• Title/Summary/Keyword: rapid preparation

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Preparation and Flame-Retardant Optimization of PU Coatings Using Chlorine-Containing Modified Polyester/IPDI- Isocyanurate

  • You, Hyuk-Jae;Shim, Il-Woo;Jo, Hye-Jin;Park, Hong-Soo;Kim, Seung-Jin;Kim, Young-Geun
    • Journal of the Korean Applied Science and Technology
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    • v.22 no.1
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    • pp.1-8
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    • 2005
  • Chlorine-containing modified polyester polyols were synthesized by two-step condensation reactions. Intermediate was synthesized by the esterification of monochloroacetic acid with trimethylolpropane in the first step. Polycondensation of the intermediate (MCAOs), 1,4-butanediol, and trimethylolpropane with adipic acid was carried out. Two-component polyurethane (PU) coatings were prepared by blending MCAOs and IPDI-isocyanurate. There new flame-retardant coatings showed various properties comparable to other non-flame-retardant coatings. They were superior to flammable coatings from the experimental results showing rapid and 10 to 13 hours of pot-life. Coatings with 30wt% monochloroacetic acid was not flammable by the vertical flame retardancy test.

Application of Dynamic Simulation for Efficient Filler-Loading in Papermaking System (제지 공정의 효율적인 충전제 투입에 대한 동적 시뮬레이션 적용)

  • 함충현;윤혜정
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.35 no.3
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    • pp.1-12
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    • 2003
  • The complexity of the papermaking system accelerates interactions between a large number of variables involved. The process operation, therefore, is subject to frequent perturbations by disturbance. Dynamic modelling is a useful tool for characterizing the transient behavior and selecting the best control strategies to reject disturbances. In this study we developed a dynamic simulation model of a fine paper production process, which consists of stock preparation, wire sections, white water circulations, and broke system. It focused on dynamic simulation in its role for developing control strategies and studying control loop dynamics related to filler loading for ash control. The results emphasized the importance of filler-loading position and length of control loop for rapid ash control and process stabilization.

Real-time Spectroscopic Ellipsometry studies of the Effect of Preparation Parameters on the Coalescence Characteristics of Microwave-PECVD Diamond Films

  • Hong, Byungyou
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1998.06a
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    • pp.49-54
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    • 1998
  • The growth of diamond films in plasma enhanced chemical vapor deposition(PECVD) processes requires high substrate temperatures and gas pressures, as well as high-power excitation of the gas source. Thus determining the substrate temperature in this severe environment is a challenge. The issue is a critical one since substrate temperature is a key parameter for understanding and optimizing diamond film growth. The precise Si substrate temperature calibration based on rapid-scanning spectroscopic ellipsometry have been developed and utilized. Using the true temperature of the top 200 ${\AA}$ of the Si substrate under diamond growth conditions, real time spectroellipsometry (RTSE) has been performed during the nucleation and growth of nanocrystallind thin films prepared by PECVD. RTSE shows that a significant volume fraction of nondiamond(or{{{{ {sp }^{2 } -bonded}}}}) carbon forms during thin film coalescence and is trapped near the substrate interface between ∼300 ${\AA}$ diamond nuclei.

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Preparation of Si-SiC Composites by Si-Infiltration (Si 침윤에 의한 Si-SiC 복합체 제조)

  • 김인술;장주민;오기동;박홍채
    • Journal of the Korean Ceramic Society
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    • v.29 no.9
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    • pp.750-756
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    • 1992
  • Reaction bonded si-SiC composites were prepared by silicon infiltration technique at temperature of 1$600^{\circ}C$ for 30 minutes in vaccum atmosphere. The microstructure and mechanical properties of Si-SiC composites were investigated and characterized. UF-15 and SE-10 as SiC powders, phenolic resin and carbon black as carbon source, and metallic silicon powder as molten Si source were used as starting materials. New SiC crystallines nucleatd and grown by reaction of Si and C were detected by TEM and SEM-EDS. The bonding between new and original SiC was found to be strong. But the wetting of SiC by unreacted metallic Si and the rapid grain growth of new SiC decreased density and fracture toughness. Fracture toughness and modulus of rupture of Si-SiC composite were about 3.2 MPa.m1/2 and 480 MPa, respectively.

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Measurement of Indoor Air Quality in a Kindergarten (유치원내 실내공기환경 측정)

  • Kim, Yun-Deok;Lim, Soo-Young
    • Journal of the Korean Institute of Educational Facilities
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    • v.14 no.1
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    • pp.52-57
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    • 2007
  • Kindergarten children are engaged in the age of physical immaturity as well as the rapid growth. The indoor air contaminants that are proved to affect even the full grown adults are obvious to have no little influence to immature small children in a growth period. In May 2004, for the multi purpose facilities and newly constructed apartments, the Ministry of Environment announced "Indoor Air Quality Control Law for the Multi Purpose Facility," which made the interests to be focused in the urgent understanding of current condition and preparation of measures about the indoor air pollution. In Dec 2005, the law was revised to obligatorily notify the amount of Formaldehyde and Volatile Organic Compounds in the case of newly constructed apartments with more than 100 houses. However, since the kindergarten takes none of the classifications, even the current condition is not grasped although it is directly connected to the health of growing children. Therefore, the study aims to analyze indoor air pollution of one selected kindergarten in Incheon city.

Preparation of $\delta$-FeOOH by Coprecipitation Method and Its Magnetic Properties (공침법에 의한 $\delta$-FeOOH의 제조 및 자기 특성)

  • 김성재;김태옥
    • Journal of the Korean Ceramic Society
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    • v.33 no.3
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    • pp.327-331
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    • 1996
  • $\delta$-FeOOH was prepared by rapid oxidation method of Fe(OH)2 using H2O2. The effects of reaction temperature and mole ratio ([OH-]/[Fe2+])의 몰비를 제조 변수로 하여 최종 생성된 $\delta$-FeOOH의 입자크기 입자형태, 자기특성을 조사하였다. Fe(OH)2 의 반응온도 및 [OH-]/[Fe2+] 비가 $\delta$-FeOOH의 입자크기 및 형상에 많은 영향을 미침을 알수 있었으며 입자 크기는 이 두인자에 비례하여 증가하였다 Fe(OH)2 의 반응온도가 4$0^{\circ}C$ [OH-]/[Fe2+]=5 Fe(OH)2 숙성 시간 2시간에서 제조된 $\delta$-FeOOH를 TEM, VSM으로 입자의 크기 및 자기특성을 조사한결과 평균 입경이 630$\AA$ 정도이고 입도 분포가 양호하였으며 포화자화 및 보자력은 각각 20.8emu/g 210 Oe였다.

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Role of estrogen and RAS signaling in repeated implantation failure

  • Hong, Kwonho;Choi, Youngsok
    • BMB Reports
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    • v.51 no.5
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    • pp.225-229
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    • 2018
  • In humans, hormonal regulation is crucial for the preparation of uterine environment leading to either successful implantation or menstrual cycle. Estrogen is a pivotal female steroid hormone that regulates the uterine dynamics along with progesterone in the estrous and menstrual cycles in humans. Estrogen signals act via nuclear estrogen receptor or membrane-bound receptor. The membrane-bound estrogen receptor plays a crucial role in the rapid response of estrogen in the uterine epithelium. Recently, RASD1 has received attention as a novel signal transducer of estrogen in various systems including female reproductive organs. In this review, we discuss the regulation of estrogen and RASD1 signaling in the uterus and also provide insights into RAS as a novel signaling molecule in repeated implantation failure.

Preparation and Properties of PVDF Multilayer Film

  • Han, Fei-Fei;Son, Tea-Won
    • Proceedings of the Korean Society of Dyers and Finishers Conference
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    • 2009.03a
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    • pp.118-119
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    • 2009
  • As the rapid development of the electronics, the demand for portable electronics and wireless sensors is growing faster, also with the increased needs of one material which can power it automatically, and then power the electrical devices. The piezoelectric effect of the PVDF material can be used for this. So in this paper, PVDF multilayer films were made for this aim. Make the PVDF / DMAc solution in the 10% concentration; use the spin coater technique to make films with the optimum process parameters: the spin rate is 1260rpm; the spin time is 70s; the dry temperature is 100$^{\circ}C$; the dry time is 30mins. And also, for obtaining the higher $\beta$-phase crystallinity, put the Ca(NH3)2.4H2O into the PVDF / DMAc solution system.

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A Study on the Preparation of Modified Belite Cement Using Converter Slag (전로슬래그를 이용한 Modified Belite Cement의 제조에 관한 연구)

  • 박종옥;김승진;박홍수;신현택
    • Journal of the Korean Ceramic Society
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    • v.32 no.8
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    • pp.873-880
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    • 1995
  • In order to prepare the modified belite (C2S-C4A3S-C4AF-CS) cement with low energy, clinkers were synthesized by converter slag, limestone, gypsum and clay. The synthesized clinkers were characterized and the hydration processes were investigated by XRD, SEM and microconduction calorimetry. The hydrates were mainly C-S-H and ettringite. The needle-like ettringite formed by the hydration of C4A3S at the early stage of hydration was filled in the inner vacant spaces of the hardened body and it might contribute to the rapid-hardening phenomena. The hardened body became stronger due to the hydration of C2S at the later period. The compressive strengths of the cement-3 mortars hydrated for 3, 7 and 28 days were 115, 128 and 211 Kgf/$\textrm{cm}^2$, respectively.

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A Study on the Architectural Planning for Lifelong Education in Elementary School (평생교육을 고려한 초등학교 건축계획에 관한 연구 - 국외의 복합화 사례를 중심으로 -)

  • Lee, Jae-Kook;Oh, Byeong-Uk
    • Journal of The Korean Digital Architecture Interior Association
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    • v.9 no.1
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    • pp.41-48
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    • 2009
  • Entering the 21st century, countries throughout the world are turning the direction of their education to be consumer-oriented and reinforcing lifelong education in preparation for the rapid advance of science and technology and the globalization, opening and informatization of the world. With the reinforcement of consumer-oriented education and lifelong education, the role of school is emphasized as a ground for lifelong education in community and efforts are being made to use schools and community facilities compositely so that schools may play the role of central facilities in community. Accordingly, the objective of this study is to analyze the relation between lifelong education and school facilities in the educational aspect, and to suggest a basic architectural direction so that schools may play central roles for social, cultural, educational, welfare, and sport activities in community.

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