• Title/Summary/Keyword: salt bath

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Effects of Vacuum Heat Treatment and Salt bath Heat Treatment Conditions on Mechanical Properties of High Speed tool Steel (금속도 공구강의 기계적 성질에 미치는 진공열처리와 염욕열처리 조건의 영향)

  • Kim, Je-Don;Kim, Kyung-Sik
    • Journal of the Korean Society for Heat Treatment
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    • v.26 no.1
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    • pp.7-13
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    • 2013
  • Vacuum heat treatment(indirect heating method) has long exposure time at high temperature and low quenching rate. Contrarily salt bath heat treatment (direct heating method) has short exposure time at high temperature and fast cooling rate. With these different features of processes, mechanical properties such as hardness, tensile strength and impact strength of products show very different results. In this study, Salt bath heat treated products showed higher tensile strength and impact strength than vacuum heat treated products but hardness was not much different. These lower mechanical properties of vacuum heat treated products are due to differences in heat process and secondary hardening with high temperature tempering process. Consequently, It indicates that salt bath heat treatment is better way than vacuum heat treatment for product to have high mechanical properties.

The Surface Properties and Wear Resistance of Cr-Mo-V Steel by Salt bath Process after Pseudo-electrolysis (의(擬)전기분해식 염욕질화처리를 통한 Cr-Mo-V강의 내마모와 표면성질에 관한 연구)

  • Jung, Gil Bong;Yoon, Jae Hong;Hur, Sung Kang
    • Korean Journal of Metals and Materials
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    • v.48 no.3
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    • pp.225-234
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    • 2010
  • Salt bath nitriding, which has been developed recently by domestic company, is an emerging ecofriendly surface treatment. The salt bath nitriding is accompanied by the electrolysis process in the pretreatment step, and this whole processis called Pseudo-Electrolysised Salt bath Nitriding (PESN). The PESN creates only $NH_3$ and non-toxic salts without harmful $CN^{-}$ or toxic gas such as that found in previous salt bath nitriding. In general, ion nitriding and gas nitriding create high hardness and a strong brittle white layer on the surface. However, the PESN shows a thin white and gray layer. The PESN was applied to the defense material, 3%Cr-Mo-V steel, to study the surface characteristics at $480^{\circ}C$, $530^{\circ}C$, and $580^{\circ}C$ for 4 hrs, 20 hrs, 40 hrs, and 60 hrs of nitriding time condition. As a result, the best nitriding layer was found at $530^{\circ}C$ for 40 hrs. If we improve corrosion resistance and nitriding layer depth, the PESN will be able to be applied to the defense industry parts.

Effect of Vacuum Heat Treatment and Salt Bath Heat Treatment Conditions on Mechanical Properties of Hot Work Die Steel (열간 금형강의 기계적 성질에 미치는 진공열처리와 염욕열처리 조건의 영향)

  • Kim, Je-Don;Kim, Kyung-sik;Park, Ki-Ho
    • Design & Manufacturing
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    • v.8 no.2
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    • pp.23-29
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    • 2014
  • Salt bath heat treatment is usually used but recently vacuum heat treatment is increased for the heat treatment of hot work die steels. The differences in two heat treatment processes were compared by testing the mechanical properties of heat treated products. With two different features of processes, mechanical properties such as hardness, tensile strength and impact strength of products show very different results. In this study salt bath heat treated products showed higher tensile strength and impact strength than vacuum heat treated products but hardness was not much different. These lower mechanical properties of vacuum heat treated products are due to differences in heating and quenching process.

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A Study on Surface properties of Cr-Mo-V Steel by Eco-friendly Salt Bath Nitriding Treatment (Cr-Mo-V강의 친환경 염욕질화처리에 의한 표면특성 연구)

  • Jung, Gil-Bong
    • Journal of the Korea Institute of Military Science and Technology
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    • v.13 no.2
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    • pp.275-282
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    • 2010
  • The improved properties of surface layer can be achieved by so-called "new salt bath nitriding(NSBN)", which has been developed by a domestic company. This process based upon modified traditional salt bath nitriding process, increased hardenability with minimum toughness deterioration. This process also offers not only less white layer surfaces but also more eco-friendly one. That is, NSBN is the new eco-friendly surface treatment technology removing harmful $CN^-$ and toxic gas. According to the research of applying NSBN to Cr-Mo-V steel which has been used in defense industry, showed the improved result of wear resistance and surface hardening than non-coated condition. In further, we expect NSBN to curtail expenses and productivity improvement applied to the various defense industry parts.

Vibration Analysis of a Pulsator type Washing System (펄세이터형 세탁 시스템의 진동 해석)

  • 이신영;강주석;윤중락;이장무;윤구영;김남권
    • Journal of KSNVE
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    • v.7 no.2
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    • pp.261-272
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    • 1997
  • Recently washing machines are to be in lower vibration and lower sound because of better environment. Vibration problems in washing machines occur in both washing mode and spinning mode, but vibration in spinning mode becomes main problem because of its high rotating speed and continuity. Vibration while spinning is mainly due to rigid body motion of total washing system which includes suspending rods, washing bath, spinning bath, and gear sets. In this study, some researches were done in order to analyze the rigid body motion of washing system and flexible vibration of spinning bath. A basic mathematical model was established, and the effect of position of salt water and shape change of salt water case were considered. And the effect of lengths of suspending rods, attaching angles, vertical and horizontal position, stiffness of spring on the change of vibration were also considered. To identify the effect of salt water on vibration, some measurements were done. When salt water was positioned at upper part, the effect was most and this coincides with the tendency of simulation.

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A Study on the One Bath Two Step Dyeing of Nylon/ Cationized Cotton Blends with Acid Dye/Direct Dye (나일론/카티온화 면 혼방품의 산성염료/직접염료에 의한 1욕 2단 염색에 관한 연구)

  • 성우경
    • Textile Coloration and Finishing
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    • v.12 no.1
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    • pp.44-51
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    • 2000
  • The conventional one bath exhaust dyeing system of nylon]/cotton blends with acid dye/direct dye involves a lot of neutral salt which affect dyeability of acid dyes. Because of conventional one bath exhaust dyeing system of nylonl/cotton blends with acid dye/direct dye needs acid dyes adjusted at a neutral liquor, suitable acid dye is limited. To improve dyeing property of nylon/cotton blends, cotton component was pretreated with cationizing agent containing chlorohydrine group in aqueous solution of sodium hydroxide. This study was carried out to investigate dyeing possibilities of nylon/cationized cotton blends with acid dye/direct dye in a non-neutral salt dyebath by one bath two step method. The concentration of direct dye was 1.0%, 0.7%, 0.3%o.w.f. respectively at a non, 1%, 3%owf of reserving agent for being almost equal color strength between nylon and 3% cationized cotton when nylon/3% cationized cotton blends was dyed with acid dye/direct dye at concentration of acid dye(1%o.w.f.) by one bath two step method.

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Plasma Surface Treatment of Aluminum Extrusion Die (알루미늄 압출용 금형의 플라즈마 표면처리)

  • Choi, In Kyu;Lee, Su Young;Kim, Sang Ho
    • Journal of the Korean institute of surface engineering
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    • v.47 no.6
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    • pp.282-286
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    • 2014
  • Wear characteristic of the nitrided SKD61 which is a typical mold material using for the extrusion of Al6061 alloy was investigated. The surface of SKD61 was nitrided by salt bath and plasma processes. The thickness of surface nitride layer was about $8.9{\mu}m{\sim}21.3{\mu}m$. Reciprocating friction wear test conducted using pin on disk type indicated the plasma treatment followed salt bath has a lower friction coefficient and a smaller adhesive wear with Al6061 alloy. That was identified by the $Fe_4N$ which has a better wear resistance than FeN mainly formed by plasma nitriding.

Characterization of vanadium carbide coating deposited by borax salt bath process

  • Aghaie-Khafri, M.;Daemi, N.
    • Advances in materials Research
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    • v.1 no.3
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    • pp.233-243
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    • 2012
  • Thermal reactive diffusion coating of vanadium carbide on DIN 2714 steel substrate was performed in a molten borax bath at $950-1050^{\circ}C$. The coating formed on the surface of the substrate had uniform thickness ($1-12{\mu}m$) all over the surface and the coating layer was hard (2430-2700 HV), dense, smooth and compact. The influence of the kinetics parameters, temperature and time, has been investigated. Vanadium carbide coating was characterized by scanning electron microscopy (SEM), energy dispersive X-ray spectrometry (EDX) and X-ray diffraction analysis (XRD). The corrosion resistance of the coating was evaluated by potentiodynamic polarization in 3.5% NaCl solution. The results obtained showed that decrease of coating microhardness following increasing time and temperature is owing to the coarsening of carbides and coating grain size.

Heat Balance during the Electrowinning of Neodymium Metal in Molten Salt (네오디뮴 금속의 전해 채취 중의 열수지)

  • Cho, Sung-Wook;Yu, Jeong-Hyun;Choi, Ho-Gil
    • Resources Recycling
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    • v.31 no.3
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    • pp.81-87
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    • 2022
  • Energy consumption per unit weight of metal (kwh/kg of metal) is one of the most important economic indicators in the process of molten salt electrolysis. It is related to the heat loss of salt bath and the current efficiency of the process. The current efficiency is highly dependent on electrolysis temperature. On the other hand, the temperature of salt bath may increase significantly due to the difference (larger energy input than consumption) in heat balance at the beginning of electrolysis, which may cause different electrolysis temperature from an initially targeted value. This results in a bad effect on current efficiency. Therefore, it will be helpful to the reduction of energy consumption to compare the calculated and measured values of the temperature change of salt bath through the heat balance review at the early stage of electrolysis and to evaluate the energy loss to outside. In this study, based on the authors' experimental data, the heat balance was reviewed at the beginning of the electrolysis, and it was possible to evaluate the energy loss to the outside and the increase of the temperature of the salt bath quantitatively. Through such a method, heat loss reduction plan can be derived and current efficiency can be improved so that energy consumption can be reduced.

Studies on the One Bath Exhaust Dyeing System of Polyester/Cationized Cotton Blends with Disperse Dye/Reactive Dye (폴리에스테르/카티온화 면 혼방품의 분산염료/반응성염료에 의한 일욕염색계에 관한 연구)

  • 성우경
    • Textile Coloration and Finishing
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    • v.10 no.2
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    • pp.18-28
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    • 1998
  • in order to overcome disadvantage of the conventional two bath dyeing method of polyester/cotton blends, it had prompted significant effort to the development of the one bath dyeing method which can accomplish sayings in time, energy and water usage. Also, when dyeing polyester/cotton blends by the one bath dyeing method, the high salt concentrations needed for the reactive dye can cause particles of disperse dye, used for the polyester component, to aggregate. A supplementary problem that can occasionally be happened is the change of hue that occurs on dyed polyester in an alkaline dyebath. To improve dyeing property of polyester/cotton blends, cotton component was pretreated with epichlolohydrine-trimethylamine hydrochloride in aqueous solution of sodium hydroxide to produce a cationized cotton that can be dyed under neutral conditions with reactive dye in a non-electrolytic or il little electrolytic dyebath. The one bath dyeing method of polyester/cationized cotton blends with disperse dye/reactive dye mixture resulted in a satisfactory dyeing property and color yield in comparison with ordinary two bath dyeing method.

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