• Title/Summary/Keyword: pulp consistency

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Studies on the Pulping Characteristics of Larchwood (Larix leptolepis Gordon) by Alkaline Process with Additives (첨가제(添加劑) 알칼리 법(法)에 의한 일본 잎갈 나무의 펄프화(化) 특성(特性)에 관(關)한 연구(硏究))

  • Lim, Kie-Pyo;Shin, Dong-Sho
    • Journal of the Korean Wood Science and Technology
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    • v.7 no.2
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    • pp.3-30
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    • 1979
  • Larch ($\underline{Larix}$ $\underline{leptolepis}$ GORDON), one of the major afforestation species in Korea in view of its growing stock and rate of growth, is not favored as a raw material for pulp due to its low yield of pulp and difficulties with bleaching arising from the high content of extractives in wood, and the high heartwood ratio and the active phenolics, respectively. The purpose of this study is to investigate the characteristics of firstly pulping with various additives of cellulose protector for the yield of pulp, and secondly bleaching with oxygen for chlotination-alkali extraction of five stage-sequence to reduce chlorine compounds in bleaching effluents. The kraft cooking liquor for five age groups of larchwood was 18 percent active alkali with 25 percent sulfidity and 5 : 1 liquor-to-wood ratio, and each soda liquor for sap-and heart-wood of the 15-year-old larchwood was 18 percent alkali having one of the following cellulose protectors as the additive; magnesium sulfate ($MgSO_4$, 2.5%), zinc sulfate ($ZnSO_4$, 2.5%), aluminium sulfate ($Al_2(SO_4)_3$, 2.5%), potasium iodide (KI, 2.5%), hydroquinone (HQ, 2.5%), anthraquinone (AQ, 0.1%) and ethylene diamine (EDA, 2.5%). Then each anthraquinone-soda liquor for the determination of suitable cooking condition was the active alkali level of 15, 17 and 19 percent with 1.0, 0.5 and 0.1 percent anthraquinone, respectively. The cooking procedure for the pulps was scheduled to heat to 170$^{\circ}C$ in 90 minutes and to cook 90 minutes at the maximum temperature. The anthraquinone-soda pulps from both heartwood and sapwood of 15-year-old larchwood prepared with 0.5 percent anthraquinone and 18 percent active alkali were bleached in a four-stage sequency of OCED. (O: oxygen bleaching, D: chlorine dioxide bleaching and E: alkali extraction). In the first stage oxygen in atmospheric pressure was applied to a 30 percent consistency of pulp with 0.1 percent magnesium oxide (MgO) and 3, 6, and 9 percent sodium hydroxide on oven dry base, and the bleached results were compared pulps bleached under the conventional CEDED (C: chlorination). The results in the study were summarized as follows: 1. The screened yield of larch kraft pulp did not differ from particular ages to age group, but heartwood ratio, basic density, fiber length and water-extractives contents of wood and the tear factor of the pulp increased with increasing the tree age. The total yield of the pulp decreased. 2. The yield of soda pulp with various chemicals for cellulose protection of the 15-year-old larchwood increased slightly more than that of pure soda pulp and was slightly lower than that of kraft pulp. The influence of cellulose protectors was similar to the yield of pulps from both sapwood and heartwood. The effective protectors among seven additives were KI, $MgSO_4$ and AQ, for which the yields of screened pulp was as high as that of kraft pulp. Considering the additive level of protector, the AQ was the most effective in improving the yield and the quality of pulp. 3. When the amount of AQ increased in soda cooking, the yield and the quality of the pulp increased but rejects in total yield increased with decreasing the amount of active alkali from 19 to 15 percent. The best proportion of the AQ seemed to be 0.5 percent at 17 percent active alkali in anthraquinone-soda pulping. 4. On the bleaching of the AQ-soda pulp at 30 percent consistency with oxygen of atomospheric pressure in the first stage of the ODED sequence, the more caustic soda added, the brighter bleached pulp was obtained, but more lignin-selective bleaching reagent in proportion to the oxygen was necessary to maintain the increased yield with the addition of anthraquinone. 5. In conclusion, the suitable pulping condition for larchwood to improve the yield and quality of the chemical pulp to the level for kraft pulp from conventional process seemed to be. A) the selection of young larchwood to prevent decreasing in yield and quality due to the accumulation extractives in old wood, B) the application of 0.5 percent anthraquinone to the conventional soda cooking of 18 percent active alkali, and followed, C) the bleaching of oxygen in atmospheric pressure on high consistency (30%) with 0.1 percent magnesium oxide in the first stage of the ODED sequence to reduce the content of chlorine compounds in effluent.

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Studies on the Pulping Conditions of Separating Useful Components from Disposable Diaper Waste (폐 일회용 기저귀의 유용 성분 회수를 위한 해리조건 연구)

  • Lee, Tai-Ju;Choi, Do-Chim;Nam, Yun-Seok;Jo, Jun-Hyung;Lee, Ho-Seon;Ryu, Jeong-Yong
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.47 no.2
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    • pp.1-8
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    • 2015
  • Disposable diaper has been used in order to handle urine and feces conveniently. At present the amount of disposable diaper waste increases gradually. Incineration and landfill have been the only ways to dispose of disposable diapers. However, if they are disposed by landfill, decomposition will take more than one hundred years. In addition, another way of dispose incineration has caused air pollution. Therefore, it is necessary to study recycling process for disposable diaper since plastic and wood fibers of diaper are useful materials to recycle. In this study, pulping condition of disposable diaper waste was studied in order to effectively separate the components. Recovery rates of plastic and fibers were analyzed under different pulping conditions. It was found that optimum pulping consistency was 5%, time was 60 minutes, temperature was $50^{\circ}C$, and cut size is $21cm{\times}21cm$. The recovery rate of plastic and fibers can be achieved above 70% under the optimum pulping condition.

The Role of Charge and Retention in Effective Wet end Management

  • Rantala, T.;Nokelainen J.;Ojala, T;Dr. Taina Sopenlehto
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2000.06a
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    • pp.1-10
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    • 2000
  • The development of paper machines, increasing machine speeds with new, mostly low basis weight and/or high ash content paper grades, as well as the fact that several trends regarding process items have increased the sensitivity of papermaking. At the same time, papermakers are looking for flexibility in the production line. We can say that with all PMs the biggest benefits with the lowest capital spending can be achieved by focusing on improved wet end management. In order to manage wet end chemistry on a paper machine, our goal is to control sub-process through which we can influence the operation of the entire wet end with maximum effect. Key measurements and controls are-white water consistency control which is the most effective way to control retention - charge demand measurement and control which takes care of concentration of the anionic material entering to PM -ash measurements and controls which are deeply related to retention and paper quality This paper presents and concentrates to two of these key controls ; retention and charge. The purpose of charge control is to give the process control the tools to react to changes caused by amount of dissolved and colloida material incoming to wet end system. It is called coagulation or fixing control. Retention control is then taking care of retention aid flow to the process by responding any changes seen in white water consistency. It is called flocculation control. Each of these solutions separately , and even more effectively all together, stabilize the wet end operations and so greatly improve the produced paper quality and machine runnability. Practical results will be presented and they are referring to the latest mill cases. We have developed the first wet end measuring system in the late 1980s and control solutions based on this modern measuring technology were completely updated in 1990s. This paper introduces the principle, operation , and results of our unique wet end analyzers (retention and charge ) which are at the level of automation solutions as a part of paper machine quality control Especially our newest member of the platform , on-line charge analyzer has reached and set new standards to the on-line charge monitoring.

The Role of Charge and Retention in Effective Wet End Management

  • Rantala, T.;Nokelainen, J.;Ojala, T.;Sopenlehto, Taina
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.32 no.5
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    • pp.44-53
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    • 2000
  • The development of paper machines, increasing machine speeds with new, mostly low basis weight and/or high ash content paper grades, as well as the fact that several trends regarding process items have increased the sensitivity of papermaking. At the same time, papermakers are looking for flexibility in the production line. We can say that with all PMs, the biggest benefits with the lowest capital spending can be achieved by focusing on improved wet end management. In order to manage wet end chemistry on a paper machine, our goal is to control subprocesses through which we can influence the operation of the entire wet end with maximum effect. Key measurements and controls are - white water consistency control which is the most effective way to control retention. - charge demand measurement and control which takes care of concentration of the anionic material entering to PM. - ash measurements and controls which are deeply related to retention and paper quality. This paper presents and concentrates to two of these key controls: retention and charge. The purpose of charge control is to give the process control the tools to react to changes caused by amount of dissolved and colloidal material incoming to wet end system. It is called coagulation or fixing control. Retention control is then taking care of retention aid flow to the process by responding any changes seen in white water consistency. It is called flocculation control. Each of these solutions separately, and even more effectively all together, stabilize the wet end operations and so greatly improve the produced paper quality and machine runnability. Practical results will be presented and they are referring to the latest mill cases. We have developed the first wet end measuring system in the late 1980s and control solutions based on this modern measuring technology were completely updated in 1990s. This paper introduces the principle, operation, and results of our unique wet end analyzers (retention and charge) which are at the level of automation solutions as a part of paper machine quality control. Especially our newest member of the platform, on-line charge analyzer has reached and set new standards to the on-line charge monitoring.

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Studies on the Asplund Pulping of Wood for Paper Pulp(II) -Effect of some cellulose stabilizers added to the alkaline chip-treatment and the peroxide bleaching on the quality of larchwood asplund pulps- (제지용(製紙用) 아스플룬드펄프 제조(製造)에 관한 연구(II) -일본 잎갈나무��의 알카리 전처리(前處理)와 아스플룬드 펄프의 과산화물(過酸化物) 표백(漂白)에서 셀룰로오스 안정제(安定劑)의 영향(影響)에 관하여-)

  • Lim, Kie-Pyo
    • Journal of the Korean Wood Science and Technology
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    • v.9 no.3
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    • pp.7-15
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    • 1981
  • A Japanese larch has been reforested very much in Korea, but it is not used as a wood resources for paper pulp by now. So this study is carried out to utilize the larchwood for paper pulp manufacture through the Asplund pulping process. The experiment on increasing in the brightness of the pulp is made through the addition of $MgSO_4$, $ZnSO_4$, $Al_2(SO_4)_3$, and KI as a cellulose stabilizer in chip treatment with caustic soda which is followed by high-temperature defibration and conventional peroxide bleaching (5% NaOH plus 2% additive salt per wood in cold pretreatment), or in high-consistency (30%) pulp bleaching of hydrogen peroxide and peracetic acid (100% acitve oxygen per lignin) for conventional one. The results obtained are as follows: 1. The solution of 0.5% additive salts had different pH by the sort of bases that was pH 5.7 in $MgSO_4$, liquor, pH 4.9 for $ZnSO_4$, and pH 2.9 for $Al_2(SO_4)_3$, and in the precepitation of bases which ranged to pH 6-13 for $MgSO_4$, pH 5-12 for $ZnSO_4$, and pH 3-10 for $Al_2(SO_4)_3$. 2. The cellulose stabilizer affective in high-consistency peroxide bleaching was KI, $MgSO_4$, and $ZnSO_4$, but has made a little improvement in de lignification and brightness of pulp in comparison with no addition. 3. The higher alkalinity in the chip treatment has made the higher strength and brightness of larchwood Aspiund pulp instead of downing the pulp yield. And the effective compound for cellulose stabilizer in caustic soda pretreatment of chip was $ZnSO_4$, $Al_2(SO_4)_3$ and KI in order for the conventional peroxide bleaching after Asplund pulping. 4. Therefore, the more effective additives for cellulose stabilization in high-temperature defibration of larchwood suppose to be $ZnSO_4$, $Al_2(SO_4)_3$, and KI, while KI and $MgSO_4$ for peroxide bleaching.

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Analysis of Disintegration Characteristics of OCC (골판지 고지의 해섬 특성 해석)

  • Lee Hak Lae;Youn Hye Jung;Lee Sang Gil;Kang Tae Young;Heo Young Dae
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.36 no.4 s.107
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    • pp.1-8
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    • 2004
  • Linerboards and corrugating mediums are being produced using recycled old corrugated containers (OCC) as major raw materials. The utilization rate of recycled fibers is ex­pected to increase further in the future to reduce raw material cost. Use of recycled fibers as raw materials for linerboard, however, causes many problems for papermakers. As the utilization rate of recycled fiber and number of recycling of fibers increases, quality and process problems including strength reduction and deterioration of machine runn­ability will increase. To overcome the problem of strength reduction associated with the use of recycled fibrous materials for producing quality linerboards, diverse extensive research efforts and new technological approaches have been taken. In this study, disintegration characteristics of aee was evaluated by determining the unslushed contents. The amount of unslushed content of KOCC was lower than AOCC. But contaminants content of KOCC was higher than AOCC. As the consistency in disintegration increased, the amount of unslushed fiber content decreased.

Modification of KOCC with Ultrasonic Wave Treatment (초음파처리에 의한 KOCC의 개질)

  • Ming, He;Lee, Yong-Kyu;Won, Jong Myoung
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.45 no.5
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    • pp.44-48
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    • 2013
  • Ultrasonic treatment of KOCC was tried to explore the possibility for improvement of KOCC quality as a raw material for making industrial packaging paper and paperboard. The effect of pH, stock consistencies and treatment times on the ultrasonic response of KOCC were investigated. WRV, apparent density, tensile index and burst index were improved as pH of KOCC slurry is increased. However highest tear index and stiffness were obtained at pH 8. It was also found that the highest WRV and strength properties could be obtained at 0.5% of KOCC consistency during ultrasonic treatment. WRV and most strength properties were improved with ultrasonic treatment time. It was found that ultrasonic treatment can be used as a useful mean for KOCC modificaton.

Influences of Wet-Pressing Types on Internal Structure of Paper (습부압착 방식이 종이의 내부구조에 미치는 영향)

  • Lee Jin-Ho;Park Jong-Moon
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.37 no.4 s.112
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    • pp.32-37
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    • 2005
  • To Increase the productivity of a paper machine, the maximization of the machine speed is a kind of simple way As the machine speed increases, more intense wet pressing is required to persist the outlet consistency of press part and reduce the water removal of dryer part. With more intense pressing, there are concerns that the quality of paper will be affected. This study was carried out to evaluate the influence of wet-pressing on internal structure of paper, The nip pressure at the first and third nip in triple nip press was controlled. Paper structures, strength properties and pore properties were evaluated. As a result, first nip pressure more strongly influenced the paper structural properties than third nip pressure in triple nip pressing condition. Because of the high water content and low wet-web strength of paper web in first nip, increasing the first nip pressure induced the incipient crushing of wet-web and then caused a potential of web break during the following coating or printing processes.

Filtration characteristic of quantity of coagulant and variable pressure (응집제의 주입량 및 압력변화에 따른 여과특성)

  • Lee, Sung-ho;Lim, Taek-jun;Cho, Jun-hyung
    • Journal of Forest and Environmental Science
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    • v.17 no.1
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    • pp.29-36
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    • 2001
  • Compared to other industries, pulp and paper industry use a lot of water. As a result, a large amount of the waste water is discharged in the pulp and paper industry. This study was investigated to prevent the environmental pollution terribly faced with our society nowadays. In the waste water of pulp and paper, there are so many things in the waste water, like fiber, filler, and other organic solvent etc. so we must remove them from our environment. This study was investigated to experiment on test of impressed filtration with the kind and quantity of coagulant and the variance of pressure. In this study, we used feds, alums. $CaCl_2$, polymer as a coagulant and these pressure was 49, 98, 147, 196kpa. According to this study, we measured the speed of filtration and turbidity, measuring filtrated water. According to the values, we know the fact that as the consistency of coagulant and pressure were high, the filtration was good.

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Strength Property Improvement of OCC-based Paper by Chemical and Mechanical Treatments (II) (골판지 고지의 물리화학적 처리에 의한 강도향상(제2보))

  • Lee, Jong-Hoon;Seo, Yung B.;Jeon, Yang;Lee, Hak-Lae;Shin, Jong-Ho
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.32 no.2
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    • pp.1-7
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    • 2000
  • In the previous experiment, it was found that OCC pre-treatment with Hobart mixer at 20-25% consistency for 3 hrs or more followed by the application of the equal refining time, caused the increase of tensile strength, burst strength, compressive strength and tear resistance, compared to the no pre-treated. Four completely different fibers, which were Hw-BKP, Sw-BKP, White ledger, and OCC were selected for this experiment to investigate the effect of mechanical pre-treatment process on different fibers. From the experiment, it was found that the mechanical pre-treatment did not decrease fiber length at all, but decreased freeness, com-pared to the no pre-treated, when the same refining time was applied. WRVs of the pre-treated fibers were higher than the no pre-treated at the same freeness level. It was speculated that the mechanical pre-treatment induced only hydrophilic nature of fibers without damaging fiber length by delaminating fiber walls. The fiber surface area and the physical strength differences of handsheets will be discussed in the next publication.

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