• 제목/요약/키워드: quality control(QC)

검색결과 179건 처리시간 0.024초

해양퇴적물내 다환방향족탄화수소 분석을 위한 표준작업절차서 제안 (Proposal of Standard Method for the Analysis of Polycyclic Aromatic Hydrocarbons in Marine Sediments)

  • 이효진;김기범;최윤석
    • 한국해양환경ㆍ에너지학회지
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    • 제14권3호
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    • pp.163-175
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    • 2011
  • 현재 국내의 수많은 연구기관과 대학에서 다양한 화학분석법과 기기를 이용하여 다환방향족탄화수소(polycyclic aromatic hydrocarbons, PAHs)자료를 산출해 내고 있으나, 자료에 대한 엄격한 정도관리가 이루어지지 않은 관계로 자료를 산출한 상대 기관에 대한 신뢰가 부족하고, 농도에 대한 절대 비교가 불가능한 경우가 많았다. 그러므로 본 연구에서는 최신의 분석방법으로 국내외학술지 및 연구보고서에 게재되어진 20여 편의 참고문헌으로부터 보편적으로 받아들여지는 분석방법과 자료질을 조사하여 이를 반영한 표준작업 절차서를 제시하였다. 이 절차서에 따라 표준물질 첨가법으로 회수율을 검정하였을 때 좋은 회수율 값을 보여주었다. 또한 PAHs 분석하고 있는 기존의 연구 기관들의 경우 굳이 실험법을 바꾸지 않더라도 표준시료의 사용 등 환경정도관리를 통해 산출되어진 자료가 신뢰성을 획득할 수 있는 방안을 절차서 내에 포함하였다.

GC/MS를 이용한 소변 중 대마 대사체 분석의 측정불확도 평가 (Uncertainty Evaluation of the Analysis of 11-Nor-9-carboxy-${\Delta}^9$-tetrahydrocannabinol in Human Urine by GC/MS)

  • 김진영;정재철;서승일;서용준;이정직;김종상;인문교
    • 약학회지
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    • 제52권6호
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    • pp.480-487
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    • 2008
  • We described an estimation of measurement uncertainty in quantitative analysis of 11-nor-9-carboxy-${\Delta}^9$-tetrahydrocannabinol (THCCOOH), the major metabolite of ${\Delta}^9$-tetrahydrocannabinol, in urine sample by solid-phase extraction (SPE) and GC/MS detection. The analytical results were compared and the different contributions to the uncertainty were evaluated. Inter-day and inter-person validation were performed using statistical analysis of several indicative factors. Measurement uncertainty associated with target analyte in real forensic samples was estimated using quality control (QC) data. Traceability of measurement was established through traceable standards, calibrated volumetric glassware and volume measuring device. The major factors of contribution to combined standard uncertainty, were calibration linearity, inter-day repeatability and inter-person reproducibility, while those associated with preparation of analytical standards and sampling volume were not so important considering the degree of contribution. Relative combined standard uncertainties associated with the described method was 12.05% for THCCOOH.

초음파 의료영상에서 ATS 535H 팬텀을 이용한 해상력 특성 평가 (Evaluation of the Resolution Characteristics by Using ATS 535H Phantom for Ultrasound Medical Imaging)

  • 민정환;정회원;강혜경
    • 대한방사선기술학회지:방사선기술과학
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    • 제46권1호
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    • pp.15-21
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    • 2023
  • This study was purpose to assessment of the resolution characteristics by using ATS 535H Basic quality assurance (QA) phantom for ultrasound. The ultrasound equipment was used Logiq P6 (Ultrasound, GE Healthcare System, Chicago, IL, USA). And the ultrasound transducer were used Convex 4C (4~5.5 MHz), Linear 11L (10~13 MHz), Sector 3SP (3~5.5 MHz) probe. As for the noise power spectrum (NPS) comparison results by using ATS 535H Basic QA ultrasound phantom and Convex 4C, Linear 11L, Sector 3SP probe. The NPS value of the Convex 4C probe image was 0.0049, Linear 11L probe image was 0.0049, Sector 3SP probe image was 0.1422 when the frequency is 1.0 mm-1. The modulation transfer function (MTF) comparison results by using ATS 535H Basic QA ultrasound phantom and Linear 11L probe the MTF value of the 3 cm focus image was 0.7511 and 4 cm focus image was 0.9001 when the frequency is 1.0 mm-1. This study was presented characteristics of spatial resolution a quantitative evaluation methods by using ultrasound medical images for QA of ultrasound medical QA phantom. The quality control (QC) for equipment maintenance can be efficiently used in the clinic due to the quantitative evaluation of the NPS and MTF as the standard methods. It is meaningful in that it is applied mutatis mutandis and presented the results of physical resolution characteristics of the ultrasound medical image.

EPR/알라닌 선량계를 이용한 치료용 선형가속기 정도관리 활용 연구 (Research on the use of Therapeutic Linear accelerator Quality Control using EPR/alanine Dosimeter)

  • 김윤하;김효진;강영록;이동연
    • 한국방사선학회논문지
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    • 제18권3호
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    • pp.239-248
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    • 2024
  • 방사선치료는 고에너지를 사용함으로 인체에 부작용이 발생할 수 있다. 이에 따라 적정 선량의 설정과 발생장치에서 만들어진 방사선에 대한 신뢰도를 확보하는 것이 중요하다. EPR/알라닌 선량평가는 물 동등성, 선량 응답 선형성과 낮은 페이딩 등의 장점이 있으므로 방사선치료 장비의 품질관리에서 유용하게 사용될 것으로 생각한다. 따라서 본 연구에서는 선형가속기 6 MV 에너지를 활용하여 알라닌의 질량에 따른 EPR/알라닌 선량평가의 신호와 선량반응곡선을 비교하였다. 조사된 알라닌 선량계의 EPR 신호를 통해 선량반응곡선과 1차 회귀방정식을 제작하였다. 이를 통해 질량에 따른 신호 크기와 선량반응곡선을 비교하고 선량반응곡선 측정 불확도를 통해 신뢰도를 확인하였다. 그 결과, 질량이 커짐에 따른 EPR 신호의 크기는 64.5 mg 기준으로 약 1.3배 증가하며, 선량반응곡선의 민감도도 커지는 것을 알 수 있었다. 측정 불확도는 5.84 ~ 8.93 % (신뢰구간 약 95 %, k=2)로 평가되었다. 본 연구를 통해 선형가속기의 품질보증과 품질관리에 EPR/알라닌 선량평가 시스템이 적용 가능할 것으로 생각된다.

품질관리관행과 중소기업 성과간의 관계에 대한 연구: 조직내 맥락적 양면성의 매개효과 검증을 중심으로 (The Quality Circle, SMEs' Performance, and Mediating Role of Organizational Ambidexterity)

  • 이순옥;이재훈;조효비
    • 벤처창업연구
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    • 제12권3호
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    • pp.163-176
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    • 2017
  • 4차 산업혁명과 창조경제라는 화두가 지배하고 있는 오늘날의 경영환경하에서 중소기업들은 지속가능한 성장을 위하여 혁신역량 확보에 많은 노력을 기울이고 있다. 특히 혁신역량 혹은 혁신성과를 창출하기 위하여 중소기업들은 조직의 양면적 특징, 즉 탐색과 활용이라는 양면성에 관심을 기울이고 있다. 이에 본 연구에서는 국내 중소기업들을 대상으로 혁신성과를 창출할 수 있는 핵심 요소로서 조직의 맥락적 양면성을 고찰하고 이들 양면성을 자극하고 촉진하는 요인과 혁신성과간의 관계를 발견하기 위하여 실증분석을 실시하였다. 이를 위해 조직내 맥락적 양면성의 선행요인으로 대표적 경영혁신 기법이자 전사적 차원의 혁신 활동인 품질관리관행을 채택하였으며, 양면성의 결과변수로 혁신성과(급진적/점진적 제품혁신)을 설정하여, 일련의 회귀분석을 실시하였다. 연구 결과, 품질관리관행인 품질분임조활동은 조직의 두 가지 맥락적 양면성 즉, 탐색과 활용 모두에 정(+)의 영향을 미치는 것으로 나타났으며, 맥락적 양면성은 혁신성과에도 정(+)의 영향을 미치는 것으로 나타났다. 그리고 맥락적 양면성은 품질분임조활동과 혁신성과간의 관계를 완전매개하고 있는 것으로 나타났다. 이상의 연구결과는 중소기업의 혁신성과를 달성하기 위해서는 맥락적 양면성의 확보가 필수적이며, 맥락적 양면성을 촉진 또는 자극하기 위해서는 품질분임조와 같은 품질관리활동이 반드시 선행되어야 함을 시사하고 있다.

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현장측정에 기초한 대기오염물질의 측정방식에 대한 비교연구-주요 기준성 오염물질을 중심으로 (Evaluation of Analytical Techniques for Some Gaseous Criteria Pollutants through a Field Measurement Campaign in Seoul, Korea)

  • 김세웅;김기현;김진석;이강웅;김경렬;문동민;김필수;손동헌
    • 한국대기환경학회지
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    • 제15권4호
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    • pp.403-415
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    • 1999
  • To properly assess air pollution levels, application of quality assurance and quality control(QA/QC) is believed to be an essential step. In order to cope with such scientific principle, a field study was designed with an aim of comparing: 1) the methods of calibration for airborne pollutants and 2) the protocols developed for their measurements. Measurements were made at Han Yang University, Seoul during 29 May through 1 June 1998 under the management of the Division of Measurements and Analysis(DMA) of Korean Society for Atmospheric Environment(KOSAE). In this work, we report our results of intercomparative measurements on several gaseous criteria pollutants that were investigated mainly by the two institutes-Seoul National University(SNU) and the Korean Research Institute for Standards and Science(KRISS). Although measurements of major gaseous pollutants had been made routinely by many scientific institutes and organizations in Korea, most scientists involved in those studieswere obliged to do their experiments on the basis of their own procedural steps spaning from the preparation of gaseous standards to the methodological selections for the calibration. Hence, this campaign offered a unique opportunity to examine many important aspects on the measurements of these important gaseous pollutants. In the course of our study, we investigated the compatibility of data sets obtained by the two institutes in concert with reference data sets collected concurrently from a government-managed monitoring station. On the basis of our study, we conclude that different data sets made by different participants during this campaign agree well within the reasonable range of uncertainties.low, which indicated that during this period the potential acidity of precipitation was high but the neutralizing capacity was low. For Spring, pAi was very low but pH was slightly high. This was likely due to the large amount of $CaCO_3$ in the soil particles transported over a long range from the Chinese continent that were incorporated into the precipitation, and then neutralized the acidifying species with its high concentraton.

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연안준설 및 준설토 해양투기 해양환경평가 개선방안 (Improvement of the Marine Environmental Assessment for Dredging and Ocean Disposal of Coastal Sediment in Korea)

  • 이대인;박달수;엄기혁;김귀영;조현서;김종규;서영교;백근욱
    • 환경영향평가
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    • 제18권3호
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    • pp.131-141
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    • 2009
  • We studied improvement in marine environmental impact assessment and related management systems of coastal sediments that are dredged inshore but disposed offshore. After reviewing and diagnosing the existing assessment procedures and problems, we recommend to design the core assessment items and improve the reliability of assessment byenhancing the quality assurance/quality control (QA/QC) and verification processes. We proposed eco-friendly disposal plan for dredging sediment such as reuse system in land development was explored. A marine environmental database system was established to support the assessment processes. Guidelines for marine research and modelling were proposed for improving assessment of dredging and disposal of coastal sediment. Also, applying of screening and scoping for marine environmental assessment was reviewed.

민간환경감시활동을 통한 환경교육 (Citizen Volunteer Monitoring as a Tool for Environmental Education)

  • 강성현;김은희;신종원
    • 한국환경교육학회지:환경교육
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    • 제10권2호
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    • pp.311-324
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    • 1997
  • General citizens can be a valuable resource for various types of environmental monitoring when they are well-trained and managed. Successful use of volunteer monitors depends on understanding that citizens are partners sharing expanded roles as the guardians of their local environment. Citizen volunteer monitoring programs are developed for three reasons: 1) to supplement environmental data collected by professional staffs in governmental agencies and scientific institutions; 2) to educate the public about local environmental problems; 3) to build a constituency of citizen to practice sound environmental management at a local level and build public support for environmental protection. All three goals can be achieved with a well-organized program which provides useful and credible data. Initial step in planning a successful volunteer monitoring project is to clearly identify the use to be made of the data. Technical advice from the identified potential user groups should be convened early in the planning stage to refine the program objectives and determine if volunteers can provide the level of expertise required. Data users must have confidence in the representativeness, consistency, and accuracy of data collected by volunteers. Effective quality assurance and quality control(QA/QC) procedures are essential to ensure the utility of environmental monitoring data. Volunteers must be trained in advance to carry out specific environmental monitoring tasks. Another components of successful volunteer monitoring programs is to give the volunteers praise and feedback as well as to encourage experienced volunteers to impose increased responsibilities. The increase of volunteer monitoring programs in Korea will play a major role in developing a participatory system in which the people are "empowered" to make decisions and make a difference.

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대기 중 다환방향족탄화수소 측정방법의 성능평가 - 하이볼륨 샘플링 및 GC/MS 분석방법을 대상으로 (Evaluation of a Method for the Measurement of PAHs in the Ambient Atmosphere - Focusing on High Volume Sampling and GC/MS Analysis)

  • 서영교;박대권;백성옥
    • 한국환경보건학회지
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    • 제35권4호
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    • pp.322-333
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    • 2009
  • In this study, a measurement method was evaluated for the determination of polycyclic aromatic hydrocarbons (PAHs) in the ambient atmosphere. PAHs were sampled by high-volume samplers, and were then analysed with a GC/MS system. Particulate PAHs were collected on $8"{\times}10"$ quartz fiber filter, while vapor phase PAHs were adsorbed on polyurethane foam (PUF). Target compounds included a total of 36 PAHs, which are known to be frequently detected in the urban atmosphere. It was not necessary to clean-up samples before samples were analyzed using GC/MS, and the overall performance of the method was tested by a variety of quality control and quality assurance schemes. It is generally known that the clean-up procedure can negatively affect the recovery of samples. Precision and accuracy was evaluated using SRM provided by US NIST, and the results were generally satisfactory and reliable. However, the GC/MS method appeared not to be adequate for 6-rings PAHs, such as coronene, due to its lower sensitivity. In addition, collection efficiencies for low molecular compounds, such as 2-rings PAHs, were poor because of the lower retention volume of the PUF adsorbent. As a result, it was concluded that the method based on high-volume sampling and GC/MS analysis can give very reliable data by simultaneous sampling of both particulate and vapor phases for 3-rings to 5-rings PAHs of environmental concern.

브롬화 난연제의 환경오염도 관리 방안 (Monitoring of Brominated Flame Retardants (BFRs) for the management of Their Contamination in Environments)

  • 김용범;이상훈;정용
    • 환경영향평가
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    • 제14권2호
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    • pp.83-96
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    • 2005
  • Brominated flame retardants have the market share of 40%, comparing others because of their low cost and highly effective retardation against the flame. However, their toxic effects in human and properties of the accumulation in the environments have been issued among the international organization such as EU, OECD and etc. It, therefore, was surveyed the classification, toxic effects, and the usage of Brominated flame retardants, the trends for their managements in the world and Korea, and their contaminated levels in Korean Peninsula. In addition, the management directions for them were proposed. Penta, octa, and deca-BDE among brominated retardants will seem to be prohibited by the regulation as a flame retardants for plastics in Europe because of their toxic effects. Although Penta and Octa BDEs was used marginally in Korea, deca-BDE was 27% of brominated flame retardants (49,050 ton) which had been used in 2002. However, risk assessment for brominated retardants might not launched in Korea, yet. These reports demonstrate that toxic brominated retardants such as PBDEs will be assessed for their usage and the level of contamination in the environment in the area of the point sources like the industrial areas, incinerators and etc. However, the law to regulate the hazardous chemicals seems not to be dictated the monitoring of their contamination in the environment. We, therefore, suggest how to evaluate and to monitor the toxic contaminants with EIA (Environmental Impact Assessment) and LCA (Life Cycle Assessment) system. Further, to establish the management system of BFRs (such as the monitering of contamination levels in environments, life cycle assessment, and risk assessment for the toxic chemicals), It can be recommended the law to deal with the method analyzing chemicals will be established, which contains QA/QC (Quality Assurance and Quality Control) to evaluate the analytic capability of the companies to prepare EIS (Environment Impact Statement) or other institutes for analyzing chemicals.