• Title/Summary/Keyword: residual carbon

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$\beta$-SiC Formation Mechanisms in Si Melt-C-SiC System (용융 Si-C-SiC계에서 $\beta$-SiC 생성기구)

  • 서기식;박상환;송휴섭
    • Journal of the Korean Ceramic Society
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    • v.36 no.6
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    • pp.655-661
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    • 1999
  • ${\beta}$-SiC formation mechanism in Si melt-C-SiC system with varying in size of carbon source was investigated. A continuous reaction sintering process using Si melt infiltration method was adopted to control the reaction sintering time effectively. It was found that ${\beta}$-SiC formation mechanism in Si melt-C-SiC system was directly affected by the size of carbon source. In the Si melt-C-SiC system with large carbon source ${\beta}$-SiC formation mechanism could be divided into two stages depending on the reaction sintering time: in early stage of reaction sintering carbon dissolution in Si melt and precipitation of ${\beta}$-SiC was occurred preferentially and then SIC nucleation and growth was controlled by diffusion of carbon throughy the ${\beta}$-SiC layer formed on graphite particle. Furthmore a dissolution rate of graphite particles in Si melt could be accelerated by the infiltration of Si melt through basal plane of graphite crystalline.

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A binder system for low carbon residue and debinding behaviors in injection molding of NdFeB powder (NbFeB 분말사출성형에소 저잔류탄소를 위한 결합제 및 탈지거동)

  • 최준환
    • Journal of Powder Materials
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    • v.6 no.2
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    • pp.132-138
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    • 1999
  • A new binder system and debinding process for low carbon residue in the injection molding of Nd(Fe, Co)B powder are investigated. In the injection molding of magnetic materials, it is demanded to reduce carbon residue which deteriorates their magnetic properties. The binder system developed is composed of polyethylene glycols (PEGs) and polypropylene (PP). PEG was selected as a major binder is component to be extracted in a molecular state by solvent extraction in ethanol, which step would leave no residue. PP was selected as a minor binder component to be subsequently removed by thermolysis which step would leave carbon residue. The behaviors of solvent extraction with the variations of PEG molecular weight, temperature, and time were examined. The dependency of residual carbon content on thermolysis atmosphere was also studied. Opened pore channels introduced in a green body by the solvent extraction and microstructures of the sintered magnets were observed using SEM.

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Evaluation of Variation in Residual Strength of Carbon Fiber Reinforced Plastic Plate with a Hole Subjected to Fatigue Load (피로하중에 의한 홀 노치 탄소섬유강화 복합재의 잔류강도변화 평가)

  • Kim, Sang-Young;Kang, Min-Sung;Koo, Jae-Mean;Seok, Chang-Sung
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.34 no.10
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    • pp.1411-1417
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    • 2010
  • CFRP (Carbon Fiber Reinforced Plastic) has received considerable attention in various fields as a structural material, because of its high specific strength, high specific stiffness, excellent design flexibility, favorable chemical properties, etc. Most products consisting of several parts are generally assembled by mechanical joining methods (using rivets, bolts, pins, etc.). Holes must be drilled in the parts to be joined, and the strength of the components subjected to static and fatigue loads caused by stress concentration must be decreased. In this study, we experimentally evaluated the variation in the residual strength of a holenotched CFRP plate subjected to fatigue load. We repeatedly subjected the hole-notched specimen to fatigue load for a certain number of cycles, and then we investigated the residual strength of the hole-notched specimen by performing the fracture test. From the results of the test, we can observe the initiation of a directional crack caused by the applied fatigue load. Further, we observed that the residual strength increases with a decrease in the notch effect due to this crack. It was evaluated that the residual strength increases to a certain level and subsequently decreases. This variation in the residual strength was represented by a simple equation by using a model of the decrease in residual strength for plain plate, which was developed by Reifsnider and a stress redistribution model for hole-notched plate, which was developed by Yip.

A study on fatigue properties of plasma carburized low carbon Cr-Mo steel (플라즈마 침탄한 저탄소 Cr-Mo강의 피로특성에 관한 연구)

  • Park, Kyeong-Bong;Sin, Dong-Myung;Lee, Chang-Youl;Lee, Ktung-Sub
    • Korean Journal of Materials Research
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    • v.10 no.7
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    • pp.505-514
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    • 2000
  • The carburizing behavior and fatigue properties of the plasma carburized low carbon Cr-Mo steel(0.176C-1.014Cr-0.387Mo) have been investigated. The effective case depth in plasma carburized steel increased up to 50% in comparison with that of gas carburizing, and this case depth increased with the increasing surface carbon content. With increasing time in plasma carburizing, the surface carbon content increased but its increasing rate decreased. Fatigue properties were studied in terms of microstructure, case depth, retained austenite and residual stress near the surface. The fatigue limit of the plasma carburized steel was higher than that of gas carburized one. The initiation of microcracks and initial crack propagation were retarded due to a relatively little surface and internal oxidation layer in plasma carburized steel. Fractography showed the crack initiated at the surface, and transgranular fracture at surface layer was more predominant in plasma carburized steel compared to that of gas carburized steel.

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Influence of Filler Systems and Microstructures of SBR on Stress Softening Effect of SBR Vulcanizates (SBR의 미세 구조와 보강 시스템이 SBR 가황물의 응력 풀림 효과에 미치는 영향)

  • Choi, Sung-Seen;Han, Dong-Hun;Woo, Chang-Su
    • Elastomers and Composites
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    • v.41 no.3
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    • pp.164-171
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    • 2006
  • Stress softening behaviors of SBR vulcanizates reinforced with silica or carbon black were studied. Two types of SBR with different 1,2-unit contents of 18 and 60 wt% were used and three filler systems of carbon black and silica with/without silane coupling agent were employed. Stress softening behaviors of the SBR vulcanizates were varied with the SBR types as well as the filler systems. The silica-filled rubber specimens had higher residual strains than the carbon black-filled ones. The residual strains of silica-filled vulcanizates were remarkably reduced by adding a silane coupling agent. The maximum loads at 50% maximum stretch of the carbon black-filled vulcanizates were lower than those of the silica-filled ones. On the contrary, the maximum loads at 200% maximum stretch of the carbon black-filled vulcanizates were higher than those of the silica-filled ones. The maximum loads of the specimens with the 1,2-unit content of 60 wt% are higher than those with the 1,2-unit content of 18 wt% irrespective of the filler systems.

A Study of the Heat Treatment Effect on the Fatigue Crack Growth Behavior in Dissimilar Weld Metal Joints of SA508 Low-Carbon Steel and AISI316 Austenitic Stainless Steel (SA508 저탄소강과 AISI316 오스테나이트강의 이종 용접부 피로균열 성장 거동에 미치는 열처리 영향 연구)

  • Kim, Chung-Seok
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.17 no.3
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    • pp.16-21
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    • 2018
  • The effect of heat treatment on the fatigue crack growth behavior in welded joints between the heat-affected zone (HAZ) of SA 508 Cl.3 low-alloy steel and HAZ of AISI 316L stainless steel is investigated. When the crack propagates across SA 508 Cl.3 or AISI 316L SS and HAZ into the weldment, the fatigue crack growth rate (FCGR) in the HAZ region does not change or decrease despite the increase in stress intensity factor ${\Delta}K$. The residual stress at the HAZ region is more compressive than that at the base Δ materials and weldment. The effect of the welding residual stress on the crack growth behavior is determined by performing a residual stress relief heat treatment at $650^{\circ}C$ for 1h and subsequent furnace cooling. The FCG behavior in the HAZ region in the as-welded specimen and the residual stress relief heat-treated specimen is discussed in terms of the welding residual stress.

The Effects of Heat Treatment on the Fatigue Life and Welding Residual Stress of Welded Carbon Steel Plates (탄소강 후판용접부의 피로수명 및 잔류응력에 미치는 열처리 영향)

  • An, I.T.;Kim, W.T.;Jo, J.R.;Moon, Y.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.16 no.3
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    • pp.141-147
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    • 2003
  • The effects of heat treatment on the fatigue life and welding residual stress of welded plates were investigated in this study. The plates were welded by flux cored arc welding process, and post weld heat treated at $600^{\circ}C$ for 1 hour. The residual stresses of welded plates before and after post weld heat treatment were measured by hole drilling method. To measure the fatigue life of welded plates, low cycle fatigue tests under strain control and high cycle fatigue tests under load control were performed respectively, by using cylindrical specimens containing weld metal and heat affected zone. The obtained result shows that the post weld heat treatment reduces the residual stress, and resultantly changes the fatigue life of welded plate. Goodman diagrammatic analysis has also been performed to study the effect of post weld heat treatment on the high cycle fatigue life.

Investigation into the Effects of Process Parameters of DED Process on Deposition and Residual Stress Characteristics for Remanufacturing of Mechanical Parts (기계 부품 재제조를 위한 DED 공정 조건에 따른 적층 및 잔류응력 특성 분석)

  • Kim, D.A.;Lee, K.K.;Ahn, D.G.
    • Transactions of Materials Processing
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    • v.30 no.3
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    • pp.109-118
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    • 2021
  • Recently, there has been an increased interest in the remanufacturing of mechanical parts using metal additive manufacturing processes in regards to resource recycling and carbon neutrality. DED (directed energy deposition) process can create desired metallic shapes on both even and uneven substrate via line-by-line deposition. Hence, DED process is very useful for the repair, retrofit and remanufacturing of mechanical parts with irregular damages. The objective of the current paper is to investigate the effects DED process parameters, including the effects of power and the scan speed of the laser, on deposition and residual stress characteristics for remanufacturing of mechanical parts using experiments and finite element analyses (FEAs). AISI 1045 is used as the substrate material and the feeding powder. The characteristic dimensions of the bead shape and the heat affected zone (HAZ) for different deposition conditions are obtained from the experimental results. Efficiencies of the heat flux model for different deposition conditions are estimated by the comparison of the results of FEAs with those of experiments in terms of the width and the depth of HAZ. In addition, the influence of the process parameters on residual stress distributions in the vicinity of the deposited region is investigated using the results of FEAs. Finally, a suitable deposition condition is predicted in regards to the bead formation and the residual stress.

The Study for Impact Strength change of Microcellular foamed Recycled ABS (초미세 발포 플라스틱의 재생 후 강도변화에 대한 연구)

  • 성갑제;차성운;윤재동
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2002.10a
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    • pp.896-899
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    • 2002
  • Microcellular foaming Process has several merits, impact strength elevation, thermal insulation, noise insulation, and raw material saving etc. This method make the glass transition temperature of polymers low, and diminish the residual stress of polymers. This characteristics of Microcellular foaming process influences the physical properties of recycled polymers. This paper describes about the impact strength change of Microcellular foamed recycled ABS.

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The study on the manufacturing intermediary materials for the carbon nanofiber reinforced Cu matrix noncomposite (일방향 탄소나노섬유 강화 Cu 기지 나노복합재료용 중간재 제조에 관한 연구)

  • 백영민;이상관;엄문광
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2003.10a
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    • pp.46-49
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    • 2003
  • Cu have been widely used as signal transmission materials for electrical electronic components owing to its high electrical conductivity. However, it's size have been limited to small ones due to its poor mechanical properties, Until now, strengthening of the copper at toy was obtained either by the solid solution and precipitation hardening by adding alloy elements or the work hardening by deformation process. Adding the at toy elements lead to reduction of electrical conductivity. In this aspect, if carbon nanofiber is used as reinforcement which have outstanding mechanical strength and electric conductivity, it is possible to develope Cu matrix nanocomposite having almost no loss of electric conductivity. It is expected to be innovative in electric conduct ing material market. The unidirectional alignment of carbon nanofiber is the most challenging task developing the copper matrix composites of high strength and electric conductivity In this study, the unidirectional alignment of carbon nanofibers which is used reinforced material are controlled by drawing process in order to manufacture the intermediary materials for the carbon nanofiber reinforced Cu matrix nanocomposite and align mechanism as well as optimized drawing process parameters are verified via experiments and numerical analysis. The materials used in this study were pure copper and the nanofibers of 150nm in diameter and of $10~20\mu\textrm{m}$ In length. The materials have been tested and the tensile strength was 75MPa with the elongation of 44% for the copper it is assumed that carbon nanofiber behave like porous elasto-plastic materials. Compaction test was conducted to obtain constitutive properties of carbon nanofiber. Optimal parameter for drawing process was obtained by experiments and numerical analysis considering the various drawing angles, reduction areas, friction coefficient, etc Lower reduction areas provides the less rupture of cu tube is not iced during the drawing process. Optimal die angle was between 5 degree and 12 degree. Relative density of carbon nanofiber embedded in the copper tube is higher as drawing diameter decrease and compressive residual stress is occurred in the copper tube. Carbon nanofibers are moved to the reverse drawing direct ion via shear force caused by deformation of the copper tube and alined to the drawing direction.

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