• Title/Summary/Keyword: pulping temperature

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Bagasse Pulping by Using Caro's Acid

  • Youself, Hussein-Abou
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.33 no.5
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    • pp.30-36
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    • 2001
  • Caro's acid (persulphuric acid) has been proposed as a promising reagent used in pulping of lignocellu-losic materials. Bagass was subjected to caro's acid pulping under different pulping conditions of per acid concentration (2~8 percent), pulping temperatures (40~$60^{\circ}C$) and pulping time (120~240 min). The influence of different parameters of caro's acid pulping process on the chemical and strength properties of the produced pulps had been studied. Peracid concentration and pulping temperature are the most important variables of the pulping process. High degree of delignification and good deliberation were achieved at moderate pulping conditions in the studied range. Pulping experiments of bagasse by using caro's acid had been carried out for determination of the optimum comditions of the process. In inch case to effectively tackle the problem, a specific design of an experiment is selected depending on the goals to be achieved in the experimentation. The study could enable us to excepect the bagasse pulp properties (yield, Kappa number, DP) that be stated as function of the independent variables of caro's acid pulping process (per acid concentration, pulping temperature and pulping time).

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Studies on Seasonal Variation of Linerboard Strength (I) - Effect of Pulping Temperature of OCC on Strength- (계절에 따른 골판지 원지의 강도변화에 대한 연구 (1) - OCC의 해리온도가 강도에 미치는 영향 -)

  • Lee, Kwang Seob;Pak, Yell Rim;O, Jun;Jo, Woo Sang;Jo, Ik Jeong;Ryu, Jeong Yong
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.48 no.3
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    • pp.91-98
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    • 2016
  • Linerboards have been produced by recycling recovered paper such as old corrugated containers(OCC). Usually linerboards produced during summer season show weak strength compared with those of produced during winter. In order to cope with the weak strength of linerboards produced during summer, and to confirm uniform quality, it is important to understand the seasonal effect on strength properties. Effect of pulping temperature of the OCC for linearboard production was investigated by controlling pulping temperatures at $18^{\circ}C$ and $51^{\circ}C$. Low pulping temperature ($18^{\circ}C$) caused more generation of fines in stock. Consequently retention and drainage of linerboard defibrated at high pulping temperature ($51^{\circ}C$) were better than those of $18^{\circ}C$. Strength properties of handsheet at low pulping temperature were higher than those of high pulping temperature and it could be confirmed that low pulping temperature during winter is one reason of seasonal variation of recycled linerboard strength. It is considered that surface modification of OCC fibers by harsh pulping action during winter caused increase of paper strength.

Effects of Pulping Conditions in the Reconstituted Tobacco Sheet Making Process on the Properties of the Pulp Slurry (판상엽 펄퍼 운전 조건에 따른 펄핑특성 변화)

  • Sung, Yong-Joo;Han, Young-Lim;Kim, Kun-Soo;Rhee, Moon-Soo;Ha, In-Ho;Lee, Ki-Yeul;Lee, Young-Eh;Kim, You-Choul
    • Journal of the Korean Society of Tobacco Science
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    • v.28 no.2
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    • pp.117-123
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    • 2006
  • The pulping process in a papermaking process for a reconstituted tobacco sheet (RECON) was evaluated. For the practical information, the experiments were conducted in a real mill. Two pulping conditions were chosen and changed depending on the feasibility, such as the pulping temperature and the properties of pulping water. The higher pulping temperature resulted in the easier dissolution of solubles from the raw materials. However, the efficiency of screw press process was decreased by the higher pulping temperature, which resulted in the reduction of the HWS and the concentration in the #1 screw press filtrate. The addition of SEL(Strong extracted liquor) to pulper affected the efficiency of dissolution and the final concentration of #1 screw press filtrate. Although the higher SEL resulted in the less dissolution of the solubles from the raw materials, the concentration of the #1 screw press filtrate was greatly increased by the higher addition of SEL, which could provide much better efficiency to the following evaporation process of the filtrate and could increase the whole productivity.

Study of Rice Husk Pulping for utilization of Rice Husk Fiber (왕겨섬유 활용을 위한 왕겨 펄프화 연구)

  • Oh, Min-Taek;Sun, Yong-Joo
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.44 no.3
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    • pp.63-69
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    • 2012
  • The rice husk is one of the major agricultural residue in KOREA. In this paper, the effects of various pulping conditions on the properties of rice husk pulp and handsheets made of rice husk fiber were evaluated in order to utilize the rice husk as an alternative source for wood pulp. Two typical alkali pulping, such as soda pulping and Kraft pulping were applied with various conditions of the pulping processes. The higher effective alkali and higher pulping temperature resulted in the higher efficiency in removal of lignin and ash, which leaded to the higher strength properties of handsheets made of rice husk fiber, but the lower yield of rice husk pulp. The better efficiency in production of rice husk pulp and the stronger handsheets were obtained by the Kraft pulping.

Neutral Deinking of Photocopied Papers with Nonionic Surfactants (비이온 계면활성제를 이용한 복사고지의 중성탈묵)

  • 정영재;이학래
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.33 no.2
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    • pp.58-67
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    • 2001
  • MOW (Mixed Office Waste) mainly consisted of photocopied paper is being recycled to produce tissue or fine paper products. Toner particles that are fused and set on paper surface in photocopying process turns into large and plate-shaped particles after repulping which prevents them to be removed effectively in flotation deinking. The immediate purpose of this study is to find the effective deinking technology that increases the recycling potential of photocopied papers for manufacturing tissue and fine paper products. In this study the effects of pulping temperature and the type of hydrophobic groups of nonionic surfactants on the deinking efficiency of photocopied paper has been investigated. Particle size distribution of the toner particles after pulping and flotation, brightness, yield and ash removal were investigated. The size of toner particles after pulping increased as the pulping temperature was increased. When pulping at the low temperature finer toner particles were generated, however, greater amount of toner particles was found to attach to the fiber. When the pulping temperature was greater than Tg of the toner, the amount of coarse hairy particles increased. When nonionic surfactants with a double bond in hydrophobic groups were used, toner removal efficiency, brightness and ash removal were increased. As the addition level of surfactant was increased, yield decreased rather sharply without improving brightness.

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Delignification Kinetics of Trema orientalis (Nalita) in Kraft Pulping

  • Jahan, M. Sarwar;Rubaiyat, A.;Sabina, R.
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.39 no.5
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    • pp.7-11
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    • 2007
  • Kraft pulping of Trema orientalis (Nalita) was studied in order to find kinetic data for delignification. Pulping runs were carried out in the temperature range of $160-180\;^{\circ}C$ under constant and well-defined conditions. The delignification was found to be first order with respect to residual lignin and was chemically controlled. The rate of delignification reaction was increased 1.11-1.23 for $10\;^{\circ}C$ temperature increase in the range of $160-180\;^{\circ}C$ range. A mean value of 93% of lignin was removed at the transition between bulk and residual delignification. The influence of cooking temperature on the rate constant was expressed by an Arrhenius-type equation. The obtained activation energy of the delignification reaction was 6,164 cal/mol. The transition point between bulk and residual phase was shifted to lower lignin and carbohydrate yield with the increase of temperature.

Impact of hexeneuronic acid to kappa number determination in hardwood chemical pulps (활엽수 화학 펄프내 잔류 hexeneuronic acid가 카파 값에 미치는 영향)

  • Shin, Soo-Jeong;Sung, Yong-Joo;Park, Jong-Moon
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.42 no.2
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    • pp.35-40
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    • 2010
  • Variations in hexeneuronic acid content in hardwood alkaline pulps were investigated to evaluate their contribution to kappa number. Out of diverse chemical pulps the highest hexeneuronic acid content were measured in yellow poplar kraft pulping, which was assumed to enhance ca. 7.0 of kappa number determined by acid permanganate consumption. In yellow poplar soda-anthraquinone pulping, hexeneuornic acid was contributed to increment of 5.0-6.0 kappa number. In eucalyptus alkaline pulping, hexeneuronic acid content was not significantly different from soda-anthraquinone pulping. Increment of Kappa number by hexeneuronic acid was 4.5-5.6 depending on pulping method and pulping time at target temperature.

Studies on the Pulping Conditions of Separating Useful Components from Disposable Diaper Waste (폐 일회용 기저귀의 유용 성분 회수를 위한 해리조건 연구)

  • Lee, Tai-Ju;Choi, Do-Chim;Nam, Yun-Seok;Jo, Jun-Hyung;Lee, Ho-Seon;Ryu, Jeong-Yong
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.47 no.2
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    • pp.1-8
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    • 2015
  • Disposable diaper has been used in order to handle urine and feces conveniently. At present the amount of disposable diaper waste increases gradually. Incineration and landfill have been the only ways to dispose of disposable diapers. However, if they are disposed by landfill, decomposition will take more than one hundred years. In addition, another way of dispose incineration has caused air pollution. Therefore, it is necessary to study recycling process for disposable diaper since plastic and wood fibers of diaper are useful materials to recycle. In this study, pulping condition of disposable diaper waste was studied in order to effectively separate the components. Recovery rates of plastic and fibers were analyzed under different pulping conditions. It was found that optimum pulping consistency was 5%, time was 60 minutes, temperature was $50^{\circ}C$, and cut size is $21cm{\times}21cm$. The recovery rate of plastic and fibers can be achieved above 70% under the optimum pulping condition.

Kraft Pulping of Sapwood-A Sawmill Waste

  • Jahant M. Sarwar;Chowdhury D.A. Nasima;Islam M. Khalidul;Mun Sung Phil
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.37 no.5 s.113
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    • pp.41-49
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    • 2005
  • This paper deals the effect of anthraquinone (AQ) on the contribution of sulphidity in kraft pulping of sapwood. The pulping conditions namely- active alkali concentration, pulpingtime, temperature and liquor ratio were varied in low ($15\%$) and high ($30\%$) sulphidity. $0.1\%$ AQ was added in the low and high sulphidity pulping with varying active alkali concentration and cooking time. At optimum conditions, low sulphidity kraft process produced about $44\%$ pulp yield with kappa number of about 23. But in high sulphidity kraft process kappa number was reduced to about 20 at the same yield. An addition of AQ reduced alkali requirement by $2\%$ on oven dried raw material and cooking time by 1 hour to produce pulp yield of about $44\%$ at kappa number 20. AQ is more effective in low sulphidity pulping than the high sulphidity pulping. The breaking length of kraft-AQ pulp was slightly higher than that of kraft pulp.

Nitric-Acid Pulping of Municipal Wastepapers and its Spent-Liquor Utilization for Fertilizers(I) -Study on the Nitric-Acid Pulping Conditions of OCC Pulp- (도시 폐휴지의 질산 펄프제조와 펄프폐액의 입상 비료화 기술개발(I) -폐골판지 상자(OCC)의 질산 펄프제조 조건-)

  • 임기표;위승곤;김창래;양정훈
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.32 no.4
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    • pp.74-80
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    • 2000
  • A series of studies on nitric-acid pulping of municipal recycled waste papers were carried out to substitute the bleached chemical pulp imported for producing printing paper as well as to use its solidified spent-liquor as fertilizer. The first experiment was carried out to find the optimum treatment conditions such as pulp consistency, nitric acid charge and temperature in $HNO_3$-alkali pulping process. The results obtained were as follows: 1. Some selective delignification of OCC pulp was conducted by $HNO_3$-alkali process. The higher the temperature and concentration of nitric acid, the lower the pulp yield and kappa number of treated pulp. while its brightness was increased. 2. The higher consistency required the stronger mixing in case of more than 5% pulp. 3. In the laboratory, the suitable $HNO_3$-treating condition seemed to be less than 6% consistency, lower than 500% $HNO_3$charge on pulp and lower than $100^{\circ}C$ in cooking temperature. 4. The spent liquor with 1.77% N-content seemed to be slow-release nitrogen fertilizer suitable for agriculture.

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