• Title/Summary/Keyword: primary calibration

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Plant Back Interval of Fluopyram Based on Primary Crop-derived Soil and Bare Soil Residues for Rotational Cultivation of Radish (Fluopyram의 전작물 유래 및 나지조건 토양잔류성에 기초한 알타리무의 식물식재후방기간)

  • Kim, Young Eun;Yoon, Ji Hyun;Lim, Da Jung;Kim, Seon Wook;Cho, Hyunjeong;Shin, Byeung Gon;Kim, Hyo Young;Kim, In Seon
    • Korean Journal of Environmental Agriculture
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    • v.40 no.2
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    • pp.99-107
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    • 2021
  • BACKGROUND: Pesticide uptake by a rotational crop after being used for the primary crop is a potential cause of violation against the pesticide law if the pesticide is not registered in the secondary crop. This study was conducted to investigate the plant back interval (PBI) of fluopyram for the rotational cultivation of radish. METHODS AND RESULTS: Two experimental approaches were performed the evaluation of residues in radish cultivated successively in soil 16 days after treated with fluopyram onto pepper plant (T1) and in radish cultivated in bare soil treated with fluopyram at PBI 30 and PBI 60 days (T2). A modified QuEChERS method coupled with LC/MS/MS analysis showed good linearity of matrix-matched standard calibration of fluopyram with the coefficient values of determination greater than 0.995. Recovery values at levels of 0.01, 0.05, 0.1 and 0.25 mg/kg ranged from average 84.9 to 117.6% with RSD less than 10%. Fluopyram residues in radish harvested from T1 and T2 were found as levels less than maximum residue limit. CONCLUSION: This study suggests 20~30 days as the PBI of fluopyram for the rotational cultivation of radish in the greenhouse soil treated with fluopyram used for pepper as the primary crop.

Development of a V-Band Millimeter-Wave Source Module

  • Kwon, Jae-Yong;Lee, Dong-Joon;Bakti, Aditia Nur;Angin, Windi Kurnia Perangin
    • Journal of electromagnetic engineering and science
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    • v.16 no.4
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    • pp.225-228
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    • 2016
  • KRISS-V, a V-band millimeter-wave source module for a primary RF power standard and calibration system developed by the Korea Research Institute of Standards and Science is here presented. The output power of KRISS-V is several times higher than that of commercial amplifier/multiplier chains and is highly stable (the standard deviations of output power are less than 0.01% in the worst case). The spectral purity of KRISS-V is high enough to consider it a single-tone signal generator. We also added programmable attenuation capability to KRISS-V for remote power control. Moreover, the in-house source module is cost-effective and adaptable to various measurement schemes. The structure of the model as well as detailed component information are introduced so that it can be reproduced.

Results of the key comparison in absolute pressure from 1 Pa to 1000 Pa

  • Hong, Seung-Soo;Shin, Yong-Hyeon;Chung, Kwang-Hwa;A. P. Miiller
    • Journal of Korean Vacuum Science & Technology
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    • v.6 no.3
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    • pp.109-115
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    • 2002
  • This paper describes a CCM key comparison of low absolute-pressure standards at seven National Measurement Institutes that was carried out during the period March 1998 to September 1999 in order to determine their degrees of equivalence at pressures in the range 1 Pa to 1000 Pa. The Korea Research Institutes of Standards and Science(KRISS) participated from 10 Pa to 1000 Pa pressure range in 1999. The primary standards, which represent two principal measurement methods, included five liquid-column manometers and four static expansion systems. The transfer standard package consisted of four high-precision pressure transducers, two capacitance diaphragm gauges to provide high resolution at low pressures, and two resonant silicon gauges to provide the required calibration stability.

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Determination of Amine Compounds Using 1-(N,N-Dimethylamino) pyrene-6-sulfonyl chloride as a New Fluorescent Derivatizing Reagent for HPLC (새로운 HPLC용 형광유도체화제인 1-(N,N-dimethylamino) pyrene-6-sulfonyl chloride를 이용한 아민화합물의 분석)

  • 이윤중;김용희;조정길
    • YAKHAK HOEJI
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    • v.35 no.4
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    • pp.288-294
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    • 1991
  • A new fluorescent derivatizing reagent was developed to be used in HPLC for the trace determination of primary and secondary amines. This new reagent, 1-(N,N-dimethylamino)pyrene-6-sulfonyl chloride, was synthesized by the chlorination of sodium 1-(N,N-dimethylamino)pyrene-6-sulfonate which was obtained from 1-(N,N-dimethylamino)pyrene after sulfonation. Ephedrine and norephedrine were derivatized quantitatively by this reagent. The optimum conditions for the derivatization such as pH, reagent concentration, reaction time and reaction temperature ware examined. The structures of derivatives were identified by IR, $^{1}$H-NMR and MS methods. The fluorescence properties and the stability of the derivatives were examined. The derivatives were separated on silica column with an isocratic elution using the mixture of n-hexane and ethylacetate and monitored by fluorescene detector. Linear calibration curves were obtained and detection limits in a 10 $\mu$l injection volume were 5 picomole for ephedrine and norephedrine.

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Launch Site Activities for the Launch of an Earth Observation Satellite

  • Im, Jeong-Heum
    • The Bulletin of The Korean Astronomical Society
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    • v.37 no.2
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    • pp.195.1-195.1
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    • 2012
  • Korea Aerospace Research Institute has developed an earth observation satellite whose primary mission objective is to provide high resolution electro optical earth images for Geographical Information Systems (GIS) establishment and the applications for environmental, agriculture and ocean monitoring. It was successfully launched into its mission orbit by using a commercial launch vehicle on 18th of May, 2012. This paper describes a series of launch activity at the launch site including its transportation to the launch site. Before conducting the launch site operation, satellite operation plane was prepared. Combining the satellite operation plan and launch vehicle activities, an integrated launch site operation plan and schedule have been drawn up. After arrival of the spacecraft at the launch site, post-ship check out has been conducted. And then it was fuel loaded and integrated with launch vehicle hardware. After completion of final electrical check out, count down procedure was executed. on 18th of May, it was launched into the space and was separated from the launch vehicle as planned. About 3 months of early operation and calibration/validation, now the satellite is conducting its normal mission.

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A study on the Development of a Precise Ratio Transformer (초정밀 비례변성기 개발에 관한 연구)

  • Kim, Han-Jun;Kang, Jeon-Hong;Han, Sang-Ok
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.07a
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    • pp.603-604
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    • 2005
  • A precise ratio transformer which is used to a ratio arm of a precise impedance measurement bridge at low frequencies was developed. The developed ratio transformer has the ratio taps of 1:1, 2:1, $\cdots$, to 10:1 in order to measure the primary impedance standards by substitution and special winding techniques for 10:1 ratio that is used frequently for impedance build up/down. The calibration results of the transformer has inphase and quadrature error of $0.073\times10^{-6}$ and $0.14\times10^{-6}$ respectively at 1.6 kHz.

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Development and Its Characteristics of a Dissipation Factor Standard (손실계수 표준기 제작 및 그 특성)

  • Kim, Han-Jun;Kang, Jeon-Hong;Han, Sang-Ok
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.527-528
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    • 2006
  • A dissipation factor standard of decade type having the range of 1 to 0.0001 at the frequency of 1 kHz and 10 kHz was fabricated using "T" networks combined R and C components. The values of the fabricated dissipation factor standard were adjusted within 1% of the nominal values at 0.0001 dial range and 0.05% at the others. This dissipation factor standard is used as a working standard for calibration of a impedance measurement meter at KRISS and as a primary standard of dissipation factor field at NML-SIRIM in Malaysia.

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Calibration of HEPD on KOMPSAT-1 Using the KCCH Cyclotron

  • Shin, Young-Hoon;Rhee, Jin-Geun;Min, Kyoung-Wook;Lee, Chun-Sik;Lee, Ju-Hahn;Kwon, Young-Kwan;Kim, Jong-Chan;Ha, Jang-Ho;Park, Se-Hwan;Lee, Chang-Hack;Park, H.S.;Kim, Yong-Kyun;Chai, Jong-Seo;Kim, Yu-Seog;Lee, Hye-Young
    • Proceedings of the KSRS Conference
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    • 1999.11a
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    • pp.208-213
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    • 1999
  • Space Physics Sensor (SPS) on-board the KOMPSAT-1 consists of the High Energy Particle Detector (HEPD) and the Ionospheric Measurement Sensor (IMS). The HEPD is to characterize the low altitude high energy particle environment and the effects on the microelectronics due to these high energy Particles. It is composed of four sensors: Proton and Electron Spectrometer(PES), Linear Energy Transfer Spectrometer (LET), Total Dose Monitor (TDM), and Single Event Monitor(SEM). 35MeV proton beam from the medical KCCH cyclotron, at Korea Cancer Center Hospital in Seoul, is used to calibrate the PES. Primary proton beam of 35MeV scattered by polypropylene target is converted to various energy Protons according to the elastic collision kinematics. In this calibration, the threshold level of the proton in the PES can be determined and the energy ranges of PES channels are also calibrated.

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External Validation of a Clinical Scoring System for Hematuria

  • Lee, Seung Bae;Kim, Hyung Suk;Kim, Myong;Ku, Ja Hyeon
    • Asian Pacific Journal of Cancer Prevention
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    • v.15 no.16
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    • pp.6819-6822
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    • 2014
  • Background: The aim of this study was to evaluate the accuracy of a new scoring system in Korean patients with hematuria at high risk of bladder cancer. Materials and Methods: A total of 319 consecutive patients presenting with painless hematuria without a history of bladder cancer were analyzed, from the period of August 2012 to February 2014. All patients underwent clinical examination, and 22 patients with incomplete data were excluded from the final validation data set. The scoring system included four clinical parameters: age (${\geq}50$ = 2 vs. <50 =1), gender (male = 2 vs. female = 1), history of smoking (smoker/ex-smoker = 4 vs. non-smoker = 2) and nature of the hematuria (gross = 6 vs. microscopic = 2). Results: The area under the receiver-operating characteristic curve (95% confidence interval) of the scoring system was 0.718 (0.655-0.777). The calibration plot demonstrated a slight underestimation of bladder cancer probability, but the model had reasonable calibration. Decision curve analysis revealed that the use of model was associated with net benefit gains over the treat-all strategy. The scoring system performed well across a wide range of threshold probabilities (15%-45%). Conclusions: The scoring system developed is a highly accurate predictive tool for patients with hematuria. Although further improvements are needed, utilization of this system may assist primary care physicians and other healthcare practitioners in determining a patient's risk of bladder cancer.

Intercomparison of the KAERI Reference Photon and Beta Radiation Measurements (한국원자력연구소 기준 광자 및 베타선장 측정의 국제상호비교)

  • Chang, Si-Yeong;Kim, Bong-Hwan;Kim, Jang-Lyul;McDonald, J.C.;Murphy, M.K.
    • Journal of Radiation Protection and Research
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    • v.21 no.4
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    • pp.255-262
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    • 1996
  • This paper describes the results of intercomparison measurements of KAERI reference photon and beta radiation fields between the KAERI and the PNNL(Pacific Northwest National Laboratory), recently performed at KAERI radiation calibration and dosimetry laboratory on the basis of the ANSI N13.11 criteria for personal dosimeter performance test. Each laboratory used her own radiation detectors or measurement devices traceable to her national primary standard in measuring the exposure rates for photon fields, the absorbed dose rates for beta radiation fields. The agreements in reference radiation measurements between two laboratories were found to be less than ${\pm}2.0%$ for photon fields, ${\pm}1.0%$ for beta radiation fields. Therefore, it could be concluded that KAERI reference radiation fields comply well with the international standard and thus can further serve as a national basis for the researches and developments in radiation protection dosimetry in Korea.

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