• 대한치과기공학회지
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• 제30권1호
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• pp.33-39
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• 2008

Recently natural characteristics and esthetics have been interested increasing in clinical dentistry. Thus the evaluation of the shade of dental porcelain has become an important part in dental research. Noritake Super Porcelain EX-3 Vita shade A2 (Noritake, Japan) Vintage HaLo Vita shade A2 (Shofu, Japan), Vita omega 900 Vitapan 3D-master shade 2M2 (Vita, Germany) were conducted for six times for repeated firing in a way to observe the change of color with respect to the number of firing. The repeated firing was implemented with the vacuum firing and air firing, and by using Shade Eye-EX Chroma meter (Shofu, U.S.A.), the changes in values of shade, value and chroma were compared. With the above results, the change of color was not noticed only in Vita when repeated firing was applied.

• 대한치과기공학회지
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• 제4권1호
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• pp.5-7
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• 1982

This study was performed to examine the effect of repeated firing on porcelain color stability. Sixty sepcimens of generally uniform size and shape(9.7 12mm)were prepared using the manufactorer's specifications and among them 50 specimens that showed no defect after firing procedure were selected. All samples, abraded with sandpaper disc, ultrasonically cleaned, and air fired to amedium glaze were devided into 10 groups according to the number of repeated firing and, upon completion, mounted on a 13 by 16cm board. 30 persons(five dentists, ten dental techanicians, and fiftheen students) were asked to compare the samples for variations, in hue, chroma and value under natural and artificial light. The results were as follows:(1) There were no color change detected in the first four firings.(2) Slight color change were noticed in subsequent firings(ie: greater decreases in value with slight increases In chroam)(3) However, the hue remained constant in all 10 groups after repeated firings.

• The Journal of Advanced Prosthodontics
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• 제5권1호
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• pp.44-50
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• 2013

PURPOSE. The aim of this study was to evaluate the effects of repeated porcelain firing process on the corrosion rates of the dental alloys. MATERIALS AND METHODS. Cr-Co, Cr-Ni and Pd-Ag alloys were used for this study. Each metal supported porcelain consisted of 30 specimens of 10 for 7, 9 and 11 firing each. Disc-shaped specimens 10 mm diameter and 3 mm thickness were formed by melting alloys with a propane-oxygen flame and casted with a centrifuge casting machine and then with the porcelain veneer fired onto the metal alloys. Corrosion tests were performed in quintuplicate for each alloy (after repeated porcelain firing) in Fusayama artificial saliva solution (pH = 5) in a low thermal-expansion borosilicate glass cell. Tamhane and Sheffe test was used to compare corrosion differences in the results after repeated firings and among 7, 9 and 11 firing for each alloy. The probability level for statistical significance was set at ${\alpha}$=0.05. RESULTS. The corrosion resistance was higher (30 mV), in case of 7 times firing (Commercial). On the other hand, it was lower in case of 11 times firing (5 mV) (P<.05). Conclusion. Repeated firings decreased corrosion resistance of Pd-Ag, Cr-Co and Cr-Ni alloys. The Pd-Ag alloy exhibited little corrosion in in vitro tests. The Cr-Ni alloy exhibited higher corrosion resistance than Cr-Co alloys in in vitro tests.

• 대한치과보철학회지
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• 제35권4호
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• pp.706-718
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• 1997

Ceramometal crowns are common restorations in fixed prosthodontics because of their casting accuracy, the high strength properties of the metal, and the cosmetic appearance of porcelain. However, deterioration of the initial fit of the metal coping has been observed after the porcelain firing cycle. The distortion due to repeated firing makes it difficult to fit crown margin and elicits microleakage. The major causes of distortion are the residual stress that accumulate during wax-up, casting, cold work and the induced stress caused by the mismatch of porcelain-metal thermal contraction. This study examined the marginal fit changes of metal copings in relation to repeated firing and the effects of heat treatment that reduce the distortion resulted from residual stress. The marginal changes of the copings that were treated with conventional method and those treated with heat before repeated firing, were evaluated. The metal die which represented preparations of a maxillary central incisor was fabricated, and 45 wax patterns were cast with nonprecious metal alloys. The heat treatment of each group was performed as follows. Group 1(control) : Casting - Devesting - Cold work - Firing Group 2 : Casting - Heat treatment - Devesting - Cold work - Firing Group 3 : Casting - Devesting - Cold work - Reinvesting - Heat treatment - Devesting - Firing The copings were fired 3 times. After each firing, the marginal fit changes were measured with inverted metallurgical microscope at the 4 reference points located at labial, lingual, and both proximal surface. Measurements were compared, and statistically analyzed. The results were as follows ; 1. In all groups, the highest value of marginal fit changes of the copings studied were found after the first firing cycle. 2. When the distortion of each experimental group at the first firing cycle were compared, group 1 exhibited the greatest changes($20-27{\mu}m$), followed by group 2($9-13{\mu}m$), and group 3($8-10{\mu}m$). 3. The copings treated with heat before devesting(group 2) revealed significantly smaller marginal fit changes than the copings treated with conventional method(group 1). (p<0.01) 4. The copings treated with heat after reinvesting(group 3) revealed significantly smaller marginal fit changes than the copings treated with conventional method(group 1). (p<0.01) 5. No siginificant differences in marginal fit changes were found between the copings treated with heat before devesting(group 2) and the copings treated with heat after reinvesting(group 3). (p>0.01)

• 한국산학기술학회논문지
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• 제21권5호
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• pp.648-655
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• 2020

현대의 자동소총의 공이는 공이치기에 의해 타격을 받아 장전된 탄약의 뇌관을 기폭 시키는 역할을 한다. 이 과정에서 공이는 충격하중을 받게 되며 소총의 수명주기 동안 반복적인 힘을 받게 된다. 소총의 내구도 시험에서 전체의 96.26% 진행 중 공이가 조기에 파손되는 현상이 발생하였다. 이에 따라 원인분석과 재현시험을 통해 파손현상 사례연구를 실시하였다. 파손이 발생한 공이의 파단면을 현미경 및 SEM 분석결과 반복충격에 의해 표면 원주방향 전체에서 균열이 시작해 심부로 피로균열이 발생했다. 반복충격에 의해 균열이 성장하다 마지막에 피로파괴가 발생하였으며, 노치에 의한 것으로 추정되었다. 검증을 위해 원주방향 0.03mm의 노치를 생성한 공이로 재현시험결과 동일한 형태의 파단면을 가지면서 전체 수명의 64.25%에서 파손되었다. 파손사례연구를 위한 노치형태별 재현시험결과 한쪽 측면 노치 0.3mm, 0.5mm의 공이는 각각 65.53%, 50.76%에서, 6개 지점의 노치 0.03mm는 85.65%에서 파손되었다. 마지막으로 표면 거칠기가 거칠고 툴 마크가 육안으로 확인이 가능한 공이는 내구수명을 만족하며 381㎛의 내부균열이 진행되었다. 본 연구를 통해 노치형태별 파손에 대해 고찰하였으며, 반복충격을 받는 부품의 신뢰성 확보를 위해 노치와 표면 거칠기 품질관리가 중요한 것을 알 수 있다.

• 대한치과기공학회지
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• 제31권1호
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• pp.23-36
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• 2009

The goal of esthetic restoration is to achieve morphologic, optical, and biologic acceptance. Creation of a natural looking ceramic restoration, which blends harmoniously with surrounding dentition, is not always achieved. A successful color match is an important aspect of any esthetic dental restoration. Since natural enamel has inherent translucency, it is important that ceramic restorations reproduce the translucency and color of the natural teeth. However, the final color match of porcelain crowns to adjacent natural dentition remains some problem. Difficulties related to color matching arise from the structural differences that exist between metal ceramic crowns and natural teeth, the limited range of available ceramic shades, inadequate shade guides, different types of metal alloys, repeated firing, the condensation technique, and varying compositions of ceramic materials. Many factors contribute to the esthetic success of dental restoration: optical properties such as color and its elements of hue, value, and chroma; translucency and opacity; light transmission and scattering; and metamerism and fluorescence. The purpose of this study was to determine the color changes of metal-ceramic system with different veneering porcelain powder after repeated firing. The objectives of this in vitro study were to measure the lightness($L^*$), chromaticity($a^*$), chromaticity($b^*$), chroma($C^*$), hue(h), reflectance(%), color difference(${\Delta}E$). The following conclusions were obtained: 1. An increase in the number of firings resulted in decrease in lightness($L^*$) but increase in chromacticity($a^*$) with all porcelain. After the second sintering resulted in decrease in chromacticity($b^*$) with opaque-dentin porcelain and dentin porcelain but in increase with enamel porcelain and translucency porcelain. And after the second sintering resulted in decrease in chroma($C^*$) with opaque-dentin porcelain and dentin porcelain, but on the whole side in decrease with enamel porcelain and translucency porcelain. 2. After the second firing, a increase in the number of firings resulted in decrease reflectance(%) in all wavelength. 3. There were noticeable color differences(${\Delta}E$) between first sintering and multiple firings(dentin porcelain: 5.29~8.15, opaque-dentin porcelain: 4.83~8.2, enamel porcelain: 8.93~13.15, translucency porcelain: 9.37~12.91), but the color difference(${\Delta}E$) after second sintering were down to 4.87 in all porcelain. 4. Given the NBS Criteria, a 'trace' was not found this study but a 'slight' was found 2-3, 3-5 in dentin porcelain, 2-3 in opaque-dentin porcelain, 3-5, 5-10 in enamel porcelain and translucency porcelain, a 'noticeable' was 2-5, 3-10, 5-10 in dentin porcelain and opaque-dentin porcelain, 2-3, 2-5, 3-10 in enamel porcelain 2-3, 3-10 in translucency porcelain, an 'appreciable' was 1-2, 1-3, 2-10 in dentin porcelain 1-2, 1-3, 2-10, 3-10 in opaque-dentin porcelain, 2-10 in enamel porcelain, 2-5, 2-10 in translucency porcelain, a 'much' was 1-5, 1-10 in dentin porcelain and opaque-dentin porcelain, 1-2, 1-3, 1-5 in enamel porcelain 1-2, 1-3, 1-5, 1-10 in translucency porcelain, a 'very much' was 1-10 in enamel porcelain.

• The Journal of Advanced Prosthodontics
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• 제6권6호
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• pp.462-467
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• 2014

PURPOSE. This study investigated the influence of surface conditioning procedures and repeated firings on monoclinic content and strength of zirconia before cementation. MATERIALS AND METHODS. Sintered bar-shaped zirconia specimens were subjected to no surface treatment (control), air abrasion, or grinding (n=21). Their roughness was evaluated using a profilometer, and microscope analysis was performed on one specimen of each group. Then, 2 or 10 repeated firings (n=10) were executed, the monoclinic content of specimens was analyzed by X-ray diffraction, and a three-point flexural strength test was performed. Surface roughness values were compared using one-way analysis of variance (ANOVA) and Tukey honestly significant difference (HSD) tests, the monoclinic content values were tested using Kruskal-Wallis and Mann-Whitney U tests, and the flexural strength values were tested using two-way ANOVA and Tukey HSD tests (P=.05). Spearman's correlation test was performed to define relationships among measured parameters. RESULTS. Surface-treated specimens were rougher than untreated specimens and had a higher monoclinic content (P<.005), and the relationship between roughness and monoclinic content was significant (P<.000). Neither surface treatment nor firing significantly affected the flexural strength, but Weibull analysis showed that for the air-abraded samples the characteristic strength was significantly lower after the $10^{th}$ firing than after the $2^{nd}$ firing. CONCLUSION. After firing, a negligible amount of monoclinic content remained on the zirconia surfaces, and rougher surfaces had higher monoclinic contents than untreated surfaces. Multiple firings could be performed if necessary, but the fracture probability could increase after multiple firings for rougher surfaces.

• The Journal of Advanced Prosthodontics
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• 제6권4호
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• pp.309-316
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• 2014

PURPOSE. The color of the ceramic restorations is affected by various factors such as brand, thickness of the layered the ceramic, condensation techniques, smoothness of surface, number of firings, firing temperature and thickness of dentin. The aim of this study was to evaluate the color change and surface roughness in dental porcelain with different thicknesses during repeated firings. MATERIALS AND METHODS. Disc-shaped (N=21) metal-ceramic samples (IPS Classic; Ivoclar Vivadent; Shaar, Liechtenstein) with different thickness were exposed to repeated firings. Color measurement of the samples was made using a colorimeter and profilometer was used to determine surface roughness. ANOVA and Tukey tests with repeated measurements were used for statistical analysis. RESULTS. The total thickness of the ceramics which is less than 2 mm significantly have detrimental effect on the surface properties and color of porcelains during firings (P<.05). CONCLUSION. Repeated firings have effects on the color change and surface roughness of the dental ceramics and should be avoided.

• The Journal of Advanced Prosthodontics
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• 제6권6호
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• pp.427-433
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• 2014

PURPOSE. Surface color is one of the main criteria to obtain an ideal esthetic. Many factors such as the type of the material, surface specifications, number of firings, firing temperature and thickness of the porcelain are all important to provide an unchanged surface color in dental ceramics. The aim of this study was to evaluate the color changes in dental ceramics according to the material type and glazing methods, during the multiple firings. MATERIALS AND METHODS. Three different types of dental ceramics (IPS Classical metal ceramic, Empress Esthetic and Empress 2 ceramics) were used in the study. Porcelains were evaluated under five main groups according to glaze and natural glaze methods. Color changes (${\Delta}E$) and changes in color parameters (${\Delta}L$, ${\Delta}a$, ${\Delta}b$) were determined using colorimeter during the control, the first, third, fifth, and seventh firings. The statistical analysis of the results was performed using ANOVA and Tukey test. RESULTS. The color changes which occurred upon material-method-firing interaction were statistically significant (P<.05). ${\Delta}E$, ${\Delta}L$, ${\Delta}a$ and ${\Delta}b$ values also demonstrated a negative trend. The MC-G group was less affected in terms of color changes compared to other groups. In all-ceramic specimens, the surface color was significantly affected by multiple firings. CONCLUSION. Firing detrimentally affected the structure of the porcelain surface and hence caused fading of the color and prominence of yellow and red characters. Compressible all-ceramics were remarkably affected by repeated firings due to their crystalline structure.

• 대한치과기공학회지
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• 제45권3호
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• pp.55-60
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• 2023

Purpose: This study aimed to evaluate the effects of a special heat treatment on Pd-Au-Ag metal-ceramic alloy after degassing treatment and on changes in the hardness of the alloy during the firing process. Methods: Specimen alloys were cast and subjected to degassing at 900℃ for 10 minutes. These specimens were then subjected to a special heat treatment at 600℃ for 15 minutes in a dental porcelain furnace. Further, the specimens were subjected to simulated firing in the porcelain furnace. The resulting specimens were then tested for hardness, and changes in the microstructure were observed. Results: There was a decrease in the hardness of the alloy during the simulated firing of the cast alloy due to the coarsening of the particles. Meanwhile, additional heat treatment after degassing was found to play a crucial role in preventing a decrease in hardness. This treatment effectively suppressed the coarsening of the precipitates during repeated firing at high temperatures. Conclusion: Specific heat treatment of the Pd-Au-Ag metal-ceramic alloy prevented a decrease in its hardness and extended the lifespan of the metal-ceramic prosthesis.