• The Korean Journal of Ceramics
• /
• v.5 no.1
• /
• pp.50-54
• /
• 1999

$(Pb_xLa_{1-x}) (Zr_yTi_{1-y})O_3$ (PLZT) thin films with electrooptic effect are promising for the optical application such as display or light shutter. However, it is difficult to use inexpensive and transparent glass substrates because the conventional process for preparation of PLZT requires temperatures above $600^{\circ}C$. In order to deposit a perovskite PLZT thin films at low processing temperatures through alkoxide route, we have offered several seeding processes which reduce the activation energy for crystallization. In this study, we optimized the stacking structure of multilayered PLZT for obtaining single phase perovskite at lower temperatures. As a result, ferroelectric PLZT thin films with different compositions were successfully prepared at a temperature as low at $500^{\circ}C$.

• Journal of the Korean Ceramic Society
• /
• v.34 no.4
• /
• pp.420-428
• /
• 1997

Alumino-borosilicate glasses containing nano-sized CuCl crystals for nonlinear optical application were prepared by the melting and precipitation process, and structural and optical properties were investigated by using XRD, TEM, SAXS, and optical spectroscopy. the average radius of the precipitated CuCl particles was about 2 nm. The blue shift of Z3 resonance peak with decreasing the precipitated CuCl particles size was found and the radius increased with decreasing the glass transition temperature of the matrix glass and with increasing the temperature and duration time of the precipitation heat treatment.

• 한국정보디스플레이학회:학술대회논문집
• /
• 2002.08a
• /
• pp.828-830
• /
• 2002

In this study, we have investigated a simple process of preparation of white pigment particles by physical coating with functionalized wax for the electrophoretic display. We will discuss, especially, the implementation of bistable pigment providing high mobility by using unique charge control agent and also optical properties of wax coated $TiO_2$ particles.

• Proceedings of the KIEE Conference
• /
• 1999.11d
• /
• pp.1096-1098
• /
• 1999

The performance of as plasma display panels (PDP) is influenced strongly by the surface glow discharge characteristics on the MgO thin films. This paper deals with the optimum preparation conditions of MgO Protecting layer by RF unbalanced magnetron sputtering(UBMS) in surface discharge type AC PDP. The samples prepared with the do bias voltage of -10V showed lower discharge voltage, lower erosion rate as a consequence of ion bombardment, higher optic transparency and higher crack resistance in annealing process than those samples prepared by conventional magnetron sputtering or E-beam eraporation.

• Journal of the Korean Ceramic Society
• /
• v.26 no.4
• /
• pp.471-478
• /
• 1989

In this study we investigated the gelation time of sol which containing mixtures of TEOS with H2O, ethanol, HCl in the preparation of monolithic silica glass through Sol-Gel method. In this case apparent activation energies were observed by Arrhenius equation. We investigated the conversion from gel to glass in drying and heat treatment stages using DT-TG, FT-IR, XRD analysis and dried gel conversed to glass by heat treatment up to 85$0^{\circ}C$. The results of this experiment showed that the gelation time of solutions were promoted when increasing the amount of addition of H2O and HCl catalyst for TEOS and high reaction temperature of solution.

• Journal of Electrochemical Science and Technology
• /
• v.8 no.2
• /
• pp.146-154
• /
• 2017

In this study, copper (II) oxide was prepared for use in a copper electroplating solution. Copper chloride powder and copper (II) oxide are widely used as raw materials for electroplating. Copper (II) oxide was synthesized in this study using a two-step chemical reaction. Herein, we developed a method for the preparation of copper (II) oxide without the use of sintering. In the first step, copper carbonate was prepared without sintering, and then copper (II) oxide was synthesized without sintering using sodium hydroxide. The optimum amount of sodium hydroxide used for this process was 120 g and the optimum reaction temperature was $120^{\circ}C$ regardless of the starting material.

• Bulletin of the Korean Chemical Society
• /
• v.35 no.2
• /
• pp.477-482
• /
• 2014

We immobilized Thermomyces lanuginosus lipase to catalyze transesterification reaction in DMF. This lipase was selected after screening among other commercial lipases. We found that prepared immobilized lipase is particularly useful for preparation of 6-O-acylsucrose with higher conversion rate even in 10 g scale. Several solvents were evaluated for selective transesterification reaction. We noticed that the immobilized lipase retained more than 80 % activity after 5 cycles of 96 h reaction. A general method was also developed to purify the products using simple crystallization and precipitation process. Furthermore, 6-O-vinyladipoylsucrose was subjected to synthesis of the corresponding polymer by radical initiator. The sucrose branched polymer can be used further for evaluation of its biodegradability and other biological applications.

• Proceedings of the Membrane Society of Korea Conference
• /
• 1995.04a
• /
• pp.45-45
• /
• 1995

Filtration, one of the most important process in the various industrials, is defined as the separation of two or more compounds from a fluid by passing the mixture refers to the separation of solid, immisible particles from liquid or gaseous mixture. Membrane filtration which is a type of filtration extends it's application further to include the separation, concentration, and filtration. The main objective of this investigation is the preparation of organic solvents-resistant polyimide membranes by using phase inversion technique and their application as a UF membrane. Specially, the dope solution was prepared from the newly developed method. The newly developed method is that the dope solution was directly prepared from the polyimide solution which was prepared by the modified one-step polymerization. The effects of the parameters for membrane preparation such as the casting solution composition and the casting conditions were investigated and the performance and chemical stabfiity of membrane are going to be tested.

• Journal of the East Asian Society of Dietary Life
• /
• v.9 no.4
• /
• pp.409-420
• /
• 1999

$\ulcorner$GANPYUN CHOSUN YORI-JEBUP$\lrcorner$,a book of cooking was written in Korean in 1934. The kinds of food were analyzed of cooking method, materials, measuring unit of materials by this book. Findings from this book are summarized as follows: 1. There were 8 kinds of Bap and 18 kinds of Zook. 2. There were 31 kinds of Korean Soup. 10 kinds of Ziggae, 4 kinds of Jun-gol. 3. There were Side-dishes including 6 kinds of Jim, 5 kinds of Jijimee, 7 kinds of Sanjuk, 9 kinds of Junyua. 18 kinds of Na-mool, 4 kinds of Moo-chim, 3 kinds of Ho, and 15 kinds of Po and were 8 kinds of dry side-dish. 4. Utensil to be used che(sieve), sot(pot). nambi(pan), Sugarak(spoon), and yang peon(bowl). 5. The measuring units were various. for example mal, dei, hob, etc. 6. The processing of cooking included preparation and boiling process. The processing of preparation were puting. mixing, and being cold, and the processing of heating were steaming and boiling.

• Elastomers and Composites
• /
• v.29 no.1
• /
• pp.9-17
• /
• 1994

Methylmetharylate grafted latex(MGL) was prepared by emulsion graft copolymerization of methyl methacrylate onto natural rubber latex(NRL) by using t-butyl hydroperoxide and tetraethylene pentamine in an aqueous medium. Blending of MGL and NRL with different mixing ratio carried out and viscosity and particle size distribution of blend latex were determined. It was found that the optimum condition of mature time, vulcanizing temperature and time for preparation of blend latex films were investigated. latex films prepared by dipping process were meaured. As the reuslt, blend latex(NR-d-MG) films obtained from two-dipping system were more excellent than NR and MG film obtained from one-dipping system.