• Progress in Superconductivity
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• v.8 no.1
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• pp.98-103
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• 2006

[$Bi_2Sr_2Ca_1Cu_2O_x$](BSCCO 2212) tubes were fabricated by centrifugal melting process(CMP). BSCCO 2212 powder was melted in a Pt crucible and solidified in a rotating steel mold. The BSCCO 2212 tube samples separated from steel mold were heat-treated at $800^{\circ}C\;and\;810^{\circ}C$ in oxygen flow. The critical current($I_c$) of the samples was measured by transport measurement at 77K, and the microstructure was investigated by scanning electron microscope. The $J_c$ at 77K of the tubes heated treated at $800^{\circ}C\;and\;810^{\circ}C$ were 197 and 240 $A/cm^2$, respectively. It was observed that the plate like grains in BSCCO 2212 tube was more developed in the sample heat treated at $810^{\circ}C\;and\;800^{\circ}C$ heated tube. It is found that the critical current($I_c$) of the BSCCO 2212 sample was dependent on the heating schedule regarding the growth of the BSCCO 2212 grains.

• Transactions on Electrical and Electronic Materials
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• v.5 no.2
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• pp.55-60
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• 2004

High-temperature Superconductor(HTS) tubes were fabricated in terms of different chemical compositions and various SrSO$_4$additions by centrifugal forming method. For powder melting by induction the optimum range of melting temperatures and preheating temperature were 1050$^{\circ}C$, 1100$^{\circ}C$ and 550$^{\circ}C$ for 30 min, respectively. The mould rotating speed was 1000 rpm. A tube was annealed at 840$^{\circ}C$ for 72 hours in oxygen atmosphere. The plates like grains more than 20 $\mu\textrm{m}$ were well developed along the rotating direction of mould regardless of initial chemical compositions and the amounts of SrSO$_4$in Bi2212. The specimen with Bi2212 composition exhibited T$\_$c/ of 83 K, while the specimens fabricated with other compositions are lower than 60 K. The measured I$\_$c/ and J$\_$c/ at 77 K(B = 0 T) in Bi2212 with 7 % SrSO$_4$ composition were about 680 A and 380 A/$\textrm{cm}^2$.

• Progress in Superconductivity and Cryogenics
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• v.2 no.1
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• pp.1-6
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• 2000

The effects of partial substitution of fluorine on physical properties were studied in Ag-sheathes tapes of $Tl_{0.8}Pb_{0.2}Sr_{1.8}Ba_{0.2} Ca_{2.2}Cu_3O_yF_x (0{\leq}x{\leq}1)$ nominal compositions. The tapes were prepared using the powder-in-tube method incorporating an in-situ reaction method. $CuF_2$ was used as a source of F. It was found that F-doping in Tl-1223 system resulted in a decrease in formation temperatire of Tl-1223 phase. and thus significantly deteriorated their superconducting properties. Such disadvantages seem to originate by the fromation of non-beneficial phases such as SrF2 in the early stage of the powder preparation process.

• Biotechnology and Bioprocess Engineering:BBE
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• v.9 no.5
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• pp.369-373
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• 2004

In order to elucidate the possibility of artificial production of p. ferulae by solid-state culture, the optimization of culture conditions was carried out. When $NH_4H_2PO_4$ and $CaCO_3$ were used in the cultures using test tube with 30 g of Populus sawdust at $25^{\circ}C{\pm}1$ in the dark, the favored mycelial growth was observed with $1\%$ of $NH_4H_2PO_4$ and the production of polysaccharide was 7.85 mg/100 mg of mycelium with $1\%$ of $CaCO_3$. The mixtures of $80\%$ of Populus Sawdust and $20\%$ of rice bran at $60\%$ of water content were determined to be optimal for the production of fruiting bodies in the sawdust culture. When three treatments containing various ratios of garlic powder were conducted, yields of fruiting bodies were drasti[ally higher than those of Synthetic mixture without garlic powder The highest yield (143 g/bag) was obtained with $7\%$ garlic powder. The yield of synthetic mixture containing $7\%$ of garlic powder was $83\%$ higher than that of Sawdust culture. The reason why garlic powder did support growth was not clear but it is possible that garlic powder might contain effective components for the formation of fruiting body. The optimal synthetic mixture composition consisted of cotton seed $77\%$, lime $6.4\%,\;K_2HPO_4\;0.2\%,\;KH_2PO_4\;0.2\%,\;CaHPO_4\;0.2\%$, corn flour $4\%$, wheat flour $5\%$, and garlic pow-der $7\%$.

• Journal of the Korean Ceramic Society
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• v.42 no.4
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• pp.260-268
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• 2005

A heat-resisting diatomite protection tube, using diatomite as a main component, was manufactured through an extrusion molding of ceramic slurry in different component ratios. And its mechanical strength, carbon analysis and microstructural non-homogeneity were investigated. After fixing $60wt\%$ of porous diatomite whose particle size was $50\~100\;{\mu}m$, the optimum mixture ratio with composition variables by changing $1\;wt\%$ of each component that was silica sol$(4.3\~7.3\;wt\%)$ as an inorganic binder, CMC (Sodium CarboxyMethyl Cellulose $(6\~9\;wt\%)$) as an organic binder and paper powder$(4.7\~7.7\;wt\%)$ was obtained. As a result of the investigation on a composition containing $60\;wt\%$ diatomite, $5.3\;wt\%$ silica sol, and $7\;wt\%$ CMC, a heat-resisting protection tube that could be used as a molten steel probe for measuring the temperature and components of molten steel was developed. The bending strength, compressive strength, and elastic modulus of the protection tube developed, that contained $\le2.3\;wt\%$ carbon, were 7.1 MPa, 7.5 MPa, and 1090 MPa, respectively.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.18 no.5
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• pp.468-472
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• 2005

High-temperature Superconductor(HTS) tubes were fabricated in term of different processing variables such as preheating temperature, speed of mold rotation and cooling rate by centrigugal forming method. For powder melting by induction the optimum range of melting temperatures and preheating temperature were $1050{\circ}C{\sim}1100{\circ}C\;and\;550{\circ}C\;for\;30\; min$, respectively The mould roating speed was 1000 rpm. A tube was annealed at $840 {\circ}C$ for 72 hours in oxygen atmosphere. The plate-like grains were well developed along the loafing direction and typical grain size was about more than $40{\mu}$. It was found that Ic values increased with increasing the Preheating temperature and speed of mold rotation. While Ic decreased with increasing the cooling rate. The measured Ic in $50mm{\times}70mm{\times}2.5mm$ tube was about 896 Amp.

• Journal of the Korean Society for Heat Treatment
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• v.33 no.4
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• pp.185-192
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• 2020

In this study, materials characterization of pure copper and copper based carbon nano-tube composite prepared by powder metallurgy method were investigated. Prior to evaluate materials characterization, spark plasma sintering processing variables such as sintering temperature, pressure, thickness and diameter of compacts was optimized to ensure the microstructure and materials property of pure Cu and Cu-CNT composite. In addition, corrosion behavior of Cu-based CNT composite produced by powder sintering method was investigated. It was confirmed from this study that the corroded surfaces of the composite shows less dissolution compared with pure copper in 3.5 wt% NaCl solution. The measured corrosion current density (I_corr) indicates improved corrosion property of Cu based composite containing small additions of CNTs in chloride containing media. Micro-galvanic activity between Cu and CNT was not observed in given sintering condition.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09a
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• pp.158-159
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• 2006

Ultrafine Au-Pb particles prepared by two method, (1) simultaneous evaporation of Au and Pb in inert gas and (2) subsequent vapor condensation of Pb in a differentially evacuated tube onto flying Au nanoparticles prepared by gasevaporation technique, were observed by electron microscopy. In the method (1), the particles that grew at the region where the two smoke masses converged, consisted of alloy phases. In the method (2), the particles consisted of two or three phases of Au, $Au_2Pb$, $AuPb_2$ and Pb phases in turn from the inner part, Pb-rich particles being composed of only two phases of $AuPb_2$ and Pb.

• Journal of the Korean Society of Food Science and Nutrition
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• v.15 no.4
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• pp.51-55
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• 1986

The general bag for powder materials such as sugar, salt and detergent used at present is a simple rectangular bag. In the practical uses, it has a lot of faults: it is difficult to reseal after partial usages, occurrence of loss in the case of sharing or adding, difficult for measured uses. Author made a new type of the measuring bag for powder materials in order to improve the problems. The new type of the bag for powder materials consists of a body, fall-induced tube with length scale line, and a pin to open and reseal. It shows various effectiveness: measured use$({\pm}0.6g)$ of powder materials, eatings don't occur during long period after opening, and no skin contamination during use of detergent. Consequently, the new one Is suitable for the measured use of powder materials such as sugar, salt, detergent, MSG and so on.

• Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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• 2000.02a
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• pp.3-5
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• 2000

Among the various processing techniques used in HTS wire fabrication, the PIP(Powder In Tube) method is currently one of the most promising for applications on an industrial scale. In this study, we have fabricated Bi-2223/Ag superconducting tapes using the modified PIT process, where several process factors were changed and improved, ie., powder packing, drawing, rolling and heat treatment. We obtained Bi-2223 tape that have high critical current, 46 a at 77.3 K, have high critical current, 46A at 77.3 K, self field although the tape was not pressed but only rolled. The critical current of 100m class long length tape was measured 21.6A at the same criterion. Besides, the critical current of Bi-2223/Ag tape was measured applying magnetic fields with different directions at various temperatures.