• Title/Summary/Keyword: quartz crystal microbalance

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Performance Evaluation of Explosive Specific Bio-receptor Using QCM Sensing Platform for Resonance Frequency Shift Detection (공진점변화검출용 QCM 센싱플랫폼을 이용한 폭발물 특이적 바이오수용체 성능평가)

  • Lim, Si-Hyung;Jeong, Hyun-Jin
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.21 no.3
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    • pp.280-284
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    • 2011
  • The mass change during the molecular interaction between explosive specific bio-receptors and target molecules has been measured using quartz crystal microbalance(QCM), which has a mass change detection limit up to ~ng/$cm^2$. The environmental effect on the molecular interaction has been evaluated. In the liquid phase molecular interaction experiments, the high selectivity of the bio-receptor to DNT compared with toluene has been shown and the sensitivity for various concentrations of DNT has been demonstrated.

On-Line Measurement of Solid Particles in Air Using a Quartz Crystal Microbalance (수정진동자 미량저울을 이용한 공기 중 먼지의 온라인 측정)

  • Choi, Kwang-Jae;Kim, Young-Han;Chang, Sang-Mok
    • Journal of Sensor Science and Technology
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    • v.8 no.4
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    • pp.314-319
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    • 1999
  • The measurement of solid particles suspended in air is conducted with a quartz crystal microbalance. The measurement system is connected to a personal computer and multiple sensors are utilized to make simultaneous measurement possible. In this paper, the detail of experimental setup is extensively explained for the possible future application of the system in other areas. It is found that the measurement system is suitable for an on-line continuous determination of the concentration of solid particles in air.

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Quartz crystal Microbalance(QCM)-based Immunosensor for the Determination of LDL(Low-Density Lipoprotein)

  • Kim, Sang-Hyun;Yoon, Hyun-Chul;Kwak, Joo-Won;Kim, Hak-sung
    • Proceedings of the Korean Biophysical Society Conference
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    • 1996.07a
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    • pp.44-44
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    • 1996
  • Immunoserisor for the determination of LDL(Low-Density Lipoprotein) was developed by using quartz crystal microbalance(QCM) system. LDL is known to be a good indicator for the diagnosis of atherosclerosis and hypercholesterolemia. The immunosensor consists of four parts; detection cell, oscillating circuit, oscilloscope, and frequency counter, and this was interfaced with personal computer for signal processing. (omitted)

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Hydrogen Absorption Characteristics of Al/Pd Film (Al/Pd 박막의 수소 흡수 특성)

  • Cho, Young-Sin
    • Transactions of the Korean hydrogen and new energy society
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    • v.17 no.2
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    • pp.234-240
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    • 2006
  • Al film(135.5 nm thick) with Pd film(39.6 nm thick) on the top of it was made by thermal evaporation method. Hydrogen absorption of Al/Pd film was measured by quartz crystal microbalance(QCM) method at room temperature. The sample was activated by hydrogen absorption and desorption cycling at room temperature. Hydrogen was introduced into the film by increasing hydrogen gas pressure step by step up to 640 torr at room temperature. Hydrogen concentration reached up to 25% at $5{\sim}10$ torr. But at high pressure the concentration decreased. This strange tendency was not understood yet. Further study is needed to find out the mechanism of hydrogen absorption in Al in Al/Pd film.

Optimization of Quartz Crystal Microbalance-Precipitation Sensor Measuring Acetylcholinesterase Activity

  • Kim, Nam-Soo;Park, In-Seon;Kim, Dong-Kyung
    • Journal of Microbiology and Biotechnology
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    • v.16 no.10
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    • pp.1523-1528
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    • 2006
  • The optimization of a batch-type quartz crystal microbalance (QCM)-precipitation sensor measuring acetylcholinesterase (AChE) activity was conducted. To covalently bind AChE onto the gold electrode of a QCM surface, glutaraldehyde cross-linking to a cystamine self-assembled monolayer was tried at different cystamine concentrations. At the optimum conditions of the QCM-precipitation sensor, 0.1 M potassium phosphate buffer (pH 8.0), containing 0.01% Tween 80, was used as the reaction buffer, with the enzyme amount of 5 units for immobilization and the substrate concentration of 50 mg/ml. The current biosensor might find a future applicability to the sum parameter detection on organophosphorus and carbamate pesticides.

Study on Morphology Investigation and Electron-Transfer Property of Self-Assembled Viologen Monolayers (자기조립된 Viologen 단분자막의 모폴로지 관찰과 전하이동 특성 연구)

  • Lee, Dong-Yun;Park, Sang-Hyun;Kwon, Young-Soo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.07a
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    • pp.395-396
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    • 2005
  • We fabricated self-assembled monolayers(SAMs) onto quartz crystal microbalance(QCM) using viologen, which has been widely used as electron acceptor and electron transfer mediator. We determined the time dependence to resonant frequency shift during self-assembly process and observed the morphology of self-assembled mono layers by STM and investigated the electrochemical behavior of SAMs by cyclic voltammetry. Electrochemical deposition of viologen was investigated using electrochemical quartz crystal microbalance(EQCM). The redox reactions of viologen were highly reversible and the EQCM has been employed to monitor the electrochemically induced adsorption of SAMs during the redox reactions.

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Characterization of Surface Films Formed Prior to Bulk Reduction of Lithium in Rigorously Dried Propylene Carbonate Solutions

  • Chang, Seok Gyun;Lee, Hyo Jung;Gang, Heon;Park, Su Mun
    • Bulletin of the Korean Chemical Society
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    • v.22 no.5
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    • pp.481-487
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    • 2001
  • Surface films formed prior to bulk reduction of lithium have been studied at gold, platinum, and copper electrodes in rigorously dried propylene carbonate solutions using electrochemical quartz crystal microbalance (EQCM) and secondary ion mass spectrometry experiments. The results indicate that the passive film formation takes place at a potential as positive as about 2.0 V vs. Li/Li+ , and the passive film thus formed in this potential region is thicker than a monolayer. Quantitative analysis of the EQCM results indicates that electrogenerated lithium reacts with solvent molecules to produce a passive film consisting of lithium carbonate and other compounds of larger molecular weights. The presence of lithium carbonate is verified by SIMS, whereas the lithium compounds of low molecular weights, including lithium hydroxide and oxide, are not detected. Further lithium reduction takes place underneath the passive film at potentials lower than 1.2 V with a voltammetric current peak at about 0.6 V.

Resistance and Frequency Properties Analysis of QCM Coated with LB Films (LB막이 누적된 QCM의 저항 및 주파수 특성해석)

  • 강현욱;진철남;김정명;권명수
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1997.11a
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    • pp.465-467
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    • 1997
  • The oscillating properties of quartz Crystal Microbalance(QCM) were analyzed by electrical measurement. We tried to analyze the properties of quartz crystal coated with Langmuir-Bladgett(LB) films using the frequency and resistance at resonance in the electrical equivalent circuit. The resonant frequency was decreased linearly as to layers of LB films, however, there are some gap between theoretical values, Sauerbrey's equation and experimental values. The resistance was increase nonlinearly as to layers.

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