• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2000.10a
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• pp.25-28
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• 2000

The flow stress of 304 stainless steel during high during hot forming process were determined by conducting hot compression tests at the range of 1273 K-1423 K and 0.05 /s-2.0 /s as these are typical temperature and strain rate in hot forging operation. Based on the observed phenomena, a constitutive model of flow stress was assumed as a function of strain, strain rate, temperature. Dynamic recrystallization was found to be the major softening mechanism with this conditions as previous studies. A finite element analysis was performed to predict the recrystallized volume fraction and the mean grain size in hot compression of 304 stainless steel.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2003.05a
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• pp.427-733
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• 2003

Adiabatic shear bands have been observed in the serrated chip during high strain rate metal cutting process of medium carbon steel and titanium alloy. The recent microscopic observations have shown that dynamic recrystallization occurs in the narrow adiabatic shear bands. However the conventional flow stress models such as the Zerilli-Armstrong model and the Johnson-Cook model, in general, do not predict the occurrence of dynamic recrystallization (DRX) in the shear bands and the thermal softening effects accompanied by DRX. In the present study, a strain hardening and thermal softening model is proposed to predict the adiabatic shear localized chip formation. The finite element analysis (FEA) with this proposed flow stress model shows that the temperature of the shear band during cutting process rises above 0.5T$\sub$m/. The simulation shows that temperature rises to initiate dynamic recrystallization, dynamic recrystallization lowers the flow stress, and that adiabatic shear localized band and the serrated chip are formed. FEA is also used to predict and compare chip formations of two flow stress models in orthogonal metal cutting with AISI 1045. The predictions of the FEA agreed well with the experimental measurements.

• Applied Microscopy
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• v.43 no.2
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• pp.88-97
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• 2013

Technical investigation to figure out the problems arising during in-situ heating electron backscatter diffraction (EBSD) analysis inside scanning electron microscopy (SEM) was carried out. EBSD patterns were successfully acquired up to $830^{\circ}C$ without degradation of EBSD pattern quality in steels. Several technical problems such as image drift and surface microstructure pinning were taking place during in-situ experiments. Image drift problem was successfully prevented in constant current supplying mode. It was revealed that the surface pinning problem was resulted from the $TiO_2$ oxide particle formation during heating inside SEM chamber. Surface pinning phenomenon was fairly reduced by additional platinum and carbon multi-layer coating before in-situ heating experiment, furthermore was perfectly prevented by improvement of vacuum level of SEM chamber via leakage control. Plane view in-situ observation provides better understanding on the overall feature of recrystallization phenomena and cross sectional in-situ observation provides clearer understanding on the recrystallization mechanism.

• Transactions of Materials Processing
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• v.12 no.4
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• pp.358-363
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• 2003

Adiabatic shear bands have been observed in the serrated chip during high strain rate metal cutting process of medium carbon steel and titanium alloy The recent microscopic observations have shown that dynamic recrystallization occurs in the narrow adiabatic shear bands. However the conventional flow stress models such as the Zerilli-Armstrong model and the Johnson-Cook model, in general, do not predict the occurrence of dynamic recrystallization (DRX) in the shear bands and the thermal softening effects accompanied by DRX. In the present study, a strain hardening and thermal softening model is proposed to predict the adiabatic shear localized chip formation. The finite element analysis (FEA) with this proposed flow stress model shows that the temperature of the shear band during cutting process rises above 0.5Τ$_{m}$. The simulation shows that temperature rises to initiate dynamic recrystallization, dynamic recrystallization lowers the flow stress, and that adiabatic shear localized band and the serrated chip are formed. FEA is also used to predict and compare chip formations of two flow stress models in orthogonal metal cutting with AISI 1045. The predictions of the FEA agreed well with the experimental measurements.s.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2000.10a
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• pp.33-36
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• 2000

The dynamic recrystallization (DRX) of medium carbon steels (SCM 440 and POSMA45) was studied with torsion test in the temperature range of $900-1100^{\circ}C$ and the strain rate range of $5.0x10^{-2}\;-\;5.0x10^0/sec$. To establish the quantitative equations for DRX, the evolution of flow stress curve with strain was analyzed. The critical strain (${\varepsilon}_c$) and strain for maximum softening rate ( ${\varepsilon}^{*}$) could be confirmed by the analysis of work hardening rate ($d{\sigma}/d{\varepsilon}\;=\; \theta$). The volume fraction of dynamic recrystallization ($X_{DRX}$) as a function of processing variables, such as strain rate ( $\dot{\varepsilon}$ ), temperature (T), and strain ( $\varepsilon$ ) were established using the ${\varepsilon}_c$ and ${\varepsilon}^{*}$. For the exact prediction, the ${\varepsilon}_c$, ${\varepsilon}^{*}$ and Avrami' exponent (m') were quantitatively expressed by dimensionless parameter, Z/A respectively. The transformation-effective strain-temperature curve for DRX could be composed. It was found that the calculated results were agreed with the experimental data for the steels at any deformation conditions.

• Journal of the Korean Society for Heat Treatment
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• v.10 no.4
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• pp.246-254
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• 1997

The 6.5wt %Si-Fe alloy sheets were made by the twin roll process. The magnetic properties and microstructures of sheets annealed in the sulfur atmosphere were studied. In the as-prepared sheet, non-oriented columnar grains about $10{\mu}m$ in diameter were observed, which grew from the surface to the inner part of the sheet. When the annealing temperature was around $700^{\circ}C$, the primary recrystallization was formed around the middle part of the sheet thickness, and the grain size increased with increasing annealing temperature. At the annealing temperature of $900^{\circ}C$, the grain size became $30{\sim}40{\mu}m$. Around the annealing temperature, the motive force of the grain growth is the grain boundary energy. However, above $1000^{\circ}C$ the surface energy played an important role in the observed grain growth. When the sheet were annealed at $1200^{\circ}C$, the grains whose (100) planes were paralled to the thin plate surface grew, and all sheet surfaces were covered with these grains after 1 hour annealing. This phenomenon is called tertiary recrystallization. A difference in surface energy between (100) and (110) surfaces provides a driving force for growth of tertiary grains. The coercive force was 0.27 mOe and the AC core loss $W_{12/50}$ was 0.38w/kg for the 6.5wt%Si-Fe alloy.

• Transactions of Materials Processing
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• v.10 no.4
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• pp.338-346
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• 2001

Evaluation of microstructural changes is important for process control during open die forging of heavy ingots. The control of forging parameters, such as shape of the dies, reduction, temperature and sequence of passes, is to maximize the forging effects and to minimize inhomogeneities of mechanical properties. The hot working die steel is produced by using the multistage open die forging. The structure is altered during forging by subsequent Precesses of plastic deformation, recrystallization and grain growth. A numerical analysis using an rigid visco-plastic finite element model was performed to predict microstructural evolution of hot working die steel.

• Transactions of Materials Processing
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• v.7 no.3
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• pp.197-206
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• 1998

This paper presents the prediction of dynamic recrystallization behavior during hot forging of Inconel 718. Another experiment of pancake forging was also carried out to examine the recrystallization ration dynamically recrystallizaed grain size, and grain growth in the forging. In experiments cylindrical billets were forged by two operations with variations of forging temperature, reduction ration of deformation. and preheating process at each forging step. Also the finite element program, developed here for the prediction using the metallurgical models was used for the analysis of to Inconel 718 upsetting and the results were compared with experimental ones.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2003.05a
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• pp.195-198
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• 2003

High temperature deformation and softening behavior of SAF 2507 super duplex stainless steel (SDSS) has been investigated in connection with an FEM analysis of hot forging process. Flow curves at various strain rates and temperatures were determined first from compression tests, and the kinetics of dynamic recrystallization were also formulated through the analysis of load relaxation test results. Applying the dynamic materials and proposed by Prasad et al., it was possible to determine the characteristics of deformation behavior effectively at a given condition of deformation. Constitutive relations and recrystallization kinetics formulated from the test results were then implemented in a commercial FEM code. Flow stress compensation formulated upon the volume fraction of recrystallization and adiabatic heating was found to improve significantly the FEA solutions in predicting the forming load and the distribution of recrystallized volume fraction after forging.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2001.05a
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• pp.131-135
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• 2001

Evaluation of microstructural changes during open die forging of heavy ingots is important for process control. The objective of the control of forging parameters, such as shape of the dies, reduction, temperature and sequence of passes, is to maximize the forging effects md to minimize inhomogeneities of mechanical properties. The hot working die steel is produced by using the multistage open die forging. The structure is altered during forging by subsequent processes of plastic deformation, recrystallization and grain growth. A numerical analysis using an rigid visco-plastic finite element model was performed to predict microstructural evolution of hot working die steel.