• Title/Summary/Keyword: processing temperature

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Fabrication of Au Nanoparticle for Au-conjugate Immuno Chemistry Probe (Au-conjugate 면역화학 진단용 금 나노입자 제조)

  • Park, Sung-Tae;Lee, Kwang-Min
    • Korean Journal of Materials Research
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    • v.13 no.8
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    • pp.550-554
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    • 2003
  • Current nanogold cluster synthesized by chemical routine with 11 or 55 atoms of gold has been widely used for immuno chemistry probe as a form of nanocluster conjugated with biomolecules. It would be an undeveloped region that the 1 nm size of nanogold could be made by materials engineering processing. Therefore, objective of this study is to minimize the size of gold nanocluster as a function of operating temperature and chamber pressure in inert gas condensation (IGC) processing. Evaporation temperature was controlled by input current from 50 A to 65 A. Chamber pressure was controlled by argon gas with a range of 0.05 to 2 torr. The gold nanocluster by IGC was evaluated by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The gold nanocluster for TEM analysis was directly sampled with special in-situ method during the processing. Atomic force microscopy (AFM) was used to observe 3-D nanogold layer surfaces on a slide glass for the following biomolecule conjugation step. The size of gold nanoclusters had a close relationship with the processing condition such as evaporation temperature and chamber pressure. The approximately 1 nm size of nanogold was obtained at the processing condition for 1 torr at $1124 ^{\circ}C$.

Effects of Heat Treatment on the Nutritional Quality of Milk: II. Destruction of Microorganisms in Milk by Heat Treatment (우유의 열처리가 우유품질과 영양가에 미치는 영향: II. 열처리에 의한 우유의 미생물 사멸효과)

  • Kim, Kwang-Hyun;Park, Dae Eun;Oh, Sejong
    • Journal of Dairy Science and Biotechnology
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    • v.35 no.1
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    • pp.55-72
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    • 2017
  • The second article of 'Effects of heat treatment on the nutritional quality of milk,' titled 'Destruction of microorganisms in milk by heat treatment' and authored by Dr. Seong Kwan Cha, who worked at the Korea Food Research Institute, covers the heat-stable microorganisms that exist in milk after pasteurization. The article focusses on the microbiological quality of raw milk and market milk following heat treatment, and is divided into four sub-topics: microbiological quality of raw milk, survey and measurement of microorganisms killed in raw milk, effect on psychrophilic and mesophilic microorganisms, and effect of heat treatment methods on thermoduric microorganisms. Bacillus spp. and Clostridium spp. are sporeforming gram-positive organisms commonly found in soil, vegetables, grains, and raw and pasteurized milk that can survive most food processing methods. Since spores cannot be inactivated by LTLT (low temperature long time) or HTST (high temperature short time) milk pasteurization methods, they are often responsible for food poisoning. However, UHT (ultra high temperature) processing completely kills the spores in raw milk by heating it to temperatures above $130^{\circ}C$ for a few seconds, and thus, the UHT method is popularly used for milk processing worldwide.

Forging Process Design by High Temperature Deformation Behavior of the 6061 Aluminum Alloy (자동차 휠용 6061 Al합금의 고온변형거동에 따른 단조성형조건 설계)

  • Lee, Dong-Geun;Lee, Ji Hye;Kim, Jeoung Han;Park, Nho Kwang;Lee, Yongtai;Jeong, Heon-Soo
    • Korean Journal of Metals and Materials
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    • v.46 no.7
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    • pp.449-457
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    • 2008
  • Compression deformation behaviors at high temperature as a function of temperature and strain rate were investigated in the 6061 aluminum alloy, which is used for automobile wheel. Compression tests were carried out in the range of temperatures $300{\sim}475^{\circ}C$ and strain rate $10^{-3}{\sim}10^{-1}sec^{-1}$. By analyzing these results, strain rate sensitivity, deformation temperature sensitivity, the efficiency of power dissipation, Ziegler's instability criterion, etc were calculated, which were plastic deformation instability parameters as suggested by Ziegler, Malas, etc. Furthermore, deformation processing map was drawn by introducing dynamic materials model (DMM) and Ziegler's Continuum Criteria. This processing map was evaluated by relating the deformation instability conditions and the real microstructures. As a result, the optimum forging condition for the automobile wheel with the 6061 aluminum alloy was designed at temperature $450^{\circ}C$, strain rate $1.0{\times}10^{-1}sec^{-1}$. It was also confirmed by DEFORM finite element analysis tool with simulation process.

A Study on the Effect of Ca and P on the Microstructure in Solidification of Al-7wt%Si-0.3wt%Mg Alloy (Al-7wt%Si-0.3wt%Mg 합금의 응고시 미세조직에 미치는 Ca 및 P의 영향에 관한 연구)

  • Kwon, Il-Soo;Kim, Jeong-Ho;Kim, Kyoung-Min;Yoon, Eui-Pak
    • Journal of Korea Foundry Society
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    • v.18 no.4
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    • pp.349-356
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    • 1998
  • In this study, the influence of impurity element Ca, P on solidification behavior and morphology of eutectic silicon was examined by observation of microstructure and by DSC analysis. In the case of 1.3 ppm P, eutectic Si was fine and fibrous when the added amount of Ca was 500 ppm, However, the modification of eutectic Si was depressed by formation of polygonal Ca-Si compounds when the addition amount of Ca was greater than 1000 ppm. The addition of Ca 500 ppm depressed the primary and eutectic temperature. The primary and eutectic temperature were depressed with Ca 500 ppm but rather ascended when the addition amount of Ca was more than 1000 ppm. When the content of P was 17.5 ppm, eutectic Si had modified morphology with Ca addition. DAS was increased, the primary temperature was ascended and eutectic temperature was depressed with Ca added. Eutectic Si appeared as coarse flake phase and DAS was decreased with the increase of P content. The existence of P in the melt depressed the primary temperature and ascended eutectic temperature.

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Development of High-strength, High-temperature Nb-Si-Ti Alloys through Mechanical Alloying (기계적 합금화를 통한 고강도-고내열 Nb-Si-Ti계 합금 개발에 관한 연구)

  • Jung-Joon Kim;Sang-Min Yoon;Deok-Hyun Han;Jongmin Byun;Young-Kyun Kim
    • Journal of Powder Materials
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    • v.31 no.1
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    • pp.30-36
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    • 2024
  • The aerospace and power generation industries have an increasing demand for high-temperature, high-strength materials. However, conventional materials typically lack sufficient fracture toughness and oxidation resistance at high temperatures. This study aims to enhance the high-temperature properties of Nb-Si-Ti alloys through ball milling. To analyze the effects of milling time, the progression of alloying is evaluated on the basis of XRD patterns and the microstructure of alloy powders. Spark plasma sintering (SPS) is employed to produce compacts, with thermodynamic modeling assisting in predicting phase fractions and sintering temperature ranges. The changes in the microstructure and variation in the mechanical properties due to the adjustment of the sintering temperature provide insights into the influence of Nb solid solution, Nb5Si3, and crystallite size within the compacts. By investigating the changes in the mechanical properties through strengthening mechanisms, such as precipitation strengthening, solid solution strengthening, and crystallite refinement, this study aims to verify the applicability of Nb-Si-Ti alloys in advanced material systems.

High Temperature Deformation Behavior of Beta-gamma TiAl Alloy (Beta-gamma TiAl 합금의 고온변형거동)

  • Kim, J.S.;Kim, Y.W.;Lee, C.S.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2006.05a
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    • pp.429-433
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    • 2006
  • High Temperature deformation behavior of newly developed beta-gamma TiAl alloy was investigated in this study. The optimum processing condition was investigated with the aid of Dynamic Materials Model (DMM). Processing maps representing the efficiency of power dissipation for microstructural evolution and instability were constructed utilizing the results of hot compression test at temperatures ranging from $1000^{\circ}C$ to $1200^{\circ}C$ and strain rate ranging from $10^{-4}/s$ to $10^2/s$. The Artificial Neural Network (ANN) simulation was adopted to consider the deformation heating. With the help of processing map and microstructural analysis, the optimum processing condition was presented and the role of $\beta$ phase was also discussed in this study.

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GIS-based Meteorological Data Processing Technology for Forest Fire Danger Rating Forecast System of China

  • Zhao, Yinghui;Zhen, Zhen;Li, Fengri
    • Journal of Korean Society of Forest Science
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    • v.99 no.2
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    • pp.197-203
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    • 2010
  • The data of average temperature, average relative humidity, precipitation and average wind speed were collected from 674 meteorological stations in China. A specific procedure that processes original data into a new data format needed in forest fire danger rating forecast system of China was introduced systematically, and the feasibility of this method was validated in this paper. In addition, a set of meteorological data processing software was constructed by the secondary development of GIS in order to realize automation of processing data for the system. Results showed that the approach preformed well in handling temperature, average relative humidity and average wind speed, and the processing effect of precipitation was acceptable. Moreover, the automated procedure could be achieved by GIS and the working efficiency was about 3 times as much as that of manual handling. The informationization level of processing meteorological data was greatly enhanced.

Sensitivity Analysis of Processing Parameters for the Laser Surface Hardening Treatment by Using the Finite Element Method (유한요소법을 이용한 레이저 표면경화처리 공정변수의 민감도 해석)

  • 이세환;양영수
    • Journal of Welding and Joining
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    • v.19 no.2
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    • pp.228-234
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    • 2001
  • A methodology is developed and used to evaluate the response sensitivity of the thermal systems to variations in their design parameters. Technique for computing the sensitivity of temperature distributions to changes in processing parameters needed to decide the more effective laser input parameters for laser surface hardening treatment is considered. In this study, a state equation governing the heat flow in laser surface treatment is analyzed using a three-dimensional finite element method and sensitivity data of the processing parameter obtained using a direct differentiation method is applied to the sensitivity analysis. The interesting processing parameters are taken as the laser scan velocity and laser beam radius ( $r_{ b}$), and the sensitivities of the temperature T versus v and $r_{b}$ are analyzed. These sensitivity results are obtained with another parameters fixed. To verify the numerical analysis results, hardened layer dimensions (width and depth) of the numerical analysis are compared with the experimental ones.nes.

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High Temperature Deformation Behavior of Al-Zn-Mg-Based New Alloy Using a Dynamic Material Model

  • Jang, Bong Jung;Park, Hyun Soon;Kim, Mok-Soon
    • Metals and materials international
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    • v.24 no.6
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    • pp.1249-1255
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    • 2018
  • High temperature compression tests for newly developed Al-Zn-Mg alloy were carried out to investigate its hot deformation behavior and obtain deformation processing maps. In the compression tests, cylindrical specimens were deformed at high temperatures ($300-500^{\circ}C$) and strain rates of 0.001-1/s. Using the true stress-true strain curves obtained from the compression tests, processing maps were constructed by evaluating the power dissipation efficiency map and flow instability map. The processing map can be divided into three areas according to the microstructures of the deformed specimens: instability area with flow localization, instability area with mixed grains, and stable area with homogeneous grains resulting from continuous dynamic recrystallization (CDRX). The results suggest that the optimal processing conditions for the Al-Zn-Mg alloy are $450^{\circ}C$ and a strain rate of 0.001/s, having a stable area with homogeneous grains resulting from CDRX.

Chemical and Microbiological Quality, Capillary Electrophoresis Pattern, and Rennet Coagulation of UHT-treated and Irradiated Milk

  • Ham, Jun-Sang;Shin, Ji-Hye;Noh, Young-Bae;Jeong, Seok-Geun;Han, Gi-Sung;Chae, Hyun-Seok;Yoo, Young-Mo;Ahn, Jong-Nam;Lee, Wan-Kyu;Jo, Cheo-Run
    • Food Science and Biotechnology
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    • v.17 no.1
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    • pp.58-65
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    • 2008
  • To see the possibility of irradiation as an alternative to ultra high temperature (UHT) sterilization, the quality characteristics of milk were analyzed. Milk treated by UHT ($135^{\circ}C$ for 4 sec) and irradiation at higher than 3 kGy showed no viable counts after 7 days of storage at $4^{\circ}C$. The contents of certain amino acids of milk, such as Arg, Asp, Glu, Ile, Leu, Lys, Pro, Ser, Thr, and Tyr, were lower in irradiated groups at 10 kGy than in UHT-treated one, but no difference was observed between irradiated milks at less than 5 kGy and UHT. The capillary electrophoresis (CE) patterns of the milk irradiated at 10 kGy showed a similar trend to the raw milk, low temperature long time (LTLT, $63^{\circ}C$ for 30 min), and high temperature short time (HTST, $72^{\circ}C$ for 15 sec) treated. However, the CE pattern of UHT-treated milk was different. Rennet coagulation test agreed with the CE results, showing that all milk samples were coagulated by rennet addition except for UHT-treated milk after 1 hr. These results suggest that irradiation of milk reduce the content of individual amino acids but it may not induce severe conformational change at a protein level when compared with UHT treatment.