• 제목/요약/키워드: primary phase

검색결과 1,058건 처리시간 0.027초

Picric Acid에 의한 지방족 아민류와 4급 암모늄 염류의 이온쌍 추출 (Ion Pair Extraction of Aliphatic Amines and Quaternary Ammonium Salts by Picric Acid)

  • 김박광;이종숙;장성기;나운용;옥치환
    • 약학회지
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    • 제35권3호
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    • pp.182-189
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    • 1991
  • Systematic study on the extraction of ion pair by the use of picric acid (PCA) as an ion pair forming reagent to the aliphatic amines has not be done by spectrophotometric method. The extraction of ion pair by the use of PCA and 23 kinds of the aliphatic amines was examined. The procedure is as follows; Elving's buffer solution (pH 1.3~10, ionic strength 0.5) each amine solution, and PCA solution were taken into a test tube. The mixture was shaken mechanically with chlorform. The organic phase was filtered through a filter paper to remove water droplets. The absorbance was examined at $\lambda_{max}$ against a reagent blank. Primary and secondary whose carbon number were more than 7 or 6, respectively, are extractable as ion pairs with PCA, while tertiary amines and quaternary ammonium salts are also extractable without the correlation of carbon number. It was considered that the ion pair extraction of primary and secondary amines was affected by the number of carbon of amines, but its extraction of tertiary amines or quaternary ammonium salts was affected by kind of aliphatic amines rather than pKa values or carbon number of amines.

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Transitional implant를 이용한 임시수복과 최종 수복 (CLINICAL APPLICATION OF TRANSITIONAL IMPLANTS)

  • 김유리;민승기
    • Maxillofacial Plastic and Reconstructive Surgery
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    • 제27권6호
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    • pp.575-580
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    • 2005
  • Transitional implants were developed to support provisional restorations and to allow for load-free osseointegration of conventional implants while a patient was provided with immediate esthetics and function and are usually placed simultaneously at the time of definitive implant placement. Transitional implants are placed in a non-submerged fashion in a single-stage surgery and are designed to be immediately loaded. They generally are made of commercially pure titanium or titanium alloy and are designed as 1-piece implants composed of root and crown replacement segments. Transitional implants can be used in a wide range of indications, such as basic use as temporary implant, to support and protect the primary implants during the healing phase, single crown in the edentulous anterior region of mandibular, anchorage for orthodontic treatment, support a surgical and radiographic template, and primary implant to extremely atrophied alveolar crests of the mandible and maxilla. This article describes the clinical use of transitional implants to support the provisional complete denture and single crown in the restricted edenturous central incisor region of mandible.

A Primary Permanent-Magnet Linear Motor for Urban Rail Transit

  • Cao, Ruiwu;Cheng, Ming;Mi, Chris;Hua, Wei;Zhao, Wenxiang
    • Journal of international Conference on Electrical Machines and Systems
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    • 제1권1호
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    • pp.54-60
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    • 2012
  • In this paper, a new permanent-magnet (PM) linear motor is proposed, in which both the magnets and armature windings are placed in the short mover, while the long stator consists of iron core only. Hence, this new PM linear motor can be called a primary permanent-magnet linear motor. It exhibits the advantages of robustness, low cost, high efficiency, high power factor, and high thrust force density. It is especially suitable for long stator applications such as urban rail transit. In this paper, the topology and operation principle of this motor are discussed in detail. The steady-state characteristics including field distributions, flux-linkage, back-EMF, phase inductance and thrust force are investigated. In addition, the technique of skewing stator teeth is adopted to improve the electromagnetic performance. Results from finite element method (FEM) verified the theoretical analysis results.

Prefilming air blast 연료 노즐의 다상유동 및 반응 유동장 수치해석 (CFD simulation of a prefilming air blast fuel nozzle)

  • 정승채;김신현;박희호;류시양
    • 한국추진공학회:학술대회논문집
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    • 한국추진공학회 2017년도 제48회 춘계학술대회논문집
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    • pp.251-253
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    • 2017
  • Prefilming air blast 연료노즐의 다상유동 해석을 수행하였다. 연료가 미립화되는 과정을 관찰하였으며 liquid film의 두께와 속도를 계산하였다. Slot에서 분사된 연료는 prefilmer surface에서 얇은 액막을 형성한 후 연료노즐 lip에서 액적으로 분열되었다. 또한 계산된 liquid film의 두께와 속도를 경계조건으로 하여 반응유동장 해석을 수행하였다. 분사된 액적은 venturi throat를 지나면서 기화되었고 연료노즐 하류에 반응영역이 형성되어 안정적으로 보염이 이루어졌다.

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EELS and electron diffraction studies on possible bonaccordite crystals in pressurized water reactor fuel CRUD and in oxide films of alloy 600 material

  • Chen, Jiaxin;Lindberg, Fredrik;Wells, Daniel;Bengtsson, Bernt
    • Nuclear Engineering and Technology
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    • 제49권4호
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    • pp.668-674
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    • 2017
  • Experimental verification of boron species in fuel CRUD (Chalk River Unidentified Deposit) would provide essential and important information about the root cause of CRUD-induced power shifts (CIPS). To date, only bonaccordite and elemental boron were reported to exist in fuel CRUD in CIPS-troubled pressurized water reactor (PWR) cores and lithium tetraborate to exist in simulated PWR fuel CRUD from some autoclave tests. We have reevaluated previous analysis of similar threadlike crystals along with examining some similar threadlike crystals from CRUD samples collected from a PWR cycle that had no indications of CIPS. These threadlike crystals have a typical [Ni]/[Fe] atomic ratio of ~2 and similar crystal morphology as the one (bonaccordite) reported previously. In addition to electron diffraction study, we have applied electron energy loss spectroscopy to determine boron content in such a crystal and found a good agreement with that of bonaccordite. Surprisingly, such crystals seem to appear also on corroded surfaces of Alloy 600 that was exposed to simulated PWR primary water with a dissolved hydrogen level of $5mL\;H_2/kg\;H_2O$, but absent when exposed under $75mL\;H_2/kg\;H_2O$ condition. It remains to be verified as to what extent and in which chemical environment this phase would be formed in PWR primary systems.

Assessment of Airborne Microorganisms in a Swine Wastewater Treatment Plant

  • Kim, Ki-Youn;Ko, Han-Jong;Kim, Daekeun
    • Environmental Engineering Research
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    • 제17권4호
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    • pp.211-216
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    • 2012
  • Quantification of the airborne microorganisms (bacteria and fungi) at a swine wastewater treatment plant was performed. Microbial samples were collected at three different phases of the treatment process over a 1-yr period. Cultivation methods based on the viable counts of mesophilic heterotrophic bacteria and fungi were performed. The concentrations of airborne bacteria ranged up to about $5{\times}10^3$ colony-forming unit (CFU)/$m^3$, and those of airborne fungi ranged up to about $9{\times}10^2CFU/m^3$. The primary treatment (e.g., screen, grit removal, and primary sedimentation) was found to be the major source of airborne microorganisms at the site studied, and higher levels of airborne bacteria and fungi were observed in summer. High levels of the respirable bioaerosol (0.65 to $4.7{\mu}m$ in size) were detected in the aeration phase. Among the environmental factors studied, temperature was strongly associated with fungal aerosol generation (with a Spearman correlation coefficient of 0.90 and p-value <0.01). Occupational biorisks are discussed based on the observed field data.

Online Parameter Estimation for Wireless Power Transfer Systems Using the Tangent of the Reflected Impedance Angle

  • Li, Shufan;Liao, Chenglin;Wang, Lifang
    • Journal of Power Electronics
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    • 제18권1호
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    • pp.300-308
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    • 2018
  • An online estimation method for wireless power transfer (WPT) systems is presented without using any measurement of the secondary side or the load. This parameter estimation method can be applied with a controlling strategy that removes both the receiving terminal controller and the wireless communication. This improves the reliability of the system while reducing its costs and size. In a wireless power transfer system with an LCCL impedance matching circuit under a rectifier load, the actual load value, voltage/current and mutual inductance can be reflected through reflected impedance measuring at the primary side. The proposed method can calculate the phase angle tangent value of the secondary loop circuit impedance via the reflected impedance, which is unrelated to the mutual inductance. Then the load value can be determined based on the relationships between the load value and the secondary loop impedance. After that, the mutual inductance and transfer efficiency can be computed. According to the primary side voltage and current, the load voltage and current can also be detected in real-time. Experiments have verified that high estimation accuracy can be achieved with the proposed method. A single-controller based on the proposed parameter estimation method is established to achieve constant current control over a WPT system.

Phenomena Identification and Ranking Table for the APR-1400 Main Steam Line Break

  • Song, J.H.;Chung, B.D.;Jeong, J.J.;Baek, W.P.;Lee, S.Y.;Choi, C.J.;Lee, C.S.;Lee, S.J.;Um, K.S.;Kim, H.G.;Bang, Y.S.
    • Nuclear Engineering and Technology
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    • 제36권5호
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    • pp.388-402
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    • 2004
  • A phenomena identification and ranking table(PIRT) was developed for a main steam line break (MSLB) event for the Advanced Power Reactor-1400 (APR-1400). The selectee event was a double-ended steam line break at full power, with the reactor coolant pump running. The developmental panel selected the fuel performance as the primary safety criterion during the ranking process. The plant design data, the results of the APR-1400 safety analysis, and the results of an additional best-estimate analysis by the MARS computer code were used in the development of the PIRT. The period of the transient was composed of three phases: pre-trip, rapid cool-down, and safety injection. Based on the relative importance to the primary evaluation criterion, the ranking of each system, component, and phenomenon/process was performed for each time phase. Finally, the knowledge-level for each important process for certain components was ranked in terms of existing knowledge. The PIRT can be used as a guide for planning cost-effective experimental programs and for code development efforts, especially for the quantification of those processes and/or phenomena that are highly important, but not well understood.

Zero-Current-Switching in Full-Bridge DC-DC Converters Based on Activity Auxiliary Circuit

  • Chu, Enhui;Lu, Ping;Xu, Chang;Bao, Jianqun
    • Journal of Power Electronics
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    • 제19권2호
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    • pp.353-362
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    • 2019
  • To address the problem of circulating current loss in the traditional zero-current switching (ZCS) full-bridge (FB) DC/DC converter, a ZCS FB DC/DC converter topology and modulation strategy is proposed in this paper. The strategy can achieve ZCS turn on and zero-voltage and zero-current switching (ZVZCS) turn off for the primary switches and realize ZVZCS turn on and zero-voltage switching (ZVS) turn off for the auxiliary switches. Moreover, its resonant circuit power is small. Compared with the traditional phase shift full-bridge converter, the new converter decreases circulating current loss and does not increase the current stress of the primary switches and the voltage stress of the rectifier diodes. The diodes turn off naturally when the current decreases to zero. Thus, neither reverse recovery current nor loss on diodes occurs. In this paper, we analyzed the operating principle, steady-state characteristics and soft-switching conditions and range of the converter in detail. A 740 V/1 kW, 100 kHz experimental prototype was established, verifying the effectiveness of the converter through experimental results.

일체화된 삼상 자속구속형 고온초전도 전류제한기의 사고각에 따른 전류제한 특성 분석 (Analysis of Current Limiting Characteristics According to Fault Angles in Integrated Three-Phase Flux-Lock Type Superconducting Fault Current Limiting)

  • 박충렬;두호익;임성우;현옥배;임성훈;박형민;조용선;남긍현;이나영;최효상;한병성
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2006년도 하계학술대회 논문집 Vol.7
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    • pp.255-256
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    • 2006
  • In this paper, we investigated the. characteristics of fault current limiting according to fault angle in the integrated three-phase flux-lock type SFCL in fault types such as the single-line-to-ground fault, the double-line-to-ground fault and the three-line-to-ground fault. When the SFCL is operating under normal condition, the magnetic flux generated between primary and secondary coils of each single phase is canceled out perfectly, so that the impedance of the SFCL is also not generated and the power system can be operated normally without any loss, However, if a fault occurs even in any phase out of three phases, quench happened in SFCL elements and the current flowing secondary coil is restricted abruptly. Finally, the balance of magnetic flux in whole SFCL system is destroyed, and the fault currents in every phase could be limited at the same time irrespective of the fault types. As a result, the developed SFCL in this study were operated normally as expected and the purpose of the integration of 3 phase current limiting was also achieved successfully. However, the fault current limiting characteristics of the SFCL was dependant on the quench characteristics of HTSC elements in each phase, and it was expected that the improvement of the SFCL could be possible through the introduction of HTSC elements which have better critical characteristics.

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