• Title/Summary/Keyword: rapid extraction

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Determination of Vitamin C in Chewing Gum Using Extraction by Tetrahydrofuran (테트라하이드로퓨란에 의한 추출방법을 이용한 츄잉검의 비타민 C 정량)

  • Roh, Hoe-Jin;Kim, Pil;Park, Cheon-Ho;Lee, Kee-Jung;Noh, Bong-Soo;Choi, Jin-Hwan
    • Korean Journal of Food Science and Technology
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    • v.31 no.6
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    • pp.1484-1487
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    • 1999
  • Extraction is the most important and tedious step to determine water-soluble vitamin C in water-insoluble chewing gum. For the rapid determination of vitamin C in chewing gum, a new method of dispersion in tetrahydrofuran(THF) was performed. Vitamin C was easily extracted from gum base using THF The content of vitamin C in chewing gum was rapidly quantified with high reliability by an enzymatic method using a chewing gum sample dispersed in tetrahydrofuran.

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A Study on the 3-D Digital Modelling of the Sea Bottom Topography (3차원 해저지형 수치모델에 관한 연구)

  • 양승윤;김정훈;김병준;김경섭
    • Journal of the Korea Institute of Military Science and Technology
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    • v.5 no.2
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    • pp.50-61
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    • 2002
  • In this study, 3-dimensional virtual visualization was performed for a rapid and accurate analysis of sea bottom topography, The visualization was done through the extracted data using the developed program and the generated data using the gridding method. The data extraction program was developed with AutoLISP programming language and this program was able to extract the needed sample bathymetry data from the electronic sea chart systematically as well as effectively. The gridded bathymetry data were generated by the interpolation or extrapolation method from the spatially-irregular sample data. As the result of realization for the 3-dimensional virtual visualization, it was shown a proper feasibility in the analysis of the sea bottom topography to determine the route of submarine cable burial.

Robust Real-time Intrusion Detection System

  • Kim, Byung-Joo;Kim, Il-Kon
    • Journal of Information Processing Systems
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    • v.1 no.1 s.1
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    • pp.9-13
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    • 2005
  • Computer security has become a critical issue with the rapid development of business and other transaction systems over the Internet. The application of artificial intelligence, machine learning and data mining techniques to intrusion detection systems has been increasing recently. But most research is focused on improving the classification performance of a classifier. Selecting important features from input data leads to simplification of the problem, and faster and more accurate detection rates. Thus selecting important features is an important issue in intrusion detection. Another issue in intrusion detection is that most of the intrusion detection systems are performed by off-line and it is not a suitable method for a real-time intrusion detection system. In this paper, we develop the real-time intrusion detection system, which combines an on-line feature extraction method with the Least Squares Support Vector Machine classifier. Applying the proposed system to KDD CUP 99 data, experimental results show that it has a remarkable feature extraction and classification performance compared to existing off-line intrusion detection systems.

Solvent Extraction, Preconcentration and Determination of Thorium with Monoaza 18-Crown-6 Derivative

  • Dolak, I.;Karakaplan, M.;Ziyadanogullar, B.;Ziyadanogullari, R.
    • Bulletin of the Korean Chemical Society
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    • v.32 no.5
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    • pp.1564-1568
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    • 2011
  • A solvent extraction separation, preconcentration and determination of thorium with a new crown, 2-ethyl-N-benzyl-4,7,10,13,16-pentaoxa-1-azacyclooctadecane (MACE), is described in the study. The amount of thorium in the aqueous phase and organic phase was determined by Inductively Coupled Plasma-Optical Emission Spectroscopy and Ultraviolet-Visible, respectively. Thorium loaded organic phase was quantitatively stripped in a stage by using 1.0 M $HNO_3$. Thorium was effectively extracted with MACE in the pH range of 6-7 to produce a 3:2 complex ratio in the chloroform. A highly sensitive and rapid spectrophotometric method was described for determination of trace amounts of thorium with MACE. The effective molar absorption coefficient at 281 nm is $1.98{\times}10^3\;mol^{-1}cm^{-1}$, and the system complies with Beer's law in the range from 0.464 to 2.32 ${\mu}gm\;L^{-1}$ of thorium. Thorium was also determined in standard and environmental samples.

Sinus floor augmentation at the time of tooth removal (상악 구치부의 발치와 동시에 시행하는 상악동저 증강술을 이용한 임프란트 증례)

  • Kim, Min-Kue;Jin, Min-Ju;Ahn, Eun-Joo
    • Journal of Periodontal and Implant Science
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    • v.37 no.3
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    • pp.647-653
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    • 2007
  • Rapid crestal bone resorption following maxillary tooth loss is further accentuated in the posterior regions because of pneumatization and enlargement of the maxillary sinuses. A treatment rationale that allows preservation and augmentation of vertical available bone at the time of posterior maxil-lary tooth extraction may offer numerous therapeutic benefits which are more short courses of ther-apy and no needs of additional surgical augmentation. The present study comprised 3 patients who had 4 posterior maxillary teeth with no evident bone between the tooth apex and sinus floor, as estimated through preoperative radiographic analysis. Sinus floor augmentation at the time of tooth extraction was chosen for the ltreatment of these patients. After the tooth was carefully extracted, the empty alveolus was thoroughly debrided and a trephine approach was performed. Particulated autogenous bone was gently pushed beyond the empty alveolus to elevate the sinus membrane using an osteotome. The distance between bone crest and si-nus floor was radiographically estimated 4 months after the first procedure. Another procedure was then carried out to place the implants of 11 mm length without another augmentation procedure. All implant were clinically stable, with no sign of infection. The presented surgical procedure performed at the time of extraction of posterior maxillary teeth in close proximity to the sinus floor allowed placement of implants of proper length.

Immediate Autogenous Fresh Demineralized Tooth (Auto-FDT) Graft for Alveolar Bone Reconstruction (즉시 탈회 치아이식재를 사용한 치조골 재건술)

  • Lee, Eun-Young
    • The Journal of the Korean dental association
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    • v.54 no.5
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    • pp.348-355
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    • 2016
  • Ideal autogenous or allogenic bone graft materials should provide 1) stabilization of blood clot, 2) scaffolds for cellular proliferation and differentiation, 3) release of osteogenic growth factors, 4) appropriate resorption profile for remodeling of new bone. Teeth, especially dentin, mostly contain hydroxyapatite and type I collagen which are similar to bone, and could be valuable graft material. Clinically teeth are used as calcined or demineralized forms. Demineralized form of dentin can be more effective as a graft material. But a conventional decalcification method takes time and long treatment time may give negative effects to various osteogenic proteins in dentin. Author used a new clinical method to prepare autogenous teeth, which could be grafted into the removal defects immediately after extraction using vacuum ultrasonic system. The process could be finished within two hours regardless of the form (powder, chip or block). Teeth were processed to graft materials in block, chip, or powder types immediately after extraction. It took 120 minutes to prepare block types and 40 minutes to prepare powder. Clinical cases did not show any adverse response and the healing was favorable. Rapid preparation of autogenous teeth with the vacuum ultrasonic system could make the immediate one-day extraction and graft possible.

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Urban Road Extraction from Aerial Photo by Linking Method

  • Yang, Sung-Chul;Han, Dong-Yeo;Kim, Min-Suk;Kim, Yong-Il
    • Korean Journal of Geomatics
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    • v.3 no.1
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    • pp.67-72
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    • 2003
  • We have seen rapid changes in road systems and networks in urban areas due to fast urbanization and increased traffic demands. As a result, many researchers have put greater importance on extraction, correction and updating of information about road systems. Also, by using the various data on road systems and its condition, we can manage our road more efficiently and economically. Furthermore, such information can be used as input for digital map and GIS analysis. In this research, we used a high resolution aerial photo of the roads in Seongnam area. First, we applied the top-hat filter to the area of interest so that the road markings could be extracted in an efficient manner. The lane separation lines were selected, considering the shape similarity between the selected lane separation line and reference data. Next, we extracted the roads in the urban area using the aforementioned road marking. Using this technique, we could easily extract roads in urban area in semi-automatic way.

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Screening procedure for organochlorinated pesticide residues in meat fat using a matrix solid phase dispersion(MSPD) extraction and GC/ECD (MSPD법과 GC/ECD를 이용한 식육중의 잔류농약 분석)

  • 백미순;이영철;박병옥;김창수;박유순
    • Korean Journal of Veterinary Service
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    • v.22 no.1
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    • pp.15-23
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    • 1999
  • A multiresidue, simple and rapid isolation technique known as matrix-solid phase dispersoin (MSPD) for the extraction and quantitative gas chromatographic/electron capture detection (GC/ECD) determination of 14 organochlorinated pesticides($\alpha$-BHC, ($\beta$-BHC, ($\gamma$-BHC, aldrin, dieldrin, endrin, heptachlor, ($\alpha$-endosulfan, ($\beta$-endosulfan, endosulfan sulfate, p,p'-DDE, o,p'-DDD, p,p'-DDD, p,p'-DDT) from meat fats. The 14 pesticide were fortified into meat fat(0.5g) and blend with 2g $C_{18}$, $C_{18}$meat fat matrix blend and 2g activated florisil comprise an extraction column from which the pesticides are eluted by adding 8ml acetonitrile. Then 2${\mu}\ell$ of the eluate is analyzed by GC/ECD. Unfortified blank controls are tested similarly. The eluate contained all the pesticide analytes and was free of interfering coextractants. Recovery rate(31.3-500ng/g) were ranged from 80$\pm$4% to 97$\pm$4%. Any organochlorinated pesticides were not detected in 120 samples of beef and pork collected from slaughter houses in Kyeonggi province.

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Identification of Salmonella spp. from porcine salmonellosis by matrix-assisted laser desorption ionization-time of flight mass spectrometry

  • Yang, Hyoung-Seok;Kim, Jae-Hoon
    • Korean Journal of Veterinary Service
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    • v.41 no.2
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    • pp.105-110
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    • 2018
  • A total of 41 Salmonella (S.) strains were isolated from pigs suffered with severe watery diarrhea and were tried to identify by both matrix-assisted laser desorption ionization-time of flight mass spectrometry (MALDI-TOF MS) and polymerase chain reaction (PCR) analysis. Fibrinous exudate and ulceration in the large intestine were prevalent in gross observation, and variable degrees of enteritis were observed in the histology of large intestines. Subsequent polymerase chain reaction (PCR) analyses demonstrated that 41 strains were identified as S. Typhimurium (39 strains), though 2 stains were failed to identify. Further identification was performed using both direct smear and protein extraction method by MALDI-TOF MS analyses. In terms of extraction methods, 100% (41/41) of isolates were identified to species level of S. spp. Whereas only 43.9% (18/41) were identified to species level using the direct method. These results thus suggest that rapid and accurate diagnosis of porcine salmonellosis can be guaranteed by MALDI-TOF MS combined with protein extraction method.