• 한국식품영양과학회지
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• 제33권1호
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• pp.225-228
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• 2004

반응표면분석법(RSM)을 활용하여 유동층과립기의 흡입공기온도, 물의 투입비율, 분무압력 등이 분유의 과립화에 미치는 영향을 분석하였다. 분유의 과립화 수율은 물의 투입 비율에 많은 영향을 받고 있음을 알 수 있었으며, 겉보기밀도 및 다짐 밀도는 분무압력에 크게 영향을 받고 있음을 보여주었다. 분유의 유동층 과립화의 최적조건은 흡입공기온도6$0^{\circ}C$, 물의 투입비율 16 mL/min, 그리고 분무압력 2.1 bar이었으며, 이때 과립화 수율은 94.0%, 겉보기밀도는 0.350 g/㎤, 그리고 다짐밀도는 0.446 g/㎤로 각각 예측되었다.

• Asian-Australasian Journal of Animal Sciences
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• 제17권7호
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• pp.1019-1025
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• 2004

The experiment was conducted to investigate the feasibility of using vegetable oil and non-fat dry milk (powdered milk) with skim milk for the preparation of dahi. In this experiment, six different types of dahi were prepared from whole milk, skim milk and admixture of non-fat dry milk with different levels of vegetable oil. The prepared dahi samples were subjected to physical, chemical and microbiological analysis to evaluate their quality. It was observed that the addition of non-fat dry milk and vegetable oil with skim milk improve the physical qualities (smell and taste, body and consistency, color and texture) of prepared dahi samples. Addition of non-fat dry milk and vegetable oil also improve the total solids, fat and protein content of dahi samples. It is concluded that the addition of vegetable oil at a rate of 4 to 6% together with 5% non-fat dry milk gave the best result.

• 한국축산식품학회지
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• 제41권2호
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• pp.335-342
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• 2021

Vitamin B12 deficiency may lead to serious health issues in both infants and adults. A simple analytical method involving sample pretreatment with enzyme, followed by cyanide addition under acidic conditions; separation on an immunoaffinity column; and high-performance liquid chromatography (HPLC) was developed for the rapid detection and quantitation of vitamin B12 in powdered milk. Detection limit and powdered milk recovery were determined by quantitative analysis. The limits of detection and quantitation were 2.71 and 8.21 ㎍/L, respectively. Relative standard deviations of the intra-day and inter-day precisions varied in the ranges of 0.98%-5.31% and 2.16%-3.90%, respectively. Recovery of the analysis varied in the range of 83.41%-106.57%, suggesting that the values were acceptable. Additionally, vitamin B12 content and recovery in SRM 1849a were 54.10 ㎍/kg and 112.24%, respectively. Our results suggested that the analytical method, including the sample pretreatment step, was valid. This analytical method can be implemented in many laboratory-scale experiments that seek to save time and labor. Therefore, this study shows that immunoaffinity-HPLC/ultraviolet is an acceptable technique for constructing a reliable database on vitamin B12 in powdered milk containing starch as well as protein and/or fat in high amounts.

• 한국식생활문화학회지
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• 제31권5호
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• pp.400-410
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• 2016

The purpose of this study was to discuss how 'milk' was produced and supplied introduced and spread in the modern Joseon period. Condensed milk and powdered milk were mainly consumed in Joseon during the Japanese colonial period since they could be conveniently preserved for a long time, although raw milk was also produced and consumed. For areas adjacent to farms, milk delivery service was offered while areas with great consumption received an additional supply from different areas by rail. Since no manufacturing plants were operational in Korea, condensed milk and powdered milk consumed in Joseon had to be imported. In the case of condensed milk, when production in Japan increased, extra supply was aggressively sent into their colony, Joseon. The 'Gyeongseong Milk Association' founded in 1937 is considered significant in that it led to standardization of the production system and prices as well as pasteurization of milk. In the late Japanese colonial era, milk production and consumption were controlled. As milk was purchased as a war supply, the milk consumption market became distorted and limited.

• 한국식품위생안전성학회지
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• 제9권3호
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• pp.169-174
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• 1994

This stydy was performed to investigate the inhibitory effect of bovine milk on the atherosclerotic rats. Eighty male rats of 5-weeks of age were divided into 4 groups, control, active treatment control fed the atherogenic feed, and skim milk and whole milk groups fed powdered skim or whole milk mixed with the atherogenic feed and observed for 13 weeks. Growth, clinical and pathological changes of the rats were examined. Rats of the 4 groups did not show significant difference of feed intake and weight gain. The level of serum cholesterol, high density lipoprotein cholesterol (HDL-cholesterol) fraction, and inorganics between skim milk and whole milk groups were not significantly different though significant difference was shown between active treatment control and milk groups. Milder calcification and nearosis in aorta, heart and kidney and fat degeneration in liver were seen in the milk groups than were in active treatment control. Marked difference, however, was not found between the skim milk and whole milk groups. Both powdered skim and whole milks could have a helpful effect of vitamin D2-and -cholesterol-induced atherosclerosis in rats.

• Food Science and Biotechnology
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• 제18권5호
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• pp.1199-1203
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• 2009

Melamine is a chemical intermediate to manufacture amino resins and plastics, which cannot be used as food additive since it can cause kidney stones. A qualitative determination method of melamine residue in powdered and liquid milk was developed using Fourier transform infrared (FTIR) spectroscopic technique. The calibration sets consisted of 21 standard melamine solutions, in which 1% trichloroacetic acid aqueous solution and acetonitrile (3:1, v/v) were used as solvent. The model was validated using 10 standard melamine solutions which were unused to build up the calibration set. Infrared (IR) absorbance peaks specific to almost all chemical groups in melamine molecule were shown in the spectral range between 1,100 and 1,800/cm. Combined partial least squares (PLS)-$2^{nd}$ derivative calibration model coupled with mean centering (MC) mathematical enhancement showed the highest correlation coefficients ($R^2$>0.99). In brief, the FTIR technique can be used for quantitative analysis of melamine in milk samples.

• Journal of Nutrition and Health
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• 제15권1호
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• pp.1-8
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• 1982

유당(乳糖)을 함유(含有)하지 않은 분유식(粉乳食)을 섭취한 흰쥐의 장관내(腸管內)에는 Casein함유식(含有食)을 섭취한 때와 마찬가지로 C.P.P.가 생성(生成)되며 이 C.P.P.에 의해 장관내(腸管內) 칼슘이 증가(增加)되며 소장하부(小腸下部)에서의 칼슘흡수(吸收)가 촉진(促進)되는 것을 밝혔다. 그러나 10% 또는 30% Lactose를 첨가한 경우, 위의 제(諸) 현상(現象)은 보이지 않았다. 이것은 장관내(腸管內)에서의 칼슘의 가용화(可溶化) 및 흡수(吸收)에 대 한 C.P.P의 촉진효과(促進效果)가 유당(乳糖)과는 독립적(獨立的)으로 일어나는 것임을 시사함이다.

• 한국축산식품학회지
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• 제41권4호
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• pp.731-738
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• 2021

Herein, a novel analytical method using a high-performance liquid chromatography-fluorescence detector (HPLC/FLD) is developed for rapidly measuring an L-carnitine ester derivative in infant powdered milk. In this study, solid-phase extraction cartridges filled with derivatized methanol and distilled water were used to effectively separate L-carnitine. Protein precipitation pretreatment was carried out to remove the protein and recover the analyte extract with a high recovery (97.16%-106.56%), following which carnitine in the formula was derivatized to its ester form. Precolumn derivation with 1-aminoanthracene (1AA) was carried out in a phosphate buffer using 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (EDC) as the catalyst. Method validation was performed following the AOAC guidelines. The calibration curves were linear in the L-carnitine concentration range of 0.1-2.5 mg/L. The lower limit of quantitation and limit of detection of L-carnitine were 0.076 and 0.024 mg/L, respectively. The intra- and interday precision and recovery results were within the allowable limits. The results showed that our method helped reduce the sample preparation time. It also afforded higher resolution and better reproducibility than those obtained by traditional methods. Our method is suitable for detecting the quantity of L-carnitine in infant powdered milk containing a large amount of protein or starch.

• 한국축산식품학회지
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• 제28권2호
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• pp.240-245
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• 2008

본 연구에서는 식품 내에 존재하는 트랜스지방산 함량에 대한 기초 자료를 수집하기 위하여 서울 지역에서 수거한 레토르트식품류 2종, 분유류 6종, 비스킷류 7종 피자류 3종을 선택하여 총 4종류의 18종의 시료를 분석하였다. 레토르트식품류 2종, 분유류 6종, 비스킷류 1종은 chloroform-methanol(CM) 추출법에 의하여 조지방을 추출하였으며 비스킷류 6종, 피자류 3종은 chloroform-methanol(CM) 추출법과 acid digestion 추출법을 각각 이용하여 조지방을 추출한 후 gas chromatography(GC)에 의해 트랜스지방산 함량을 분석하였다. 레토르트식품류의 총 지방 중 트랜스지방산 함량은 1-2.8%이며 분유류의 트랜스지방산 함량은 0.4-2.4%로서 제품의 브랜드와 제조회사에 따라 차이가 많이 났다. 비스킷류의 트랜스지방산 함량은 0-2.95%로서 제품 간 가장 많은 차이를 나타내었으며 이는 첨가물의 종류에 따라 달라지는 것으로 사료된다. 피자류에서는 2.8-3.45%의 높은 트랜스지방산 함유율을 나타내었다.

• 한국축산식품학회지
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• 제28권3호
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• pp.306-311
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• 2008

본 연구는 안전성 확보차원에서 식품분야에 활용성이 증가하고 있는 감마선 조사처리가 유제품의 항원성 저감에도 효과가 있음을 보이기 위해 수행되었다. 모세관전기영동 결과 ${\alpha}_{S1}$-케이신과 ${\beta}_{A1}$-케이신이 ${\alpha}_{S0}$-케이신과 ${\beta}_{A2}$-케이신보다 상대적으로 많이 분해되었음을 확인하였다. cELISA를 이용한 in vitro 시험 결과와 기니픽을 이용한 수동피부아나필랙시스(Passive cutaneous anaphylaxis) 반응을 통해 10 kGy의 감마선 조사에서 뚜렷한 항원성 저감을 확인하였다. 이상의 결과는 감마선 조사가 우유 단백질의 항원, 특히 ${\alpha}_{S1}$-케이신과 ${\beta}_{A1}$-케이신의 구조를 변화시켜 항원성을 감소시키는 것으로 판단되며, 따라서 감마선 조사는 알레르기 유발 식품의 항원성 감소에 유용한 기술로 생각된다.