft 30min to get approximately 98% recovery in temperature $30^{\circ}C$. But, 3600d packing weft stayed under 98% recovery in the same temperature. Considering only the result of compressive elastic recovery, we should use 2700d packing weft. 4) The higher the density of packing weft is, the higher warmth retaining becomes. Although sharp increase appeared until 5min, equilibrium was kept without any increase after that time. 5) When 2700d packing weft was used, the maximum warmth retaining was approximately 60% and 64% in the conditions of density 12(thread/in) and 22(thread/in) respectively.

EAF 분전의 화학적처리에 와한 금속아연의 제조에 관한 연구 (The Study on the Recovery Process of Zinc Metal from EAF Dust by Chemical Treatment)

  • 정래윤;이진휘
    • 한국응용과학기술학회지
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    • 제27권2호
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    • pp.208-215
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    • 2010
  • EAF dust which is contained around 30% of zinc, 15% of iron and 3% of lead individually, is chemically treated by ammonium chloride, ammonia water, ammonia gas and carbon dioxide, and also tested and identified the ratios of the recovery of In by applied the variations of particle size, pH and heating temperature as well, in order to getting optimized recovery of the In metal after performing all of those processes. Experimental results showed that the rate of Zn recovery is 97% when the mixture of 1.3 of $NH_4Cl$/EAF is heated to the temperature of $400^{\circ}C$ and leached by water, and 95% recovery of In when ammonia gas and carbon dioxide is added simultaneously and adjust the 9.5 of pH to the same mixture above. For the purpose of remove the impurities in the mixed sample, which is prepared by the two samples, indicated above showing as the ratio of 95% and 97% recovery, in case of applied the cementation process to it, and also by electrolytic process, produced the In plate of 95~97%, and acquired 99-99.5% of In metal ingot finally by applied the heating process at $470{\sim}500^{\circ}C$.

생약복합제제(生藥複合製劑)의 약효연구(藥效硏究) 제7보(第7報) -생간건비탕(生肝健脾湯)의 간조직부활(肝組織復活)에 대(對)한 작용(作用)- (Studies on the Efficacy of the Combined Preparation of Crude Drugs (VII) -Effect of 'Saengkankunbi-Tang' on the Liver Tissue Recovery-)

  • 홍남두;김종우;김병운;손정곤
    • 생약학회지
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    • 제13권2호
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    • pp.70-78
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    • 1982
  • To investigate the effect of 'Saengkankunbi-Tang' on the liver tissue recovery in about 70% cutted rat liver, the observation on the photographing by the Gamma-camera and the electromicroscopic section against the rabbit liver induced by $CCl_4$, these studies were conducted. The results were summarized as follows; Observed on the liver tissue recovery, function regeneration and body weight increase in about 70% cutted rat liver, the recovery of liver tissue and body weight were increased with the passage of the time and also they were showed to the high increase rate in proportion to administration amount. The glucose content in the serum was found in increasing tide as compared with the control group. The alkaline phosphate activity in the serum showed the significant difference in the 10th day and 13th day as compared with the control group. The ammonia content in the blood showed the significant difference only in the 10th day. Observed on the photographing by the Gamma-camera against the rabbit liver induced by $CCl_4$, sample groups were shown to be significant recovery as compared with the control group. Observed on the electromicroscopic section, sample groups showed the control action of the nuclear destruction against the rabbit liver induced by $CCl_4$ and also they showed the control action of the expansion of glycogen and granular endothelial reticulum in cytoplasm. According to the above finding, it is presume that 'Saengkankunbi-Tang' can be applicable to the extensive treatment of liver disease.

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PVC 여과지를 이용한 금속 분석방법에 대한 정확도와 정밀도 평가 (Evaluation of Accuracy and Precision of Analysis of Metals with Polyvinyl Chloride Membrane Filters)

  • 변성욱;최상준
    • 한국산업보건학회지
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    • 제26권1호
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    • pp.48-57
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    • 2016
  • Objectives: This study was conducted to evaluate the accuracy and precision of airborne metal analysis using polyvinyl chloride(PVC) membrane filter by pretreatment methods. Methods: A total of 75 spiked PVC samples for Cr, Fe and Mn ranged from 6 ug/sample to 40 ug/sample were used to evaluate recovery rates for three pretreatment methods: acid extraction, hot plate ashing and microwave digestion. For Mn, an additional 75 spiked mixed cellulose ester(MCE) membrane filters were analysed to compare the recovery rates of PVC samples. All samples were analysed with an inductively coupled plasma optical emission spectrometer(ICP-OES) and manganese samples were additionally analyzed by atomic absorption spectrometer(AAS). Results: The overall mean recovery rates of PVC samples for Cr, Fe and Mn were 90% or higher regardless of pretreatment methods, but there were statistically significant differences in recovery rates for Cr(p<0.05) and Mn(p<0.01) samples by pretreatment methods. The biases and the coefficient variations of PVC samples for three metals pretreated with three kinds of pretreatment methods ranged from 1.7% to 4.7% and from 1.6% to 6.5%, respectively. The manganese PVC samples pretreated by microwave digestion and analyzed with ICP-OES had the lowest bias at 1.9% and also showed lower bias than the bias for MCE samples, 2.7%. Conclusions: In order to accurately analyze the metals sampled with PVC membrane filters, microwave digestion and ICP-OES can be recommended.

VDL Mode-2에 적용 가능한 버스트 모드 심벌 타이밍 복원기 (Burst Mode Symbol Timing Recovery for VDL Mode-2)

  • 김종만;최승덕;은창수
    • 한국항행학회논문지
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    • 제13권3호
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    • pp.337-343
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    • 2009
  • 본 논문에서는 D8PSK 변조 방식을 이용하는 VDL Mode-2 수신기에 적용 가능한 버스트 모드 심벌 타이밍 복원기를 제안하고 성능 분석과 연동실험을 실시하였다. IIR 루프필터를 사용하여 심볼 타이밍 에러를 최소화 하는 방식은 수렴 속도가 늦기 때문에 버스트 모드에 적용하기 곤란하다. 즉 빠른 수렴 특성이 중요시 된다. 본 논문에서 제안한 방식은 프리앰블을 이용하여 초기 동기가 이루어진 후 최대 심벌 전력을 갖는 방향으로 한 샘플 빠르게 또는 한 샘플 느리게 샘플 클럭을 이동하여 최적의 심벌을 취하는 방식이다. 제안된 방식을 적용한 수신기와 호주 ADS사 송신 장비와 연동 시험한 결과 100 ppm 이상에서도 잘 동작함을 확인하였다.

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Solid Phase Microextraction법을 이용한 식품포장재 중의 잔류용제 분석 (Analysis of Residual Solvents in Food Packaging Materials Using Solid Phase Microextraction Method)

  • 서택교;박상현;이윤수;김정한;권익부
    • 한국식품위생안전성학회지
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    • 제14권1호
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    • pp.76-83
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    • 1999
  • Solid phase microextraction (SPME) was used for the determination of 6 standard solvents (methanol, isopropanol, methyl ethyl ketone, ethyl acetate, cyclohexane, toluene) in food packaging materials. SPME method is a solvent-free sample preparation technique in which a fused silica fiber coated with polymeric organic liquid is introduced into the headspace above the sample. SPME method using fiber coated polydimethylisiloxane (PDMS) was compared with static headspace (SHS) method used as a reference. It was found that the optimal adsorption condition using PDMS-SPME method was 2$0^{\circ}C$ for 15 minutes for the standard solvents. Detection limits, linearity, reproducibility and recovery of both SHS and PDMS-SPME methods have been determined using 6 standard solvents. Both methods were characterized by high reproducibility and good linearity. Using SHS methods, the mean recovery of the 6 standard solvents was ranged from 75.5% to 105.8% with a mean relative standard deviation (RSD) of 0.3% to 4.8%. With PDMS-SPME method, the mean recovery of the 6 standard solvents was ranged from 86.7% to 108.3% with a mean RSD of 0.4% to 2.5%. The detection limits of both methods were the same for toluene, cyclohexane and methyl ethyl ketone; those of PDMS-SPME method were higher than those of SHS method for methanol, isopropanol and ethyl acetate. PDMS-SPME fiber shoed excellent adsorption for non-polar solvents such as toluene, while it showed relatively low adsorption for polar solvents such as methanol.

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Development of Pretreatment Method for Analysis of Vitamin B12 in Cereal Infant Formula using Immunoaffinity Chromatography and High-Performance Liquid Chromatography

  • Park, Jung Min;Koh, Jong Ho;Kim, Jin Man
    • 한국축산식품학회지
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    • 제41권2호
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    • pp.335-342
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    • 2021
  • Vitamin B12 deficiency may lead to serious health issues in both infants and adults. A simple analytical method involving sample pretreatment with enzyme, followed by cyanide addition under acidic conditions; separation on an immunoaffinity column; and high-performance liquid chromatography (HPLC) was developed for the rapid detection and quantitation of vitamin B12 in powdered milk. Detection limit and powdered milk recovery were determined by quantitative analysis. The limits of detection and quantitation were 2.71 and 8.21 ㎍/L, respectively. Relative standard deviations of the intra-day and inter-day precisions varied in the ranges of 0.98%-5.31% and 2.16%-3.90%, respectively. Recovery of the analysis varied in the range of 83.41%-106.57%, suggesting that the values were acceptable. Additionally, vitamin B12 content and recovery in SRM 1849a were 54.10 ㎍/kg and 112.24%, respectively. Our results suggested that the analytical method, including the sample pretreatment step, was valid. This analytical method can be implemented in many laboratory-scale experiments that seek to save time and labor. Therefore, this study shows that immunoaffinity-HPLC/ultraviolet is an acceptable technique for constructing a reliable database on vitamin B12 in powdered milk containing starch as well as protein and/or fat in high amounts.

Pd nanoparticles on poly(amidoamine) dendrimers modified single-walled carbon nanotubes as highly sensitive hydrogen gas sensors

  • Lee, Jun-Min;Lee, Eun-Song-Yi;Jeon, Kye-Jin;Ju, Seong-Hwa;Jung, Yeong-Ri;Kim, Sung-Jin;Lee, Woo-Young
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2009년도 춘계학술대회 논문집
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    • pp.93-93
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    • 2009
  • In order to overcome the lack of reactivity with hydrogen gas ($H_2$) and utilize unique properties of Carbon Nano Tubes (CNTs) for the application to hydrogen sensors, there have been intensive works on the surface functionalization of CNTs with various types of nanoparticles including Pd. In the present work, we have investigated the effect of dendrimers and Pd nanoparticles to the hydrogen sensing properties of CNTs by comparing three types of samples: Pd/SWNTs (Sample I), Pd/dendrimer/SWNTs (Sample II) and heat-treated Pd/dendrimers/SWNTs (Sample III). As a result of IV measurement under the $H_2$ and air, sample I was found to have a high sensitivity (25%) to $H_2$, but to have a very slow response time (324 s) and recovery rate. On the other hand, Sample II was found to show much faster response time (3 s) and good recovery rate but lower sensitivity (8.6%) than Sample I which is due to induced dipole moments in the dendrimers. Interestingly, Sample III showed both fast response time (7 s) and high sensitivity (25%), indicating that the pyrolysis of the dendrimers during heat treatment which reduce the distance between the surface of the SWNTs and the functionalized Pd nanoparticles plays a key role in improving the sensitivity. The pyrolysis of the dendrimers in Pd nanoparticle-dendrimer-SWNTs was found to enable a significant electrical conductance modulation upon exposure to extremely low concentrations (10 ppm) of $H_2$ in air. Our results demonstrate that the Pd Nanoparticle-Grafted Single-Walled Carbon Nanotubes(SWNTs) with Dendrimers can be used to detect hydrogen, makingoutstanding properties such as fast response, and recovery time, high sensitivity, low detection limit at room temperature compared with other types of hydrogen sensors.

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