• Title/Summary/Keyword: pre-treatment method

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Cochineal natural dyeing of alkali-treated PET (II) - Color, Washfastness, Abrasion Resistance, Static Electricity Characteristics - (알칼리 감량(減量) PET의 코치닐 염색(染色) (II) - 색상(色相), 세탁견뢰도(洗濯堅牢度), 마찰견뢰도(摩擦堅牢度), 마찰대전압(摩擦帶電壓)을 중심(中心)으로 -)

  • Kim, Hyun-Su;Jeon, Dong-Won
    • Journal of Fashion Business
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    • v.9 no.5
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    • pp.122-135
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    • 2005
  • It has been reported that natural dyeing is impossible without pre-treatment with metal mordanting agents. However, pre-treatment with chitosan, which has high affinity to natural dyes, could result in an excellent dyeing with various natural dyes. In this study, three treatment methods were employed; 1) Using PET without any pre-treatment (Method 1) 2) Using PET with chitosan acid solution pre-treatment (Method 2) 3) Using PET with chitosan pre-treatment and subsequent crosslinking using citric acid (Method 3) Method 2 and 3 enhanced the Cochineal dyeability remarkably compared to Mehod 1. Washfastness was also enhanced, and moisture content, static property, abrasion resistance, and fabric hand changes were investigated.

A Study for Natural Dyeing Textiles with Bean-Juice Treatment Method (콩즙 처리 방법에 따른 천연염색포의 염색성 연구)

  • Park, Kyeon-Soon;Choi, In-Ryu;Bae, Kye-In
    • Journal of the Korea Fashion and Costume Design Association
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    • v.9 no.2
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    • pp.85-92
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    • 2007
  • This study focused on bean-juice treatment method which have dyeing property to indigo, yellow soil, sappan wood, cochineal and also on the possibility of applying to mordanting. This is different from the active mordanting using chemicals. Natural mordants with development of dyeing are not harmful, also are the medicines for disease. Limestone and ash neutralize the acidic soil. bean-juice protein adhere to cellulose surface and change the physical properties of protein so that coloring of dye is better than before and film non-soluble in water is made. Therefore the color made from bean-juice process lasts after washing. This study try to show one of the ways to improve the current method using the heavy metal which can have bad effects for environment and human being. Bean-juice(raw bean, heated bean) treatment method can be the way to fix the natural dyeing problem of bad dyeing. Bean-juice had been treated under various condition with pre-treatment, post-treatment and raw bean, heated bean. Following results are obtained in this study. In the case of Indigo dyeing, pre-treatment of heated bean shows the biggest difference of color. In the case of yellow soil dyeing, pre-treatment of raw bean-juice shows the biggest gap of color. Pre-treatment of heated bean in sappan wood dyeing case and post-treatment of raw bean show bigger color difference than pre-treatment of raw bean. In cochineal dyeing, raw bean pre-treatment shows the biggest color difference.

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Thermal Characteristics Analysis of Pre-Treated Rayon Fibers for Preparing Activated Carbon Fibers (활성탄소섬유 제조시 전처리된 레이온 섬유의 열특성 분석)

  • Choi, Sang Seun;Lee, Soon Hong
    • Journal of the Korean Society of Safety
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    • v.29 no.4
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    • pp.61-72
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    • 2014
  • The aim of this study is to define the condition of optimal pre-treatment for preferable activated carbon fibers (ACFs), which are based on rayon fibers. This paper shows the ideal path of ACFs preparation process; implies that rayon fibers are pre-treated by various solvents with different times before the heating process. The pre-treated rayon fibers finally turned into desirable rayon fiber-based ACFs through optimal pre-treatment condition by heating processes. The thermal analysis method of pre-treated rayon fibers by thermo-gravimetry analyser (TGA) is an idealized tool, which analyzes the best thermal condition of pre-treatment process. Surface morphologies of resulting rayon fibers based ACFs were examined by scanning electron microscope(SEM). The results of TGA and SEM analyses show that the optimal pre-treatment condition for preparing ACFs was clearly defined, in terms of thermal stability and surface morphology.

Effect of Pre-Treatment Methods before Cooking on Mineral Retention in Siraegi (Raddish Leaves) (조리전 전처리 방법에 따른 시래기의 무기성분의 변화)

  • 박세원;유양자
    • Korean journal of food and cookery science
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    • v.13 no.5
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    • pp.635-638
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    • 1997
  • Dried raddish leaves were prepared by using three different pre-treatment methods (shady sun-drying, freezing after blanching, and shady sun-drying after blanching). Then, the retention of minerals in dried raddish leaves was determined. It was shown that the retention of most minerals (Na, K, Fe, Ca, Mg) except P was higher when shady sun-drying method was used. The retention of P was shown to be the lowest when freezing after blanching method was used.

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Reelection Device for Dyeability of Cotton Fabrics with Chestnut Husk Extract by Bean Sap Pre-treatment (밤 외피 추출물을 이용한 면직물 염색에서의 두즙 전처리효과)

  • 김병미
    • Journal of the Korea Fashion and Costume Design Association
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    • v.5 no.3
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    • pp.15-23
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    • 2003
  • Chestnut trees have been used as a dyeing material, which are grow naturally, are cultivated all the area of Korea. So, there is abundant amount of the materials and they have better colorfastness than other natural dyeing materials. But chestnut husk extract is good at silk and wool fabrics, not cotton fabrics. That's why many methods using chestnut extraction for dyeing are being studied. But most of them depend on treatment method with chemical material which doesn't fit with the aim, using natural materials. Therefore in this research, we used protein pre-treatment method which is dyeing chestnut husk extract after treating at cotton fabrics with bean sap. And we studied the effect of dyeability of chestnut husk extract to cotton fabrics. As a result of pre-treatment of bean sap at cotton fabrics, dyeability was increased. Besides laundering fastness, dry cleaning fastness, perspiration fastness and light fastness were almost increased.

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Study on pre-bonding according with HF pre-treatment conditions in Si wafer direct bonding (실리콘기판 직접접합에 있어서 HF 전처리 조건에 따른 초기접합에 관한 연구)

  • 강경두;박진성;정수태;주병권;정귀상
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.05a
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    • pp.370-373
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    • 1999
  • Si direct bonding (SDB) technology is very attractive for both Si-on-insulator(SOI) electric devices and MEMS applications because of its stress free structure and stability. This paper presents on- pre treatment conditions in Si wafer direct bonding, The paper resents on pre-bonding according to HF pre-treatment conditions in Si wafer direct bonding. The characteristics of bonded sample were measured under different bonding conditions of HF concentration, applied pressure and annealing temperature(200~ 100$0^{\circ}C$) after pre-bonding. The bonding strength was evaluated by tensile strength method. The bonded interface and the void were analyzed by using SEM and IR camera, respectively, Components existed in the interlayer were analyzed by using FT-IR. The bond strength depends on the HF pre-treatment condition before pre-bonding(Min 2.4kgf/$\textrm{cm}^2$~ Max : 14.kgf/$\textrm{cm}^2$)

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Evaluating optimal preprocessing method for separation of microalgae colonies into single cells for image quality (미세조류 이미지 품질 성능 향상을 위한 최적 전처리방법 선정 연구)

  • Sang Yeob Kim;Sung Kyu Maeng
    • Journal of Korean Society of Water and Wastewater
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    • v.38 no.2
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    • pp.109-117
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    • 2024
  • In this study, various pre-treatment methods were evaluated for microalgae separation. These methods aimed to facilitate safe, rapid, and cost-effective online imaging for real-time observation and cell counting. As pre-treatment techniques, heating, chemical hydrolysis, heating combined with chemical hydrolysis, and sonication were employed. The effectiveness of these methods was evaluated in the context of online imaging quality through experimentation on cultivated microalgae (Chlorella vulgaris and Scenedesmus quadricauda). The chemical treatment method was found to be inappropriate for improving image acquisition. The heating pre-treatment method exhibited a drawback of prolonged cell dispersion time. Additionally, the heating combined with chemical hydrolysis method was confirmed to have the lowest dispersion effect for Chlorella vulgaris. Conversely, ultrasonication emerged as a promising technique for microalgae separation in terms of repeatability and reproducibility. This study suggests the potential for selecting optimal pre-treatment methods to effectively operate real-time online monitoring devices, paving the way for future research and applications in microalgae cultivation and imaging.

Effects of ultrasound coupled with potassium permanganate pre-treatment of sludge on aerobic digestion

  • Demir, Ozlem
    • Advances in environmental research
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    • v.5 no.4
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    • pp.251-262
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    • 2016
  • The biodegradability and decomposition efficiencies increase with the pre-treatment of sludge in a digestion process. In this study, the feasibility of ultrasound coupled with potassium permanganate oxidation as a disintegration method and digestibility of aerobic reactor fed with disintegrated sludge with ultrasound coupled potassium permanganate were investigated. The first stage of the study focused on determining the optimum condition for ultrasonic pre-treatment for achieving better destruction efficiency of sludge. The second part of the study, the aerobic digestibility of sludge disintegrated with ultrasound and potassium permanganate oxidation alone and combined were examined comparatively. The results showed that when 20 min of ultrasonic pre-treatment applied, the specific energy output was 49384 kJ/kgTS with disintegration degree of 58.84%. During the operation of aerobic digester, VS/TS ratios of digesters fed with disintegrated sludge decreased indicating that disintegration methods could obviously enhance aerobic digestion performance. The highest reduction in volatile solids was 75% in the digester fed with ultrasound+potassium permanganate disintegrated sludge at the end of the operation compared to digester fed with raw sludge. Total Nitrogen (TN) and Total Phosphorus (TP) levels in sludge supernatant increased with this combined method significantly. Besides, it promoted the production of ${\bullet}OH$, thus enhancing the release of Carbon (C), Nitrogen (N) and Phosphorus (P) from the sludge. Disintegration with all methods used in this study could not improve Capillary Suction Time (CST) reduction in disintegrated digesters during the operation. The results demonstrated that the combined ultrasound treatment and potassium permanganate oxidation method improves the biodegradability compared to control reactor or their single application.

Effects of pH, molar ratios and pre-treatment on phosphorus recovery through struvite crystallization from effluent of anaerobically digested swine wastewater

  • Kim, Daegi;Min, Kyung Jin;Lee, Kwanyong;Yu, Min Sung;Park, Ki Young
    • Environmental Engineering Research
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    • v.22 no.1
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    • pp.12-18
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    • 2017
  • Struvite precipitation has been proven to be an effective method in removing and recovering ammonia nitrogen (N) and phosphate phosphorus (P) from wastewater. In this study, effects of pH, molar ratios and pre-treatment of effluent of anaerobically digested swine wastewater were investigated to improve struvite crystallization. The magnesium : ammonium : phosphate ratio of 1.2 : 1.0 : 1.0 was found to be optimal, yet the molar ratio in the wastewater was 1 : 74.9 : 1.8. From the analysis, the optimum pH was between 8.0 and 9.0 for maximal phosphate P release and from 8.0 to 10.0 for maximal ammonia N and phosphate P removal from real wastewater. Analysis from Visual MINTEQ predicted the pH range of 7-11 for ammonia N and phosphate P removal and recovery as struvite. For pre-treatment, microwave pre-treatment was ineffective for phosphate P release but ultrasound pre-treatment showed up to 77.4% phosphate P release at 1,000 kJ/L of energy dose. Precipitates analysis showed that phosphorus and magnesium in the collected precipitate had almost same values as theoretical values, but the ammonia content was less than the theoretical value.

Evaluation of Analytical Method for Determination of Potassium in Tobacco Leaf (담배 엽 중 칼륨 분석법의 평가)

  • Cho Sung-Eel;Kim Mi-Ju;Kim Sang-Un;Kim Yong-Ha;Min Young-Keun
    • Journal of the Korean Society of Tobacco Science
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    • v.28 no.1
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    • pp.51-57
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    • 2006
  • This study was carried out to improve and evaluate the analytical method for determination of potassium in tobacco leaf by various pre-treatment techniques. The time requirment of various pre-treatments was about 10 hour for dry ashing and 6 hour for microwave digestion and 3 hour for sonication. The results of recover in both pre-treatment techniques, microwave digestion and sonication, is greater than 85 % stably with reproducibility(RSD %) on replicates of less than 3 %. However the mean values for microwave digestion were lower than certified standard value of NlST SRM. Compared to the other pre-treatment techniques, analytical results for sonication technique strictly improved the accuracy and precision. In conclusion, the use of the simple sonication technique seems to be efficient for the determination of potassium in tobacco leaf in consideration for both the accuracy and reproducibility.