• Title/Summary/Keyword: recrystallization temperature

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The study of recrystallization of willemite crystal in ceramic glaze (도자기용 아연 결정유의 재결정화 연구)

  • Lee, Hyun-Soo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.30 no.4
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    • pp.136-142
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    • 2020
  • Crystallization of zinc crystalline glaze requires demanding conditions such as the formation of a nucleating agent and the amount of nucleating agent, and growth of crystalline. Zinc crystalline glaze is hard to utilize in the industry because of its narrow range of the firing temperature, and the crystallization's dependency on the quality of zinc. Stimulation of zinc crystallization and formation of frit enable zinc crystalline glaze to be reconstituted in a various range of firing schedules, leading to the development of a competitive industrial glaze.

Synthesis of $Ca_2$-based Clinker by Hydration-Burning Method: (III) Study on the Microstructural Changes during Clinker Burning (수화-소성법에 의한 $Ca_2$ 클린커의 합성: (III) 클린커소성 중의 미구조 변화)

  • 송태웅;한기성
    • Journal of the Korean Ceramic Society
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    • v.28 no.10
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    • pp.751-756
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    • 1991
  • Continuous microstructural changes on heating of hardened paste prepared from primary clinker of CA2 composition was studied. On heating period, several characteristic shrinkages and microstructural changes took place in the specimen due to the dehydration and recrystallization of calcium aluminates without regard to the accelerative shrinkage resulted from sintering. Though micropores formed by dehydration decreased with recrystallization of calcium aluminates, micropores formed by plate-type gibbsite in the hydrates were maintained up to the temperature at which CA2 becomes main phase and had influence to the microstructure of the final clinker.

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A Study on the Deep drawing drawability and Analyzing process of AZ31B Magnesium Sheet at Warm and Hot temperature (AZ31B 마그네슘 판재의 온,열간 딮드로잉 성형성 및 공정해석)

  • Han, S.H.;Choo, D.K.;Kang, C.G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2006.05a
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    • pp.48-52
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    • 2006
  • The drawability of AZ31B magnesium sheet is estimated at various temperatures (200, 250, 300, 350 and $400^{\circ}C$), and forming speed (20, 50, 100 mm/min), thickness (0.5, 0.8, 1.0, 1.4 mm). The deep drawing process of circular cup and square cup were used in forming experiments. Experimental and FEM analysis are performed to investigate drawability and affection of controlled blank holding force. Through the controlled blank holding force, drawability was improved. This result is verified by FEM analysis. Through the observation of microstructure, the main cause is investigated as a quantity of the dynamic recrystallization.

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Prediction of Flow Stress of Steel in Consideration of Recrystallization (재결정거동을 고려한 강의 유동응력 예측)

  • 이동근;박종진
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1999.08a
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    • pp.341-348
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    • 1999
  • In the finite elemenet analysis of metal forming problems, the most critical input is the flow stress of workpiece. Conventionally, the flow stress of a metal at elevated temperatures is assumed to be a function of strain, strain rate and temperature, and obtained by experiment. However, if the workpiece is not continuously deformed as in mulit-pass rolling, the flow stress obtained by experiment is no longer valid because it does not consider the microstructure evolution occurring between deformations. In the present study, it was attemped that the flow stress of steel in the austenite region be obtained equations. It was applied to the prediction of flow stress variation at each stand during hot finishing rolling of steel.

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Analysis of Microstructures in a Forged Ti-6Al-4V Disk (Ti-6Al-4V 단조 디스크의 미세조직 분석)

  • 김대영;박종진
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1997.10a
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    • pp.202-209
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    • 1997
  • The mechanical properties of Ti-6Al-4V greatly vary for changes of microstructures. Therefore, when manufacturing components with this material, it is important to understand the influence of process parameters to the resulting microstructures. In the present investgation, it was attempted to relate the process parameters with the microstructures in a hot forged Ti-6Al-4V disk. The investigation was carried out by a rigid thermo-viscoplastic FEM analysis, flow stress measurements and microstructure studies. It was found that the dynamic recrystallization would hardly occur in this material and that variations of strain, strain rate and temperature of several locations in the disk were below the assumed dynamic recrystallization zone. These findings confirmed the experimental obervations that the microstructures in the disk were only deformed without being recrystallized.

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The prediction of grain size of Al-5wt%Mg alloy by FEM (유한요소법을 이용한 Al-5wt%Mg합금의 미세조직 크기 예측)

  • 황원주;조종래;배원병
    • Transactions of Materials Processing
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    • v.8 no.6
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    • pp.620-625
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    • 1999
  • A finite element analysis is performed to predict the recrystallized volume fraction and the mean grain size in hot compression of Al-5wt%Mg alloy. In the analysis, a modeling equation of flow stress is assumed as a function of strain, strain rate, and temperature. And the influence of above varibles on flow stress is quantified by using Zener-Hollomon Parameter. In the modeling equation, effects of strain hardening and dynamic recrystallization on microstructure of Al-5wt%Mg alloy are investigated. The predicted results of recrystallized volume fraction and mean grain size are in good agreement with those of microstructures obtained from hot compression tests.

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A Study on the Mechanical Properties with the Strain rate and Strain for Aluminum 6061 Alloy in Hot Forging (알루미늄 6061 합금의 열간단조시 변형율속도 및 변형율에 따른 기계적 성질에 관한 연구)

  • 김정식;이영선;김용조;이정환
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2002.05a
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    • pp.154-158
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    • 2002
  • The mechanical properties of Al 6061 excluded bar were deformed in high temperature with the variable deformation conditions and characterized by the tensile test. Three types of different strain rate were experimentally performed by using hydraulic press, crank press and hammer and two types of the nominal strain 0.5 and 0.8 were achieved. To decide optimum forging process, the relationship among the strain rate, strain and mechanical properties was explained by analyzing the microstructures of the forged and heat heated parts. The strength was deeply related with the strain rate due to the dynamic recrystallization (DRX) in hot forging, and the best forging condition was presented in Al 6061 alloy.

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Effect of Annealing on Microstructural and Mechanical Property Variation of the Oxide-Dispersion-Strengthened Cu alloy (산화물 분산강화 동합금의 열처리에 따른 미세조직 및 기계적 특성 변화)

  • Kim Yong-Suk
    • Journal of Powder Materials
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    • v.13 no.1 s.54
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    • pp.25-32
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    • 2006
  • The alumina dispersion-strengthened (DS) C15715 Cu alloy fabricated by a powder metallurgy route was annealed at temperatures ranging from $800^{\circ}C\;to\;1000^{\circ}C$ in the air and in vacuum. The effect of the annealing on microstructural stability and room-temperature mechanical properties of the alloy was investigated. The microstructure of the cold rolled OS alloy remained stable until the annealing at $900^{\circ}C$ in the air and in vacuum. No recrystallization of original grains occurred, but the dislocation density decreased and newly formed subgrains were observed. The alloy annealed at $1000^{\circ}C$ in the air experienced recrystallization and grain growth took place, however annealing in vacuum at $1000^{\circ}C$ did not cause the microstructural change. The mechanical property of the alloy was changed slightly with the annealing if the microstructure remained stable. However, the strength of the specimen that was recrystallized decreased drastically.

Growth of Ice Crystal with Concentration of Surfactant in Water Solution (계면활성제 농도가 빙결정의 입자크기에 미치는 영향)

  • ;稻葉英男
    • Journal of Advanced Marine Engineering and Technology
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    • v.26 no.2
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    • pp.240-247
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    • 2002
  • Recently, a thermal energy storage system has been developed actively fur the purpose of saving energy and reducing the peak electrical demand. Especially, ice slurry is a promising working fluid for low temperature energy storage systems. A flow of ice crystals has a large cooling capacity as a result of the involvement of latent heat. However, there are still problems related to the recrystallization of ice crystals for realizing long term storage and long distance transportation. To find improvements fur this, a method for the creation of ice crystals resistant to recrystallization has been proposed and researched by the use of an antifreeze protein (AFP) solution etc. In the present study, it has been investigated the growth of ice crystal in several kinds of water solution added non-ionic surfactant. The results shows that size of ice crystal was smaller with increasing in added surfactant. And ice crystal was not increased with added surfactant.

MICROSTRUCTURAL OBSERVATION AND TENSILE ISOTROPY OF AN AUSTENITIC ODS STEEL

  • Kim, Tae-Kyu;Bae, Chang-Soo;Kim, Do-Hyang;Jang, Jin-Sung;Kim, Sung-Ho;Lee, Chan-Bock;Hahn, Do-Hee
    • Nuclear Engineering and Technology
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    • v.40 no.4
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    • pp.305-310
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    • 2008
  • Based on a composition of 99.4 wt% AISI 316L stainless steel, 0.3wt% Ti and 0.3 wt% $Y_2O_3$, an austenitic ODS steel was fabricated by a process of mechanical alloying, hot isostatic pressing and rolling. Fine oxide particles were observed in the matrix, and their chemical formulations were determined to be $Y_2Si_2O_7$ and TiO. Heat treatment of the cold-rolled sample at $1200^{\circ}C$ induced an isotropic tensile behavior at room temperature and at $700^{\circ}C$. This result would be mainly attributed to the equiaxed grains that form as a result of the heat treatment for recrystallization.