• 한국분말재료학회지
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• 제25권2호
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• pp.126-131
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• 2018

In the present study, we investigate the effects of milling time and the addition of a process control agent (PCA) on the austenite stability of a nanocrystalline Fe-7%Mn alloy by XRD analysis and micrograph observation. Nanocrystalline Fe-7%Mn alloys samples are successfully fabricated by spark plasma sintering. The crystallite size of ball-milled powder and the volume fraction of austenite in the sintered sample are calculated using XRD analysis. Changes in the shape and structure of alloyed powder according to milling conditions are observed through FE-SEM. It is found that the crystallite size is reduced with increasing milling time and amount of PCA addition due to the variation in the balance between the cold-welding and fracturing processes. As a result, the austenite stability increased, resulting in an exceptionally high volume fraction of austenite retained at room temperature.

• 한국해양공학회지
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• 제2권2호
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• pp.87-95
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• 1988

This paper is studied to know corrowive wear characteristics of austempered ductile cast ironin corrosive environments against mating SM45C hardened two test pieces in distilled water and NaCl aqueous solution. The corrosive wear mechanism was investigated by scanning electron microscopy and retained austenite volume fraction was investigated by X-ray diffractometer. The experimental result show that the corrosive wear characteristics depend largely on the $\textrm{Fe(OH)}_{3}$which is influenced by the critical sliding distance $L_{cr}$ and $L_{cr}$ shorted with increasing NaCl concentration. It was found that the carbides in matrix have a significant effect on their corrosive wear resisance and the fine acicular bainite showed corrosive wear resistance stronger than that of the coarse acicular and platelet bainite. From above results the model of corrosive wear mechanism in corrosive environments is proposed.

• 한국식품영양과학회지
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• 제26권6호
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• pp.1013-1020
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• 1997

To elicit the effect of fermentation on food quality of the watery Chinese cabbage pickles without fish sauce and red pepper paste(Baik-kimchi), changes in physicochemical properties and microstructure of fiber components were studied. Better water holding capacity(WHC) was showed in Baik-kimchi fermented at $25^{\circ}C$ than that of Baik-kimchi fermented at 5$^{\circ}C$. WHC measured at pH 2 and 6 were ranged from 10.18 to 16.79g/g dried sample for Baik-kimchi fermented at $25^{\circ}C$ and 6.51~14.58g/g dried sample for sample for samples at 5$^{\circ}C$, respectively. The higher WHC was resulted in pH controlled freeze-dried sample to pH 6 than that measured in pH 2 sample. The settling volume(SV) and oil adsorption capacity(OAC) increased with fermentation period and kept the same value for a little while, but slightly decreased in the over ripening period. Baik-kimchi fermented at $25^{\circ}C$ exhibited more shrunk microstructure of parenchyma cell and xylem than those of Baik-kimchi fermented at 5$^{\circ}C$. The appearance of SDF of the both Baik-kimchi ripened at 5$^{\circ}C$ and $25^{\circ}C$ could give granular shape, whereas the overripened Baik-kimchi had smooth surface of SDF. On the other hand, the IDF retained the original shape during fermentation.

• 대한금속재료학회지
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• 제47권3호
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• pp.169-174
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• 2009

The effect of sub zero treatment on the damping capacity in austempered ductile cast iron investigated. Austenite transformed in to martensite by subzero treatment, and with the decrease of subzero treatment temperature, volume fraction of martensite increased. Damping capacity of austempered ductile cast iron was highly increased by subzero treatment, with the decrease of subzero treatment temperature, damping capacity was slowly increased. With the decrease of subzero treatment time, damping capacity was rapidly increased to 30 min. and then slowly increased. With the increase of volume fraction of martensite, damping capacity rapidly increasing to 5% and then slowly increased.

• Journal of Advanced Marine Engineering and Technology
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• 제21권5호
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• pp.512-521
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• 1997

This paper deals with an evaluation of the residual stress due to shot peening induced in a car¬burized gear tooth and its application to the fatigue crack propagation problem. The residual stress is estimated based on the assumption that the main cause of residual stress is the volume difference between the case and core due to martensitic transformation in cooling, and the influ¬ence of both the reduction of retained austenite and the strain in the surface layer induced by shot peening are considered. The reliability of the method is examined by comparison with stresses measured by the X-ray diffraction method. The stresses intensity factors are computed by the influence function method and the reduction of the factor due to the residual stress is demonstrat¬ed and discussed based on the fracture mechanics.

• 한국안전학회지
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• 제12권3호
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• pp.30-37
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• 1997

This paper deals with the residual stress of carburized spur gears is calculated being on the assumption that the main cause of residual stress is the volume difference between case and core due to the martensitic transformation in cooling. A formula is proposed to estimated the residual stress from the hardness and the amount of retained austenite. The estimated residual stress is close to the stress measured by X-ray method. The estimated residual stress is applied to the analysis of the fracture mechanics of carburized spur gear teeth. The stress intensity factor due to the residual stress is demonstrated. The stress intensity factor is computed by the influence function method, and it is shown that the factor is decreased by the residual stress in Carburized gear tooth.

• 열처리공학회지
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• 제8권4호
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• pp.279-288
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• 1995

To investigate the characteristics of nitrocarburizing for high carbon chromium bearing steel, it was undertaken 4 hours holding at $850^{\circ}C$ in the atmosphere containing 60% endothermic gas and 40% ammonia. The microstructure of nitrocarburized surface consists of ${\varepsilon}-Fe_{2-3}N$, ${\gamma}^{\prime}-Fe_4N$, $Fe_3C$ and $Fe_3$(C,N), and the ${\varepsilon}$-nitride was rich in the surface-internal part. The nitrocarburized surface contains a larger volume fraction of primary carbonitrides and has more retained austenite and is slightly harder than the interior.

• 대한기계학회논문집
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• 제18권12호
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• pp.3227-3235
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• 1994

This paper deals with an evaluation of the residual stress due to shot peening induced in a carburized gear tooth and its application to the fatigue crack propagation problem. A practical method is proposed on the basis of the assumption that the residual stress is caused by the difference of volume expansion in the case and the core, and the influence of both the reduction of retained austenite and the strain due to shot peening are considered. The evaluated residual stress is close to the measured stress, though the surface stress is rather overestimated. The stress intensity factor is computed by the influence function method, and it is shown that the factor is decreased by the residual stress in shot peened gear tooth. The shot peening is fairly effective to the reduction of fatigue crack growth rate. The crack propagation is simulated and the resistance due to shot peening is quantitatively demonstrated and discussed.

• 한국해양학회지
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• 제3권2호
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• pp.47-54
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• 1968

Monthly mean values for EDTA hardness in the Han River water were determined for March 1966 through May 1967. The hardness was retained a range of 22-59 mg/L the maximum value of 59 mg/L was approached in the months of mid-winter, indicating a seasonal variation. The annual ranges of Ca and Mg were 3.7-9.1 mg/L, 1.5-10.4 mg/L, respectively. The annual range of Mg:Ca ratio was 0.18-2.60. And the hardness correlated closely with Mg volume. In Korea, fortunately, most river waters are not yet suffering from damaging pollution. We must try to establish our water quality criteria based on scientific data, and make research recommendations for the following water uses; public water supplies, aquatic life and wildlife, industry, recreation and aesthetics.

• Journal of Magnetics
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• 제20권1호
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• pp.21-25
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• 2015

Fine Nd-Fe-B-type particles were prepared by ball milling of different types of Nd-Fe-B precursor materials, such as die-upset magnet, HDDR-treated material, and sintered magnets. Coercivity dependence on the grain and particle size of the powder was investigated. Coercivity of the milled particles was reduced as the particle size decreased, and the extent of coercivity loss was dependent upon the precursor material. Coercivity loss in the finely milled particles was attributed to the surface oxidation. The extent of coercivity loss in the fine particles was closely linked to grain size of the precursor materials. Coercivity loss was more profound for the fine particles with larger grain size. Contrary to the fine particles from the sintered magnets with larger grain size the fine particles (~10 um) from the die-upset magnet and HDDR-treated material with much finer grain size still retained high coercivity (> 10 kOe for die-upset magnet, > 4 kOe for HDDR-treated material).