• Title/Summary/Keyword: rsm method

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Optimizing Nitrobenzene Synthesis Catalyzed by Sulfated Silica (SO4/SiO2) through Response Surface Methodological Approach

  • Aan Sabilladin;Aldino Javier Saviola;Karna Wijaya;Aulia Sukma Hutama;Mokhammad Fajar Pradipta;Wahyu Dita Saputri;Hilda Ismail;Budhijanto Budhijanto;Won-Chun Oh;Balasubramani Ravindran
    • Korean Journal of Materials Research
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    • v.34 no.7
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    • pp.341-354
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    • 2024
  • Today, the principles of green chemistry are being fundamentally applied in the chemical industry, such as the nitrobenzene industry, which is an essential intermediate for various commercial products. Research on the application of response surface methodology (RSM) to optimize nitrobenzene synthesis was conducted using a sulfated silica (SO4/SiO2) catalyst and batch microwave reactor. The nitrobenzene synthesis process was carried out according to RSM using a central composite design (CCD) design for three independent variables, consisting of sulfuric acid concentration on the silica (%), stirring time (min), and reaction temperature (℃), and the response variable of nitrobenzene yield (%). The results showed that a three-factorial design using the response surface method could determine the optimum conditions for obtaining nitrobenzene products in a batch microwave reactor. The optimum condition for a nitrobenzene yield of 63.38 % can be obtained at a sulfuric acid concentration on the silica of 91.20 %, stirring time of 140.45 min, and reaction temperature of 58.14 ℃. From the 20 experiments conducted, the SO4/SiO2 catalyst showed a selectivity of 100 %, which means that this solid acid catalyst can potentially work well in converting benzene to nitrobenzene.

Optimal Design of Impeller Shroud for Centrifugal Compressor Using Response Surface Method (반응표면법을 이용한 원심압축기 임펠러 쉬라우드 형상최적설계)

  • Kang, Hyun-Su;Hwang, In-Ju;Kim, Youn-Jea
    • The KSFM Journal of Fluid Machinery
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    • v.18 no.4
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    • pp.43-48
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    • 2015
  • In this study, a method for optimal design of impeller shroud for centrifugal compressor using response surface method (RSM) and multi-objective genetic algorithm (MOGA) was studied. Numerical simulation was conducted using ANSYS CFX with various configurations of shroud. Each of the design parameters was divided into 3 levels. Total 15 design points were planned by central composite design (CCD) method, which is one of the design of experiment (DOE) techniques. Response surfaces based on the results of DOE were used to find the optimal shape of impeller shroud for high aerodynamic performance. The whole process of optimization was conducted using ANSYS Design Xplorer (DX). Results showed that the isentropic efficiency, which is the main performance parameter of the centrifugal compressor, was increased 0.4% through the optimization.

Development of Ride Comfort Measuring System for Railway with Multi-function (다기능성을 갖는 철도 차량용 승차감 측정시스템 개발)

  • Kim, Young-Guk;Kim, Seog-Won;Park, Chan-Kyeong;Kim, Ki-Hwan;Park, Tae-Won
    • Journal of Sensor Science and Technology
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    • v.13 no.5
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    • pp.369-377
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    • 2004
  • Recently, the "ride comfort" problem becomes increasingly important because of today's needs for train speedup. The concept of term "ride comfort" is equivocal. Generally it is defined as the vehicle vibration. There are many studies on evaluation method of ride comfort for railway. But each of them recommends the different assessment method and the different guidance. In general, the evaluation methods defined in the standards, such as ISO 2631 and UIC 513R, and Ride Index suggested by Sperling, have been used in the railroad. But, only one or two methods of these can be evaluated by using the commercial ride comfort measuring system. Therefore, it is necessary to develop the new ride comfort measuring system for railway with multi-function. In this paper, the generalization of "ride comfort" and the design and verification of new ride comfort measuring system for railway with multi-function have been described and the application examples has been introduced.

반응면 기법을 이용한 에어포일 공력형상 최적설계

  • Park, Young-Min;Kim, Yu-Shin;Chung, Jin-Deog;Lee, Jang-Yeon
    • Aerospace Engineering and Technology
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    • v.3 no.2
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    • pp.248-255
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    • 2004
  • In this study, aerodynamic shape design of airfoils was performed by using RSM(response surface method) and two-dimensional Navier-Stokes solver. Numerical experiment points were determined by D-optimal method and quadratic response surfaces were constructed by using JMP. For the validations of design method, NACA 64621 airfoil was inversely designed to have aerodynamic characteristics of Bell airfoil. The design method was applied to the aerodynamic design of both smart UAV wing airfoil and low Reynolds rotor-blade airfoil for unmanned helicopter. The optimized airfoils showed improved performance with various constraint conditions.

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Trade-off Analysis in Multi-objective Optimization Using Chebyshev Orthogonal Polynomials

  • Baek Seok-Heum;Cho Seok-Swoo;Kim Hyun-Su;Joo Won-Sik
    • Journal of Mechanical Science and Technology
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    • v.20 no.3
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    • pp.366-375
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    • 2006
  • In this paper, it is intended to introduce a method to solve multi-objective optimization problems and to evaluate its performance. In order to verify the performance of this method it is applied for a vertical roller mill for Portland cement. A design process is defined with the compromise decision support problem concept and a design process consists of two steps: the design of experiments and mathematical programming. In this process, a designer decides an object that the objective function is going to pursuit and a non-linear optimization is performed composing objective constraints with practical constraints. In this method, response surfaces are used to model objectives (stress, deflection and weight) and the optimization is performed for each of the objectives while handling the remaining ones as constraints. The response surfaces are constructed using orthogonal polynomials, and orthogonal array as design of experiment, with analysis of variance for variable selection. In addition, it establishes the relative influence of the design variables in the objectives variability. The constrained optimization problems are solved using sequential quadratic programming. From the results, it is found that the method in this paper is a very effective and powerful for the multi-objective optimization of various practical design problems. It provides, moreover, a reference of design to judge the amount of excess or shortage from the final object.

Optimizing In Vitro Propagation of Sophora koreensis Nakai using Statistical Analysis (다양한 통계분석 기법을 이용한 개느삼(Sophora koreensis Nakai)의 기내 증식 최적 조건 구명)

  • Jeong, Ukhan;Lee, Hwa;Park, Sanghee;Cheong, Eun Ju
    • Journal of Korean Society of Forest Science
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    • v.110 no.1
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    • pp.53-63
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    • 2021
  • Sophora koreensis Nakai is an indigenous plant in Koreawith a restricted natural range, part of which is in Gangwon province. The species is known to contain phytochemicals that have beneficial effects on human health, and it is economically important in bioindustry. Because of the limited number of plants in a small range of habitats, the mass-propagation method should be developed for use and conservation. In vitro tissue culture is a reliable method in terms of mass propagation from selected clones of the species. We investigated the optimal conditions of the medium in this process, especially focusing on the concentrations of plant growth regulators(PGRs) in the culture of stem-containing axillary buds. Three statistical methods, i.e., ANOVA, response surface method(RSM), and fuzzy clustering were used to analyze the plant growth, number of shoots induced, and shoot length with various combinations of PGRs. Results from the RSM differed from those of the other two methods; thus, the method was not suitable. ANOVA and fuzzy clustering showed similar results. However, more accurate results were obtained using fuzzy clustering because it provided a probability for each treatment. On the basis of the fuzzy clustering analysis, stem tissue produced the greatest number of shoots(11.03 per explant; 63.33%) on a medium supplemented with 5-��M 6-benzylaminopurine and 2.5-��M thidiazuron(TDZ). Proliferation of shoots(2.18 ± 0.21 cm, 63.33%) was attained on a medium supplemented with 2.5-��M BA, 2.5-��M TDZ, and 2.5-��M gibberellic acid.

Statistical Optimization for Production of Carboxymethylcellulase from Rice Hulls by a Newly Isolated Marine Microorganism Bacillus licheniformis LBH-52 Using Response Surface Method (통계학적인 방법과 왕겨를 기질로 사용하여 해양에서 분리한 Bacillus licheniformis LBH-52 를 사용한 carboxymethylcellualse의 생산조건 최적화)

  • Kim, Hye-Jin;Gao, Wa;Chung, Chung-Han;Lee, Jin-Woo
    • Journal of Life Science
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    • v.21 no.8
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    • pp.1083-1093
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    • 2011
  • A microorganism utilizing rice hulls as a substrate for the production of carboxymethylcellulase (CMCase) was isolated from seawater and identified as Bacillus lincheniformis by analyses of its 16S rDNA sequences. The optimal carbon and nitrogen sources for production of CMCase were found to be rice hulls and ammonium nitrate. The optimal conditions for cell growth and the production of CMCase by B. lincheniformis LBH-52 were investigated using the response surface method (RSM). The analysis of variance (ANOVA) of results from central composite design (CCD) indicated that a highly significant factor ("probe>F" less than 0.0001) for cell growth was rice hulls, whereas those for production of CMCase were rice hulls and initial pH of the medium. The optimal conditions of rice hulls, ammonium nitrate, initial pH, and temperature for cell growth extracted by Design Expert Software were 48.7 g/l, 1.8 g/l, 6.6, and 35.7$^{\circ}C$, respectively, whereas those for the production of CMCase were 43.2 g/l, 1.1 g/l, 6.8, and 35.7$^{\circ}C$. The maximal production of CMCase by B. lincheniformis LBH-52 from rice hulls under optimized conditions was 79.6 U/ml in a 7 l bioreactor. In this study, rice hulls and ammonium nitrate were developed to be substrates for the production of CMCase by a newly isolated marine microorganism, and the time for production of CMCase was reduced to 3 days using a bacterial strain with submerged fermentation.

Design of Brushless Permanent Machine with Skewed Stator for Electrical Power Steering System (전동 조향 장치용 브러쉬리스 영구자석 전동기의 스테이터 스큐 설계)

  • Lee, Choong-Sung;Jung, Kyung-Tae;Hong, Jung-Pyo;Kim, Hae-Joong;Kim, Young-Kyun
    • Journal of the Korean Magnetics Society
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    • v.25 no.6
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    • pp.189-197
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    • 2015
  • As enforced the regulation of fuel efficiency, the electrification of automotive components in internal combustion vehicle has been applied instead of hydraulic pressure. A typical example of such parts is the EPS (electric power steering), and it is applied to most automotive at present. In electric power steering system, the core component is motor. The reduction of cogging torque and torque ripple is required to improve steering feeling and reduce NVH (Noise Vibration Harshness) in EPS. Generally the skewed design of stator or rotor is applied in order to reduce cogging torque and torque ripple. This paper propose the design and analysis methodology of Brusheless PMSM (Permanent Magnet Synchronous Motor) which is applied to skewed stator. The proposed methodology is as follows: First Intial Design PMSM with skewed stator for EPS, Second Optimal design using RSM (Response surface method), Third Performance Analysis such as Phase Back EMF, Inductance, Load torque using FEA (Finite Element Method). Finally, the reliability of proposed design methodology will be verified through the experiments of prototype sample.

A Study on the Development and the Verification of Engineering Structure Design Framework based on Neuro-Response Surface Method (NRSM) (신경반응표면을 이용한 공학 구조물 설계 프레임워크 구축 및 검증에 관한 연구)

  • Lee, Jae-Chul;Shin, Sung-Chul;Kim, Soo-Young
    • Journal of the Korean Institute of Intelligent Systems
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    • v.24 no.1
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    • pp.46-51
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    • 2014
  • The most important process of engineering system optimal design is to identify the relationship between the design variables and system response. In case of the system optimization, Response Surface Method (RSM) is widely used. The optimization process of RSM generates the design space using the typical alternative candidates and finds the optimal design point in the generated design space. By changing the optimal point depending on the configuration of the design space, it is important to generate the design space. Therefor in this study, the design space is generated by using the relationship between design variables and system response based on Neuro-Response Surface Method (NRSM). And I try to construct the framework for optimal shape design based on NRSM that the optimum shape can be predicted using the Non-dominated Sorting Genetic Algorithm-II (NSGA-II) within the generated design space. In order to verify the usefulness of the constructed framework, we applied the nonlinear mathematical function problem. In this study, we can solve the constraints of time in the optimization process for the engineering problem and effective to determine the optimal design was possible. by using the generated framework for optimal shape design based on NRSM. In the future research, we try to apply the optimization problem for Naval Architectural & Ocean Engineering based on the results of this study.

Quantitative Deterioration and Maintenance Profiles of Typical Steel Bridges based on Response Surface Method (응답면 기법을 이용한 강교의 열화 및 보수보강 정량화 이력 모델)

  • Park, Seung-Hyun;Park, Kyung Hoon;Kim, Hee Joong;Kong, Jung-Sik
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.28 no.6A
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    • pp.765-778
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    • 2008
  • Performance Profiles are essential to predict the performance variation over time for the bridge management system (BMS) based on risk management. In general, condition profiles based on experts opinion and/or visual inspection records have been used widely because obtaining profiles based on real performance is not easy. However, those condition profiles usually don't give a good consistency to the safety of bridges, causing practical problems for the effective bridge management. The accuracy of performance evaluation is directly related to the accuracy of BMS. The reliability of the evaluation is important to produce the optimal solution for distributing maintenance budget reasonably. However, conventional methods of bridge assessment are not suitable for a more sophisticated decision making procedure. In this study, a method to compute quantitative performance profiles has been proposed to overcome the limitations of those conventional models. In Bridge Management Systems, the main role of performance profiles is to compute and predict the performance of bridges subject to lifetime activities with uncertainty. Therefore, the computation time for obtaining an optimal maintenance scenario is closely related to the efficiency of the performance profile. In this study, the Response Surface Method (RSM) based on independent and important design variables is developed for the rapid computation. Steel box bridges have been investigated because the number of independent design variables can be reduced significantly due to the high dependency between design variables.