• Title/Summary/Keyword: salt solution

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Toluene 용액 캐스팅에 의한 차출용 전도성 Polyaniline-HIPS 블렌드 제조 (Preparation of the Conducting Polyaniline-HIPS Blends for Injection Molding by Toluene Solution Casting)

  • 이종혁;김은옥
    • 폴리머
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    • 제33권3호
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    • pp.203-206
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    • 2009
  • 화학적 산화중합에 의한 Polyaniline Emeraldine salt(PANI-salt)는 도펀트로 존재하는 HCl과 같은 양성 자산으로 인한 금속성 사출금형 부식이 발생한다. 본 연구에서는 비극성 유기용매인 톨루엔, 포펀트와 계면활성제 역할을 하는 dodecylbenzenesulfonic acid(DBSA)를 사용하여 유화 중합법으로 PANI-salt를 합성한 후, 공용매 toluene에서 PANI-salt와 high impact polystyrene(HIPS)를 다양한 비율로 solution-cast 혼합하여 PANI-HIPS 블렌드를 얻었다. PT-IR과 UV-Vis.로 PANI-salt 구조를 확인하였고, PANI-HIPS 블렌드의 모폴로지, 열적 및 전기적 특성을 확인하였다. PANI(50 mL)와 HIPS(1 g)을 혼합하여 사출온도 $103^{\circ}C$, 사출압력 120 psi 하에서 사출한 PANI-HIPS 사출품에서 가장 높은 전기전도도($6.02{\times}10^{-5}\;S/cm$)가 나타났다.

METHODS TO IMPROVE UTILIZATION OF RICE STRAW I. EFFECTS OF MOISTENING, SODIUM CHLORIDE AND CHOPPING ON INTAKE AND DIGESTIBILITY

  • Badurdeen, A.L.;Ibrahim, M.N.M.;Schiere, J.B.
    • Asian-Australasian Journal of Animal Sciences
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    • 제7권2호
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    • pp.159-164
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    • 1994
  • Two studies were conducted using 40 cross-bred bulls to study the effect of chopping, moistening with water or common salt solution on the nutritive value of rice straw (variety BG-400). Moistening with water did not significantly effect digestibility or intake of rice straw. As compared to straw fed in the long form, chopping did not significantly influence intake (2.33 vs 1.97kg $100kgBW^{-1}day^{-1}$, respectively), but significantly (p<0.05) decreased the digestibility (41.6 vs 37.4%) and intake of digestible dry matter (0.99 vs 0.74kg $100kgBW^{-1}day^{-1}$). Rice straw moistened with 2 or 4% common sea salt solution and directly fed to animals (Exp. 1) did not significantly effect its digestibility (43.9 and 43.1%, respectively) or intake (2.66 or 2.59kg $100kgBW^{-1}day^{-1}$, respectively), but over night storing of 2% salt solution sprayed straw (Exp. 2) significantly reduced its digestibility (33.6%). The latter is difficult to explain because the sodium concentration (mg/g straw dry matter) was lower than 4% salt solution treatment used in experiment 1 (3.30 vs 5.22). It is concluded that chopping, moistening with water or NaCl salt solution did not significantly improve the nutritive value of rice straw.

염 용액에서의 화학적 이온교환 강화유리에 관한 연구 (A Study on the Glass Strengthened in Salt Solution by Chemical Ion Exchange)

  • 이종근;김인섭
    • 한국세라믹학회지
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    • 제24권4호
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    • pp.335-342
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    • 1987
  • There were several numbers of studies on chemically strengthening glass. Most of them were strengthened in molten salt bath below transformation range of glass. Apart from them, this study used solution hydration technique by Autoclave. After determining proper concentration of AgNO3 salt solution, experimental condition varied from 4hrs to 16hrs at relatively low temperature (180, 200, 220$^{\circ}C$). The results showed that the Soda-Lime-Silica glass could be strengthened by diffusion mechanism without influence of water above 15% salt solution. Because of Ag+ ion penetration in glass surface, yellow color appeared and decreased transmittance at visible range. Modulus of rupture was increased with the amount of exchange and brittleness was decreased.

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염지액의 식염농도와 염지기간이 돼지고기의 염용성단백질의 추출성, 소편화, 보수력, 식염함량 및 기호성에 미치는 영향 (Effects of Salt Concentrations of Curing Solution on Myofibrillar Protein Extractability, Fragmentation, Water Holding Capacity, Salt Contents and Palatability of Cured Pork Loins)

  • 문윤희;김영길;현재석;이종호;정인철
    • 한국식품영양과학회지
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    • 제31권6호
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    • pp.999-1004
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    • 2002
  • 식염농도를 3, 5, 7 및 9%로 각각 조제한 2$^{\circ}C$의 염지액에 등심고기를 20일간 염지하면서 식염농도와 염지기간이 근원 섬유단백질의 추출성과 소편화도, 보수력, 식염함량 및 기호성에 미치는 영향을 검토하였다. 식염농도 3, 5 및 7%의 염지액에 염지한 등심고기 근원섬유단백질의 추출성과 보수력은 염지 20일까지, 근원섬유 소편화도는 염지 16일까지, 모두 식염농도가 높을수록 점점 높게 나타났으며, 9%의 염지액에 염지한 것은 일정한 경향을 보이지 않았다. 가열육의 색도는 염지액의 식염농도가 높을수록, 그리고 염지 16일까지 점점 양호하게 나타났다 염지액의 식염농도 3%에서는 염지육의 발색이 균일하게 되지 않았으며, 9%에서는 발색이 잘 되었으나 풍미와 종합적인 기호성이 좋지 않았다. 등심고기는 염지액의 식염농도5%에서 16일, 또는 7%에서 12일 염지하면 기호성이 우수하게 되었다.

오이장아찌 제조 중 산도, pH, 염도 및 관능적 품질변화에 관한 연구 (The Acidity, pH, Salt Content and Sensory Scores Change in Oyijangachi Manufacturing)

  • 정순택;이홍열;박현진
    • 한국식품영양과학회지
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    • 제24권4호
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    • pp.606-612
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    • 1995
  • Three different Oyijangachi(Kochujang, Doenjang and Ganjang) have been prepared by traditional method. Cucumbers have been dipped in six different solutions for 48 hrs. After dipping, the cucumbers have been aged in Kochujang, Doenjang and Ganjang for 30 days. The acidity, pH, salt content and sensory evaluation of the cucumbers which were treated by six different solutions has measured. Moisture content of fresh cucumber was 95%, and the moisture content of Kochujang, Doenjang and Ganjang of Oyijangachi was 66.78%, 76.94% and 81.33%, respectively, after 30 days of aging. Protein content fo Kochujang, Doenjang and Ganjang of Oyijangachi increased 57%, 258% and 197%, respectively, after 30 days of aging when they compared with fresh cucumber(control). Initial acidity of Oyijangachi of cucumbers which were treated with solution 1~5 at 0 day were between 0.49 and 0.56 and increased during aging. Initial acidity of Oyijangachi treated with solution 6 was 1.84 which was low because 1% of acetic acid was added and acidity increased during aging. The pH of Kochujang, Doenjang, and Ganjang of Oyijangachi decreased 4.37, 3.98 and 4.61, respectively, after 30 days aging. Salt content of Oyijangachi dipped in various salt solutions increased as the salt content of the solution increased. Salt content of three Oyijangachi increased drastically during 0~5 days of aging and slowly increase between 5~30 days of aging. The taste and smell of Kochujang Oyijangachi were highest as treated wih 12% NaCl solution(treatment 4) and the color was highest when the Oyijangachi was treated with solution 1. The taste, smell and color of Doenjang Oyijangachi were highest as treated with 12% NaCl solution plus CaCl2(treatment 5). It was observed that the firmness of Oyijangachi was generally higher as the cucumber treated.

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해양심층수염, 천일염 및 정제염을 이용한 참외절임시 품질특성 비교 (Comparison of Quality Characteristics of Salted Muskmelon with Deep Seawater Salt, Sun-dried and Purified Salts)

  • 이기동;김숙경;김정옥;김미림
    • 한국식품영양과학회지
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    • 제32권6호
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    • pp.840-846
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    • 2003
  • 참외피클을 제조하고자 해양심층수염, 천일염 및 정제염을 사용하여 참외의 절임시 이화학적, 관능적 특성에 대해 조사하였다. 참외의 절임기간 동안 중량, 수축률, 염도 및 pH의 변화는 소금의 종류에 따른 차이가 거의 없었다. 절임염수의 탁도는 천일염을 사용한 구에서 가장 높게 나타났으며, 해양심층수염과 정제염은 거의 변화가 없었다. 절임염수의 가용성 고형물 함량은 천일염을 사용한 것에서 정제염과 해양심층수염에서 보다 높게 나타났다. 절 임기간 동안 참외의 칼슘 함량은 해양심층수염과 천일염에서 절임 2일째에 약 4.3배, 3.7배까지 증가하였다. 심층수, 천일염을 사용한 참외 조직 감의 변화는 hardness가 정제염보다 다소 높게 나타났다. 관능검사 결과 해양심층수염을 절임염수로 사용한 참외의 색, 향, 맛, 물성 및 전반적인 기호도가 절임기간이 증가함에 따라 다른 천일염이나 정제염으로 절임한 참외보다 우수한 관능평점을 나타내었다.

시판 소금이 깍두기 무의 경도에 미치는 영향 (Effect of Salts on the Hardness of Cubed White Radish)

  • 박희옥;장재선
    • 한국식품영양학회지
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    • 제22권2호
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    • pp.238-245
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    • 2009
  • The principal objective of this study was to investigate the association of variable salts with the hardness of cubed white radish. We analyzed the contents of domestic sun-dried salt, Chinese sun-dried salt, domestic refined salt, Australian rock salt and Australian industrial sun-dried salt in the radish samples. Our assessment of the water content of variable salts showed that domestic refined salt was highest(7.27%) and Australian rock salt was lowest(0.16%). The NaCl contents of variable salts were as follows : 93.23% in refined salt, 93.76% in Australian rock salt, 87.85% in domestic Shinan sun-dried salt and 87.98% in Chinese sun-dried salt. The content of insoluble matter in water were $0.03{\sim}0.05%$ in all salts except 0.85% in Australian industrial sun-dried salt. The pH values of salts were as follows : 8.93 in domestic sun-dried salt, 8.62 in Chinese sun-dried salt, 6.69 in refined salt, 5.83 in Australian rock salt and 6.41 in Australian industrial sun-dried salt. Regarding the mineral component content assays, domestic salt was found to harbor lower Na content but far higher Mg, K, Ca contents than other salts. In our evaluation of the hardness of cubed white radish, we detected a continuous increase in the hardness of cubed white radish soaking in a 4% salt solution of domestic Shinan natural salt, but an initial increase followed by a decrease in the hardness of cubed white radish soaking in a 4% solution of the other salts.

데침과 열수의 침적과 Trehalose 처리가 오이 물김치의 저장중 품질에 미치는 영향 (The Properties of Blanching and Brining in Hot Solution and Trehalose Treatment on the Quality of Cucumber Kimchi during Fermentation)

  • 이혜정
    • 한국식품영양학회지
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    • 제14권4호
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    • pp.333-338
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    • 2001
  • In research. which Korean pickled cucumber was treated wish various methods, including blanching. brining in hot solution, and treating with trehalose. I examined the changes of properties of material. The Korean pickled cucumber were fermented 4∼5$^{\circ}C$ for 42 days in 1% salt solution. The physiochemical properties were pH, total acidity, total cell count, lactic acid bacteria and texture properties were also evaluated. The result showed that the effect of blanching and soaking cucumber in 100$^{\circ}C$ hot salt solution significantly reduced the softening rate of texture while a rather rapid fermentation was found for those preserved with salt. The effect of trehalose treatment inhenced fermentation but it was significantly reduced softening rate of texture. The texture evaluation of Korean pickled cucumber was found that heat treatment with blanching after soaked in hot solution and trehalose treatment had a positive effect for reduction of softening of cucumber tissue.

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상압수용액중에서 인산석고로부터 $\alpha$형 반수석고의 생성에 미치는 염류의 영향 (Effect of Salt on the Formation of $\alpha$-Calcium Sulfate Hemihydrate from by-Product Gypsum of Phosphoric Acid Process in Aqueous Salt Solution at Atmospheric Pressure)

  • 이구종;최상흘
    • 한국세라믹학회지
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    • 제25권1호
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    • pp.66-72
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    • 1988
  • The effect of salts on the formation of ${\alpha}$-hemihydrated gypsum at boiling temperature under atmospheric pressure was studied by the solubility measurement method, and the formation of ${\alpha}$-hemihydrated gypsum from by-product gypsum of phosphoric acid process in the salts solution were investigated. The order of catalytic effect of salt on the formation of ${\alpha}$-hemihydrated gypsum are as follows: NH4Cl>NaCl>NaNO3. In the salts solution of sodium nitrate, sodium chloride, and ammonium chloride, prismatic ${\alpha}$-hemihydrated gypsum was obtained and the crystal form was converted to needle form in complex solution with sulfuric acid. The P2O5 content in gypsum was largely decreased in this atmosphoric solution process.

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반응표면 분석법을 이용한 마늘 열풍건조 공정의 최적화 (Development of Optimum Processing Conditions in Air Dried Garlics Using Response Surface Methodology)

  • 김명환;김병용
    • 한국식품영양과학회지
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    • 제19권3호
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    • pp.234-238
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    • 1990
  • The effects of salt concentration immersion time in a salt solution prior to air dehydration and heating of air temperature during dehydration upon the browning reaction and pyruvic acid content of air dried garlics to a 6.5% moisture content(wet basis) were analyzed by a response surface methodology(RSM), Those values were also predicted by using a second degree polynomial regression model. Heating of air temperature was the most significant factor affecting the both browning reaction and pyruvic acid content. Salt concentration had more influence to browning reaction than immersion time whereas immersion time was more impor-tant factor than salt concentration on a retention of pyruvic acid sugested different processing conditions. While the processing conditions to minimize the browning reaction(O.D=0.009) were 0.3% of salt solution 9 min of immersion time and 5$0^{\circ}C$ of air temperature compared to control(O.D=0.022) of air dehydration at 5$0^{\circ}C$ Pyruvic acid contents were maximized(174 $\mu$mole/g garlic solid) at the 0.1% of salt solution 3 min of immersion time and 5$0^{\circ}C$ of air temperature compared to control(147 $\mu$mole/g garlic solid) of air dehydration at 5$0^{\circ}C$

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