• 제목/요약/키워드: primary phase

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TiFe 공정합금의 미소합금 첨가에 따른 미세구조 변화 및 기계적 물성 (Influence of Minor Element on Microstructure and Mechanical Properties of TiFe Ultrafine Eutectic Alloys)

  • 이찬호;조재혁;문상철;김정태;여은진;김기범
    • 한국재료학회지
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    • 제22권11호
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    • pp.615-619
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    • 2012
  • Recently, ultrafine grained (ufg, typically 100 > d > 500 nm) Ti-Fe eutectic materials have been highlighted due to their extraordinarily high strength and good abrasion resistance compared to conventional coarse grained (cg, d > $1{\mu}m$) materials. However, these materials exhibit limited plastic strain and toughness during room temperature deformation due to highly localized shear strain. Several approaches have been extensively studied to overcome such drawbacks, such as the addition of minor elements (Sn, Nb, Co, etc.). In this paper, we have investigated the influence of the addition of Gd and Y contents (0.3-1.0 at.%) into the binary Ti-Fe eutectic alloy. Gd and Y are chosen due to their immiscibility with Ti. Microstructural investigation reveals that the Gd phase forms in the eutectic matrix and the Gd phase size increases with increasing Gd content. The improvement of the mechanical properties is possibly correlated to the precipitation hardening. On the other hand, in the case of Ti-Fe-Y alloys, with increasing Y contents, primary phases form and lamellar spacing increases compared to the case of the eutectic alloy. Investigation of the mechanical properties reveals that the plasticity of the Ti-Fe-Y alloys is gradually improved, without a reduction of strength. These results suggest that the enhancement of the mechanical properties is closely related to the formation of the primary phase.

Mechanical Properties and Castabilities of Al-12Mg-5.5Zn-xSi Alloys

  • Kim, Jeong-Min;Sung, Ki-Dug;Jun, Joong-Hwan;Kim, Ki-Tae;Jung, Woon-Jae
    • 한국주조공학회지
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    • 제24권6호
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    • pp.340-346
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    • 2004
  • 초정 $Mg_2Si$와 미세한 $MgZn_2$ 석출상을 갖는 고강도 내마모 Al합금을 개발하기 이하여 Al-l2wt%Mg-5.5wt%Zn합금에 0-5wt%까지 Si을 첨가 시켰으며, 미세조직 및 기계적 성질에 미치는 영향을 조사하였다. Si의 함량이 증가함에 따라 형성되는 $Mg_2Si$상의 양이 증가하였으며, 동시에 고강선 온도가 점차적으로 증가함에 따라 효과적인 열처리가 가능해지는 것을 관찰할 수 있었다. 5wt%Si이 첨가된 합금의 경우 적절한 열처리를 통해 미세한 $MgZn_2$ 석출상이 기지에 균일하게 분포한 미세조직을 얻을 수 있었고 이를 통해 인장강도를 현저하게 증가시킬 수 있었다. 또한 Si이 첨가된 Al-Mg-Zn합금은 유동도 및 열간 균열저항성과 같은 주조성면에서도 다른 고강도 Al합금에 비하여 월등히 우수한 것으로 나타났다.

Induction of Differentiation of the Cultured Rat Mammary Epithelial Cells by Triterpene Acids

  • Paik, Kee-Joo;Jeon, Seong-Sill;Chung, Hae-Young;Lee, Kyung-Hee;Kim, Kyu-Won;Chung, Joon-Ki;Kim, Nam-Deuk
    • Archives of Pharmacal Research
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    • 제21권4호
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    • pp.398-405
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    • 1998
  • We investigated the effects of triterpene acids (TAs), ursolic acid (UA) and oleanolic acid (OA), on the induction of proliferation and differentiation of normal rat mammary epithelial cells (RMEC) or organoids cultured in Matrigel or primary culture system. To elucidate the effects, we tested their differentiation inducing activities with intercellular communication ability, cell cycle patterns, induction of apoptosis, and morphological differentiation in the three dimensional extracellular culture system. To study the changes of RMEC subpopulation in culture, the cultured cells were isolated, immunostained with peanut lectin (PNA) and anti-Thy-1.1 antibody and then analyzed with flow cytometry. Four different subpopulations, such as PNA and Thy-1.1 negative cells (B-), PNA positive cells (PNA+), Thy-1.1 positive cells (Thy-1.1+), PNA and Thy-1.1 positive cells (B+), were obtained and the size of each subpopulation was changed in culture with time in the presence of TAs. Intercellular communication was observed in culture for 7 days in TAs-treated cells, but not in culture for 4 days with scrape-loading dye transfer technique. $G_2$/M phase cells and the number of apoptotic population were increased in TAs-treated groups in cell cycle analyses. S phase fractions were reduced and the change of $G_1$ phase cells was not observed. The colonies with distinct multicelfular structures, such as stellate, ductal, webbed, squamous, lobulo-ductal colonies, were observed in Matrigel culture and the frequencies of each colony were changed in the presence of TAs. These results suggest that UA and OA have differentiation inducing effects on rat mammary epithelial cells in primary or in Matrigel culture.

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화학실험실 사고 Data를 이용한 근본원인분석 Map 개발 및 원인 분석 (Cause Analysis and Development of Root Cause Analysis Map using Data of Chemical Laboratory Accidents)

  • 이수경;윤여송;엄석화
    • 한국가스학회지
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    • 제18권4호
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    • pp.86-94
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    • 2014
  • 화학실험실 사고의 근본원인분석 Map을 개발하기 위하여 석유화학 사고 근본원인분석 Map을 참고하여 3단계 사고 요인 트리(Tree)로 구성된 Map을 작성하였다. 원인 인자 도표(Cause Factor Charting) 방식을 적용하여 실험실 사건 사고 211건을 1~5단계까지 사고 원인을 조사하고, 그 사고의 원인을 EXCEL 프로그램에 입력하였다. 그 후, 그 사고요인들을 유형과 각 단계별로 분류하여, 근본원인분석 Map 초안(draft)을 작성하였다. 또한, 연구실 사건 사고 211건의 근본원인이 근본원인분석 Map초안에 적절한지 재확인하였다. 향후 실험실에서 발생할 수 있는 사고의 원인들을 보완함으로써, 화학실험실에 관한 RCA Map이 개발되었다. 본 연구에서 제시한 근본원인분석 Map을 기반으로 발생빈도를 고려하여 사고 원인을 1~5단계로 나누어 분석한 결과, 3단계 원인은 관리시스템 35.%, 모니터링 12.2%, Human Factor Eng. 15.1%, 교육훈련 12.1% 등의 순으로 나타났다.

다상유동 분리기 모듈화를 위한 유입구 형상 설계에 관한 수치해석적 연구 (Numerical Study on the Inlet Head Configuration of Multi-Phase Separator for Modularization)

  • 홍창기;김윤제
    • 대한기계학회논문집B
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    • 제41권9호
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    • pp.571-577
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    • 2017
  • 본 연구는 수치해석 기법을 활용하여 오일샌드 플랜트에 사용되는 다상유동분리기의 다양한 유입구 형상에 따른 효율 분석에 관한 연구이다. 본 연구에 사용된 유수분리기(FWKO, Free-water knockout)는 유량 $15,89m^3/d$(100 bbl/d), SOR(Steam-to-Oil Ratio) 3.5의 값을 가지며 Stokes 이론을 기반으로 설계되었다. 모듈화를 위하여 두 개의 유수분리기를 병렬 연결하였고 이에 따른 유입구 형상 최적화를 수행하였다. 유입구를 통해 유입되는 비투멘 에멀젼은 $150^{\circ}C$, 50 bar이며, API는 17의 값을 갖는다. 유수분리공정의 평균체류시간은 물과 오일이 95% 분리되는 시간으로 정의하였다. 다상유동의 밀도차에 의한 중력분리과정을 모사하기 위하여 유한체적법(VOF, Volume Of Fluid)과 상차분모델(DPM, Discrete Phase Model)을 조합하여 활용하였으며 준과도(Pseudo-transient) 해석기법을 활용하였다.

Performance Analysis of Opportunistic Spectrum Access Protocol for Multi-Channel Cognitive Radio Networks

  • Kim, Kyung Jae;Kwak, Kyung Sup;Choi, Bong Dae
    • Journal of Communications and Networks
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    • 제15권1호
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    • pp.77-86
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    • 2013
  • Cognitive radio (CR) has emerged as one of effective methods to enhance the utilization of existing radio spectrum. Main principle of CR is that secondary users (SUs) are allowed to use the spectrum unused by primary users (PUs) without interfering PU's transmissions. In this paper, PUs operate on a slot-by-slot basis and SUs try to exploit the slots unused by PUs. We propose OSA protocols in the single channel and we propose an opportunistic spectrum access (OSA) protocols in the multi-channel cognitive radio networks with one control channel and several licensed channels where a slot is divided into contention phase and transmission phase. A slot is divided into reporting phase, contention phase and transmission phase. The reporting phase plays a role of finding idle channels unused by PUs and the contention phase plays a role of selecting a SU who will send packets in the data transmission phase. One SU is selected by carrier sense multiple access / collision avoidance (CSMA/CA) with request to send / clear to send (RTS/CTS) mechanism on control channel and the SU is allowed to occupy all remaining part of all idle channels during the current slot. For mathematical analysis, first we deal with the single-channel case and we model the proposed OSA media access control (MAC) protocol by three-dimensional discrete time Markov chain (DTMC) whose one-step transition probability matrix has a special structure so as to apply the censored Markov chain method to obtain the steady state distribution.We obtain the throughput and the distribution of access delay. Next we deal with the multi-channel case and obtain the throughput and the distribution of access delay by using results of single-channel case. In numerical results, our mathematical analysis is verified by simulations and we give numerical results on throughput and access delay of the proposed MAC protocol. Finally, we find the maximum allowable number of SUs satisfying the requirements on throughput and access delay.

Modeling the Catalytic Activity and Kinetics of Lipase(Glycerol-Ester Hydrolase)

  • Demirer, Goksel N.;Duran, Metin;Tanner, Robert D.
    • Biotechnology and Bioprocess Engineering:BBE
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    • 제1권1호
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    • pp.46-50
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    • 1996
  • In order to design industrial scale reactors and proceises for multi-phase biocatalytic reactions, it is essential to understand the mechanisms by which such systems operate. To il-lustrate how such mechanisms can be modeled, the hydrolysis of the primary ester groups of triglycerides to produce fatty acids and monoglycerides by lipased (glycerol-ester hydrolase) catalysis has been selected as an example of multiphase biocatalysis. Lipase is specific in its behavior such that it can act only on the hydrolyzed (or emulsified) part of the substrate. This follows because the active center of the enzyme is catalytically active only when the substrate contacts it in its hydrolyzed form. In other words, lipase acts only when it can shuttleback and forth between the emulsion phase and the water phase, presumably within an interphase or boundary layer between these two phases. In industrial applications lipase is employed as a fat splitting enzyme to remove fat stains from fabrics, in making cheese, to flavor milk products, and to degrade fats in waste products. Effective use of lipase in these processes requires a fundamental understanding of its kinetic behavior and interactions with substrates under various environmental conditions. Therefore, this study focuses on modeling and simulating the enzymatic activity of the lipase as a step towards the basic understanding of multi-phase biocatalysis processes.

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ZVS Operating Range Extension Method for High-Efficient High Frequency Linked ZVS-PWM DC-DC Power Converter

  • Sato S.;Moisseev S.;Nakaoka M.
    • 전력전자학회:학술대회논문집
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    • 전력전자학회 2003년도 춘계전력전자학술대회 논문집(1)
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    • pp.227-230
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    • 2003
  • In this paper, a full bridge edge-resonant zero voltage mode based soft-switching PWM DC-DC power converter with a high frequency center tapped transformer link stage is presented from a practical point of view. The power MOSFETS operating as synchronous rectifier devices are implemented in the rectifier center tapped stage to reduce conduction power losses and also to extend the transformer primary side power MOSFETS ZVS commutation area from the rated to zero-load without a requirement of a magnetizing current. The steady-state operation of this phase-shift PWM controlled power converter is described in comparison with a conventional ZVS phase-shift PWM DC-DC converter using the diodes rectifier. Moreover, the experimental results of the switching power losses analysis are evaluated and discussed in this paper. The practical effectiveness of the ZVS phase-shift PWM DC-DC power converter treated here is actually proved by using 2.5kW-32kHz breadboard circuit. An actual efficiency of this converter is estimated in experiment and is achieved as 97$\%$ at maximum.

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S파라미터를 이용한 단상 변압기의 이상 상태 진단에 대한 연구 (Diagnosis of Fault and Abnormal Conditions in a Single-Phase Transformer Using S-parameter Measurement)

  • 김정은;김광호;나완수
    • 전기학회논문지
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    • 제67권10호
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    • pp.1344-1352
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    • 2018
  • In this paper, we propose a two-port S-parameter data to diagnose the fault conditions of a single-phase transformer. Using the S-parameters we can measure the reflection and transmission characteristics of signal power at the port of a transformer, which can also be converted into ABCD parameters and Z parameters through a well-known conversion formulas. Transformer fault diagnoses can be performed based on the intuitive and qualitative/quantitative characteristics of the these parameters. In addition, we can obtain wide frequency characteristics at the primary and secondary sides of the transformer, which can be used to get time domain responses using the inverse Fourier transformation with some specific input waveform. In order to verify the effectiveness of the proposed method, the fault conditions were analyzed in simulation and experiment for 3 kVA single phase transformer with 15: 5 turns ratio, and the validity of the proposed method was verified.

Series Active Power Filters to Compensate Harmonics and Reactive Power with the Direct Compensating Voltage Extraction Method in Three-Phase Four-Wire Systems

  • Kim, Jin-Sun;Kim, Young-Seok
    • Journal of Power Electronics
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    • 제9권5호
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    • pp.691-699
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    • 2009
  • This paper presents the analysis of series active power filter for reactive power compensation, load balancing, harmonic elimination, and neutral current eradication in three-phase four-wire power systems. Generally, the three-phase four-wire system is widely employed in distributing electric energy to several office building and manufacturing plants. In such systems, the third harmonic and its 3rd harmonics are termed as triple and zero sequence components that do not cancel each other in the system neutral. Consequently, the triple harmonics add together creating a primary source of excessive neutral current. Regarding this concern, this paper presents a new control algorithm for a series hybrid active system, whereas the control approach it adopts directly influence its compensation characteristics. Hence, the advantage of this control algorithm is the direct extraction of compensation voltage reference without phase transformations and multiplying harmonic current value by gain and the required rating of the series active filter is much smaller than that of a conventional shunt active power filter. In order to show the effectiveness of the proposed control algorithm, experiments have been carried out.