• Title/Summary/Keyword: salting methods

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Salting-out extraction of ginsenosides from the enzymatic hydrolysates of Panax quinquefolium based on ethanol/sodium carbonate system

  • Wei, Yingqin;Hou, Baojuan;Fang, Haiyan;Sun, Xinjie;Ma, Feng
    • Journal of Ginseng Research
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    • v.44 no.1
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    • pp.44-49
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    • 2020
  • Background: Salting-out extraction (SOE) had been developed as a special branch of aqueous two-phase system recently. So far as we know, few reports involved in extracting ginsenosides with SOE because of the lower recovery caused by the unique solubility and surface activity of ginsenosides. A new SOE method for rapid pretreatment of ginsenosides from the enzymatic hydrolysates of Panax quinquefolium was established in this article. Methods: The SOE system comprising ethanol and sodium carbonate was selected to extract ginsenosides from the enzymatic hydrolysates of Panax quinquefolium, and HPLC was applied to analyze the ginsenosides. Results: The optimized extraction conditions were as follows: the aqueous two-phase extraction system comprising ethanol, sodium carbonate, ethanol concentration of 41.51%, and the mass percent of sodium carbonate of 7.9% in the extraction system under the experimental condition. Extraction time had minor influence on extraction efficiency of ginsenosides. The results also showed that the extraction efficiencies of three ginsenosides were all more than 90.0% only in a single step. Conclusion: The proposed method had been successfully applied to determine ginsenosides in enzymatic hydrolysate and demonstrated as a powerful technique for separating and purifying ginsenosides in complex samples.

Composite Membrane Preparation for Low Pressure Using Salting-Out Method and Its Application to Nanofiltration Process (염석법에 의한 저압용 역삼투막 제조 및 NF로의 적용)

  • Jeon, Yi Seul;Rhim, Ji Won
    • Membrane Journal
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    • v.25 no.5
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    • pp.440-446
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    • 2015
  • Nanofiltration composite membranes were prepared through the ion exchange polymers coating onto the porous microfiltration polyethylene (PE) membrane surfaces the salting-out and phase separated and pressurization (PSP) methods. The existence of coating on the surfaces was confirmed by the scanning electronic microscopy. The resulting membranes were characterized under the various conditions, such as the coating material, coating time, ionic strength etc., in terms of flux and rejection for NaCl 100 ppm solution. Under the same coating conditions of 10,000 ppm coating solution concentration and 3 atm coating pressure for both the coating materials of PEI and PSSA_MA, the flux 91.2 LMH and rejection 64.6% were obtained for PEI whereas 122.7 LMH and 38.1% were observed for PSSA_MA. From this study, it may be concluded that the composite membrane preparation is possible.

Evaluation of brine reuse on salting of chinese cabbage using electrochemical process (전기화학적 처리에 의한 배추 절임염수 재이용 가능성 평가)

  • Jung, Heesuk;Lee, Eunsil;Han, Seongkuk;Han, Eungsoo
    • Journal of Korean Society of Water and Wastewater
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    • v.28 no.5
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    • pp.541-548
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    • 2014
  • The pickling brine generated from the salting process of kimchi production is difficult to treat biologically due to very high content of salt. When pickling brine is treated and discharged, it cannot satisfy the criteria for effluent water quality in clean areas, while resources such as the salt to be recycled and the industrial water are wasted. However, sterilization by ozone, UV and photocatalyst is expensive installation costs and operating costs when considering the small kimchi manufacturers. Therefore there is a need to develop economical process. The study was conducted on the sterilization efficiency of the pickling brine using electrochemical processing. The electrochemical treatment of organic matters has advantages over conventional methods such as active carbon absorption process, chemical oxidation, and biological treatment because the response speed is faster and it does not require expensive, harmful oxidizing agents. This study were performed to examine the possibility of electrochemical treatment for the efficient processing of pickling brine and evaluated the performance of residual chlorine for the microbial sterilization.

Characteristics of Growth and Salting of Chinese Cabbage after Spring Culture Analyzed by Cultivar and Cultivation Method (봄배추 재배방법 및 품종에 따른 생육 및 절임 특성)

  • Lee, Jung-Soo;Park, Su-Hyung;Lee, Youn-Suk;Lim, Byung-Sun;Yim, Sang-Chul;Chun, Chang-Hoo
    • Food Science and Preservation
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    • v.15 no.1
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    • pp.43-48
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    • 2008
  • This experiment investigated the characteristics of salted and fresh Chinese cabbages of different cultivars and using various cultivation methods. We measured the numbers of leaves, sizes, thicknesses, moisture contents, and firmness qualities of fresh Chinese cabbage grown in a plastic house, and outdoors. 'The bulb sizes, leaf thicknesses, and moisture contents of leaves were higher after plastic house cultivation than after growth in the field. Plastic house culture increased the growth rate of Chinese cabbage. Firmness and osmolarity showed better values after outdoor cultivation, however. The growth rates and the levels of chemical components were affected by interactions between cultivation methods and cultivars of Chinese cabbage. The salt levels of salted Chinese cabbage were 1.21.7% (w/w) after cabbages cultivated outdoors were preserved, and 0.91.2 % (w/w) after vegetables grown in a plastic house were treated. The quality properties of postharvest Chinese cabbages after salting varied with cultivation method even when the same cultivars of Chinese cabbage were used. The salt contents of salted Chinese cabbage thus varied with different cultivation methods. The results indicate that the properties of Chinese cabbage vary with the culture systems adapted.

Processing Conditions of Salted Anchovy 2. Changes of Taste Compounds during Processing of Salted Anchovy by Salting Methods (염장 멸치의 제조조건 2. 염장방법에 따른 염장 멸치의 가공 중 맛성분의 변화)

  • CHO Young-Je;SHIM Kil-Bo;JU Jung-Mi;KIM Tae-Jin;YOOK Ji-Hee;CHO Min-Sung
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.36 no.1
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    • pp.18-23
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    • 2003
  • We investigated the changes of free amino acid, ATP related compounds and sensory evaluation during ripening of dry or brine salted-anchovy. The total free amino acid content of the salted-anchovy ripened at $20^{\circ}C$ was higher than that of the salted-anchovy ripened at $5^{\circ}C.$ The IMP content of raw anchovy was higher than that of any other ATP related compound and decreased rapidly during ripening, resulting in increased hypoxanthin (Hx). The sensory evaluation results indicated 5 and 4 months for dry and brine salted-anchovy, respectively, as the minimum time required to obtain an adequate ripened salted-anchovy. We concluded that processing condition of ripened salted-anchovy was to ripened for 5 months at $5^{\circ}C$ by drying salting method.

A Survey on the Sensory Preference for Making Summer Kimchi by Nationwide Region (여름철 배추김치 담금시 지역별 관능적 선호도 조사)

  • Cha, Yong-Jun;Kim, Hun;Cho, Wo-Jin;Jung, Yeon-Jung;Lee, Young-Mi;Kim, Eun-Jeong
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.32 no.3
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    • pp.393-399
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    • 2003
  • The purpose of this study was to investigate the preferred methods for making summer kimchi as a basic research of making commercial kimchi. Questionnaire were collected from 590 housewives nationwide in Korea, and the data were analyzed by SPSS program. The results were as follows: (1) The average salting time of Chinese cabbage was 3~5 hrs when the combined method of dry and brine salting was used, regardless of the region. (2) Seven jeotkals (salt-fermented fishes) including anchovy, anchovy juice, shrimp, northern sand lance juice, hair-tail viscera, flatfish and yellow corvenia were mainly used in kimchi. Among them, anchovy and anchovy juice jeotkals were preferred to all others in Southern area (Busan, Gwangju, Gyeongnam, Gyeongbuk, Jeonnam), while shrimp jeotkal in Seoul, Gwangju, Jeonbuk, Chungnam and Jeju, and northern sand lance juice jeotkal in Daegu, Daejeon and Gyeonggi, respectively. In most regions, however, blending type of 2 jeotkals was used in kimchi. (3) Eleven ingredients such as red pepper, garlic, ginger, green onion, radish, leek, onion, carrot, sugar, sesame and MSG were used as basic components for making kimchi. In particular, MSG was used as a basic ingredient regardless of region and age. However, a standard taste for making kimchi was depended on housewife in this study.

Distribution of Trypsin Indigestible Substrate(TI) in Seafoods and Its Changes during Processing 3. Changes in TI and Protein Quality of Salted and Dried Yellow Corvenia(Pseudosciaena manchurica) during Processing and Storage (어견류의 Trypsin활성 저해물질의 분포와 가공중의 변화 3. 염건조기 가공저장중의 TI 및 단백질품질변화)

  • LEE Kang-Ho;KWON Hae-Ran;RYU Hong-Soo
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.17 no.2
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    • pp.109-116
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    • 1984
  • In order to assess the protein nutritional quality of salted and dried yellow corvenia, which was prepared using the different salting methods like dry and brine salting, the changes of trypsin indigestible substrate(TI) and in vitro apparent protein digestibility were studied during storage at room temperature($24{\pm}1^{\circ}C$). It was also examined the retention of available lysine and formation of nonenzymatic brown pigments under the same conditions of preparing and storage mentioned above and confirmed the relationship between in vitro digestibility and the antinutritional factors, such as nonenzymatic browning, unavailability of lysine and TI content, TI content was gradually increased during the storage and in showed $1.5{\sim}2$ times more after 57 days storage than at the initial stage which ranged from 0.11 to 0.17mg/g solid. Of all the products, $25\%$ brine salting product contained the least TI content in 0.21 mg/g solid, while $10\%$ dry salting products was the most abundant in 0.30 mg/g solid using Hamerstrand method(1981). In vitro protein digestibility of all dried products was decreased significantly up to 30 days as the contents of TI increased, except $25\%$ brine salted products. After storing for 57 days, the in vitro digestibility was only $4\%$ drip showed in $25\%$ brine salted products. The nonenzymatic brown pigments were also developed on the level of available lysine reduced as in vitro protein digestibility was decreased throughout storage. Of all the various salted and dried products of yellow corvenia, $25\%$ salting product showed the lowest rate of browning development and loss of available lysine. Therefore, it was revealed that unavailability of lysine and development of nonenzymatic brown pigments were major factors influencing the protein quality in salted and dried yellow corvenia.

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Biogenic Amine Contents in Fish Products (수산가공품의 biogenic amine 함량 변화)

  • Cho, Young-Je;Son, Myoung-Jin;Kim, Seung-Mi;Park, Hyun-Kyu;Yeo, Hae-Kyung;Shim, Kil-Bo
    • Journal of Fisheries and Marine Sciences Education
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    • v.20 no.1
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    • pp.127-134
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    • 2008
  • The purpose of this study was to determine content of biogenic amines (Histamine, Cadaverine, Putrescine) in the salted mackerel, canned mackerel, mackerel pike, and freeze dried mackerel pike (Guamegi) collectively, all were purchased in the market. Salted mackerel was purchased at five markets (A, B, C, D, and F market) and stored for 10 days at $4{^{\circ}C}$. At the time of purchase, salted mackerel purchased at markets A, B and C was tested for biogenic amine, yet nothing was detected. However, salt mackerel purchased at market D was tested and the histamine concentration was 0.5 mg/100g. Mackerel from market F, exhibited content levels of 0.5 mg/100g histamine and 1.6 mg/100g cadaverine. Those make certain safety during self-life but that purchased F market gradually increased biogenic amine during storage. Prepared salted mackerel of varying levels of freshness and processing methods were analyzed for biogenic amines. Salting process was performed using functional brine salt. VBN (volatile basic nitrogen) was used to establish freshness levels of salted mackerel. Analyses of mackerel muscle determined the values of freshness to be 9.2 mg/100g (good freshness), 18.2 mg/100g (bad freshness), respectively. After 40 days of storage, the content of histamine, cadaverine, putrescine in the freshness of salted mackerel was 2.0 mg/kg, 2.4 mg/kg and 0 mg/kg, respectively. The content of histamine, cadaverine, putrescine in salted mackerel of poor freshness was 71.3 mg/kg, 22.9 mg/kg and 17.8 mg/kg, respectively. It was concluded the presence of biogenic amines during the salting process of salted mackerel significantly effected freshness of materials. The presence of biogenic amines were detected in mackerel that underwent the salting process after 1 month of storage at $4{^{\circ}C}$. The levels of biogenic amines in the brine salted mackerel were higher than those found in dry, salted mackerel; however, the freshness of fish had an insignificant effect on biogenic amines. The presence of histamine was detected in small quantities in canned mackerel and mackerel pike from three companies. Alternatively, cadaverine and putrescine were not detected. Guamegi, vacuumed packed or sealed with a rope was purchased from three markets (A, B, C seafood company). Guamegi was stored and observed for 180 days at $-20{^{\circ}C}$. Histamine was detected in small quantities in all products stored at $-20{^{\circ}C}$. Levels of histamine was dependent on the types of packaging, rope packaging yielded the highest level. However, other amines were not detected.

Preparation and Performance of Low Pressure PVDF Nano-composite Hollow Fiber Membrane Using Hydrophilic Polymer (친수화 고분자 소재를 이용한 저압용 PVDF 나노복합중공사막의 제조 및 성능 연구)

  • Park, Cheol Oh;Rhim, Ji Won
    • Membrane Journal
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    • v.28 no.5
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    • pp.361-367
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    • 2018
  • In this study, the nanofiltration (NF) composite membranes for the low pressure use were prepared using polyvinylidene fluoride (PVDF) hollow fiber membrane as a supporter. Poly styrene sulfonic acid (PSSA) and polyethyleneimine (PEI) were coated onto the PVDF membrane by both layer-by-layer and salting-out methods. To characterize the prepared NF membranes in terms of the flux and salt rejection, 100 mg/L feed solutions of NaCl, $MgCl_2$, and $CaSO_4$ were used at the flow rate of 1 L/min and the operating pressure of 2 bar at room temperature. The NF membranes coated with 20,000 ppm PSSA (ionic strength 1.0) solution for 3 minutes and then 30,000 ppm (ionic strength 0.1) solution for 1 minute were observed the best performance. The permeability and salt rejection were 38.5 LMH, 57.1% for NaCl, 37.9 LMH and 90.2% for $MgCl_2$ and 32.4 LMH and 54.6% for $CaSO_4$, respectively.

Review of Literature on Food Preservation of the Early Joseon Dynasty (조선전기 고문헌에 수록된 식품저장법에 대한 문헌고찰)

  • Kim, MyeongJun;Cha, GyungHee;Chung, HyeJung
    • Journal of the Korean Society of Food Culture
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    • v.35 no.1
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    • pp.28-54
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    • 2020
  • This study aims to investigate the food preservation methods adopted by the Joseon Dynasty, which existed before the 17th century. A total of 232 food preservation methods were discovered in 25 books, and could be classified by their targeted food types: vegetables (84), sea foods (60), meats (41), fruits (37), and others (10). Depending on the preservation method applied, they are classified as food drying, soaking, mud cellar preservation, and other preservation. Food drying is further classified into 8 sub-types: drying, sun-drying, shadow-drying, wind-drying, dry heat, combined drying, smoking, and others. Soaking could be sub-divided into using salt, ash, dry sand, bran, fermented paste, wet distillers grains, oil, and others. Mud cellar preservation is sub-classified into installing shelf inside the mud cellar, making the mud cellar for food preservation, and making hole or underground tunnel for food preservation. Other food preservation methods include minimizing moisture loss by applying beeswax on a section of the vegetable stem, and cutting the vegetables or fruits with their branches and leaves for food preservation.