• The Journal of Korean Academy of Prosthodontics
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• v.34 no.2
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• pp.266-276
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• 1996

Numerous factors are known to affect the accuracy of elastomeric impression materials. Factor often overlooked is the quality of the bond between putty and wash during corrective reline impression technique. The putty-wash bond strength must be strong enough to over-come the local stress at putty-wash interface. It is not always possible to avoid saliva contamination in making corrective wash impres-sion. And putty preliminary impression material con be used as a template for provisional restoration. Human saliva and the residual monomer of autopolymerizing acrylic resin are thought to affect the bond strength and the failure type. This study examined the effect of contaminants like human saliva, and residual resin monomer on the putty-wash bond strength and the effectiveness of treatment. 1. Of the tested three brands of Vinyl Polysiloxane impession meterial, Express Exhibited the greatest bond strength followed by Eamix and Perfect showed the lowest putty-wah bond strength. 2. Coating the putty substrates with human saliva did not produce decreased failure load in all the breands of Vinyl Polysiloxane impression meterail. 3. Of the three brands of VPS impression material that were exposed to methhylmethacry-late resin(Jet), only the putty-wash bond strength of the Perfect group diminished signifi-cantly. Moreover, all the specimens from group C of Perfect exhibited adhesive failure. 4. Exposing the substrates to ethylmethacrylate resin(SNAP. diminished the putty-wash bond strength significantly. With Perfect and Examix, failure occurred cohesively through the light-body, whereas with Express, failure occurred adhesive-cohesively. 5. Removing approximately 1mm thickness of the contaminated putty interface was the most effective treatment in countering the undesirable effect caused by residual resin monomer. The putty-wash bond strength of the groups that were treated with 1mm even putty reduction was not significantly different from those of control groups. With Perfect and Examix, cleaning the specimens with gauze soaked in 70% isopropyl alcohol increased the putty-wash bond strength, but was not as effective as 1mm even reduction of contaminated putty substrates. With Express, 70% isoproryl alcohol treatment exhibi0ted comparable putty-wash bond strength to that of control group.

• Journal of Dental Rehabilitation and Applied Science
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• v.34 no.2
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• pp.89-96
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• 2018

Purpose: The aim of this study was to evaluate the effect of delayed time, surface treatment, and repair materials on repair of bis-acryl composite resin through comparison of shear bond strength and to evaluate the utility of bis-acryl composite resin repair using polymethyl methacrylate resin. Materials and Methods: A total of 90 bis-acryl composite resin specimens were fabricated and classified into 9 test groups, each of 10 pieces according to delayed time, surface treatment and repair material. The shear bond strength of each specimen was measured using a universal testing machine immediately after fabrication and analyzed using a statistical analysis program (IBM SPSS statistics 20). After the shear bond strength measurement, the fracture surface of the specimen was observed. Results: The highest shear bond strength ($17.54{\pm}3.14MPa$) was observed in the experimental group bonded immediately with a light-curing flowable composite resin using a bonding agent. Conclusion: When repairing bis-acryl composite resin, it is necessary to consider whether to remake according to the delayed time. For effective repair, it is desirable to consider appropriate materials and surface treatment methods according to the site or purpose of use.

• Journal of the Mineralogical Society of Korea
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• v.21 no.2
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• pp.183-192
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• 2008

Stone cultural heritages in Korea are mostly situated out door without any notable protection thus there are severe damage from chemical and biological weathering. This in turn, causes deformation and structural damage. To counter act this problem and to increase durability, various kinds of conservation materials are used in the conservation and restoration treatment. However, there are not many practical and technological experiment done on this subject. This paper attempts quantitative evaluation of effectiveness of ethylsilicate based resin for Namsan granite in Gyeongju. When two different materials with different ethylsilicate concentration were compared, the result indicated decrease of absorption and porosity with increase of ultrasonic velocities, uniaxial compressive strength, elastic constant, tensile strength and Poisson's ratio. In addition, comparison of physical characteristic of the conservation material resulted favorably toward ones with higher concentration of ethylsilicate. This is due to the ethylsilicates characteristic to fill the internal pores of stone. There is discolouration of stone surface after treatment with conservation material. This was more prominent with the product of higher ethylsilicate concentration.

• Journal of Conservation Science
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• v.20
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• pp.67-80
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• 2007

Icheon Seolbong fortress is located in Saum-dong, Icheon, Gyeonggi-do Province that its date is founded as 4th century of Bakjae dynasty after excavation by Dankook university museum. Excavated artifacts show various kinds such as earthenwares, ceramics, metal artifacts and so on. Especially many iron artifacts were founded in where Bakjae earthenwares were found that it indicates iron artifacts were manufactured in Bakjae Dynasty. From 6 iron sickles, called Beollat and Millet, samples were taken to examine mircostructures and from the results used iron material, shape-forging, steel-making process, heat treatment were investigated. From this late 4th century Bakjae dynasty iron manufacture profess was established. From the result, different treatment were used in different area of the sickles according to the its use. Beollats were quenched in blade and it was used for special purpose that require Intensity. Millats did not have special treatment that it was used to cut rice plant and plant. Used material was steel, steel was previously made by certain steel-making process. It is formed to produce iron ware and the area where intensity is required heat treatment was employed to make it strong. From the investigation it is derived that iron ware manufacture process in Bakjae dynasty is steel making$\rightarrow$shape-forging$\rightarrow$and heat treatment.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.21 no.2
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• pp.175-181
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• 2020

This paper suggests a proper hydraulic filling method in downtown areas. Road subsidence on roadways and sidewalks in downtown areas can result in vehicle damage and casualties. The representative cause of road subsidence is the fraudulent construction in nearby construction sites. A deficiency of excavation restoration causes approximately 25~49% of subsidence. This is performed by equipment or manpower. Hydraulic filling is used in backfilling narrow pipe conduits and spaces between structures. On the other hand, standard specifications and quality assurance standards regarding hydraulic filling principles and construction conditions are insufficient. Therefore, in-door model experiments on hydraulic filling principles, backfilling material, and compaction efficiency were performed. This paper suggests guidelines by investigating and analyzing construction status. In conclusion, thrown backfilling material has a particle size distribution and permeability coefficient as major factors, and detailed standards of the factors are suggested. To improve the compaction efficiency, 90% or more, compaction by the floor should be in units of 0.3m while ensuring a lower drainage layer. When an H-shape stabilizing pile is pulled out after filling, additional hydraulic filling should be in the disturbance range.

• Analytical Science and Technology
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• v.31 no.2
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• pp.78-87
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• 2018

Asian lacquer has been used as an adhesive and coating material in Asian countries, such as China, Japan, and Korea, and other southeast Asian countries. In this study, the changes in the chemical structure of lacquer with drying was analyzed using pyrolysis/GC/MS (which is useful in analyzing polymeric material) to understand its drying procedures. Upon increasing temperature, the dried lacquer was fully pyrolyzed above the pyrolysis temperature of $500^{\circ}C$. The repeatability was good at the pyrolysis temperature of $500^{\circ}C$ (rsd = 2.6-22.3 %); however, there were differences in the pyrogram patterns when the difference in sample quantity was large. The characteristic peaks of Asian lacquer components, such as those corresponding to 1,2-benzenediol and 3-methyl-1,2-benzenediol, were detected and the compound of each peak was assigned according to the mass library. As the lacquer dried, the composition of pyrolysis products with urushiol derivatives bearing 3 C=C bonds was severely reduced compared with the ones with no C=C bonds, indicating that the polymerization is related to C=C bonds. These results can be applied to confirm the presence of lacquer in excavated relics and to monitor the changes in the composition of raw lacquer with drying.

• Journal of the Korean Academy of Esthetic Dentistry
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• v.22 no.1
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• pp.22-29
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• 2013

In general, to conduct aesthetic restorations, various analyses are carried out using a camera from the initial examination with the final prosthesis in consideration. With the reality that many dentists are using digital cameras, it can be considered that the time of digital impression has already started. Just as the recent general trend is that more and more internationally renowned photographers are switching their film cameras to digital counterparts, it is likely that CAD/CAM will show another direction in the area of the aesthetic dentistry that we may want to pursue. With the word 'digital', the convenience and economics often come to mind in the first place. However, from the dental clinical viewpoint, it is important to improve and develop the CAD/CAM system based on understanding its specialty and superiority while respecting the conventional analog techniques. However, a regretful aspect is that it is often difficult to catch up with the latest advancements for proper referencing and follow-up of digital technologies since the CAD/CAM device and material are developing very rapidly. Accordingly, although it is ideal to have hands-on experiences in various digital material and devices, and adapt to their fast changes, it must be stressed that the clinical application is to be implemented on the basis of the proven traditional way of dental clinics in order to obtain better outcomes. This presentation will explore types of approaches that can be made by combining the traditional techniques and the CAD/CAM from the aesthetic viewpoint. In addition, it is hoped and eagerly awaited that the CAD/CAM restoration may play a significant role in the field of the 'digital art'.

• Journal of the korean academy of Pediatric Dentistry
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• v.38 no.3
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• pp.229-236
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• 2011

ProRoot MTA(Dentsply Tulsa, U.S.A) which has similar component with Portland cement has setting expansion character and long setting time. Excessive expansion can cause fracture at the apical portion of the root and decreasing of volume stability. And the long setting time makes additional visits for crown restoration and slow setting process of this material can change physical properties itself. In this study, among requirements of root canal filling material(KS P ISO 6876) which is revised at 2008, we investigated the setting time and setting expansion. Objects are recently developed OrthoMTA(BioMTA, Korea), conventional ProRoot white MTA(Dentsply Tulsa, U.S.A) and White portland cement(Union, Korea). The results in setting expansion, OrthoMTA was $0.08{\pm}0.02%$, ProRoot white MTA and White portland cement were each $0.28{\pm}0.06$, $0.80{\pm}0.25%$(p<0.05). The results in setting time, OrthoMTA, ProRoot white MTA, White portland cement were each $307.78{\pm}3.83$ min, $150.44{\pm}2.35$ min, $235.33{\pm}9.07$ min(p<0.05).

• Journal of Conservation Science
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• v.32 no.1
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• pp.21-32
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• 2016

Animal glue is a traditional material used extensively as adhesive and binder in mother-of-pearl, wooden structure, traditional painting, etc. Analysis of animal glue is usually performed with IR(infrared spectroscopy) based on the IR absorption of functional group. But, it has a limitation in confirming animal glue when a sample consists of several materials because of overlapping of the absorption band. Py/GC/MS(pyrolysis/gas chromatography/mass spectrometry) is a useful tool in analyzing the constituent of polymeric materials like animal glue by identifying their pyrolysate with very small amount of sample. In this study, confirmation of animal glue in a Dancheong sample was tried with this method. Characteristic pyrolytic compounds of animal glue and tung oil used in Dancheong were identified. Dancheong sample painted with Noerok as a coloring material, animal glue and tung oil was prepared and it was possible to find characteristic peaks of animal glue after thermal degradation and artificial weathering experiment. From this, we found that animal glue can be detected using py/GC/MS in cultural heritage samples consisting of several materials and in different condition. IR was also tried to analyze Dancheong sample and the results were compared with those of py/GC/MS for the detection of animal glue.

• Journal of the korean academy of Pediatric Dentistry
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• v.31 no.2
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• pp.153-158
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• 2004

Preformed stainless steel crown is an useful restorative material for the treatment of badly broken down primary teeth. However iatrogenic damage to adjacent teeth might occur during the process of tooth reduction. Such damages might lead to plaque accumulation and increase the risks of caries initiation. Especially the damage can make a problem in the first permanent molar. Purpose of this study was to investigate an iatrogenic damage to the first permanent molar during preparation of second primary molar for preformed stainless steel crown. Twelve children restored with preformed stainless steel crown to second primary molar were selected. Contact areas were separated with separation elastics, and tooth surfaces were cleaned. After taking negative impression using vinylpolysiloxane impression material, the specimens were examined by scanning electron microscope for the detection of iatrogenic damage. The prevalence of iatrogenic damage was 66.7% and variable appearances and So we can suggest that when preparing teeth for preformed stainless steel crown, we should be careful about adjacent teeth not to make an iatrogenic damage.