• 한국잠사곤충학회지
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• 제43권1호
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• pp.41-48
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• 2001

The purification, dissolution and powdering of stained waste silk obtained from weaving and dyeing process were studied for the surface modification of textile fabric and plastic materials. The whiteness of stained waste silk could be improved through degumming and bleaching with sodium hydrosulfite. The water-soluble fibroin solution can be obtained by dissoving the degummed waste silk in a boiling solution of 50% calcium chloride for 60 minutes. The salts and heavy metals contained in fibroin solution were removed by electric dialysis, wool fiber filtration and gel filtration chromatography. The fibroin powder was prepared by using a fine grinder after the alkali treatment for weakening the silk fiber. The fine fibroin powder of particle size around 30 ㎛ was obtained with a ultra fine-mill, while it was finer below 10 ㎛ with a ball-mill. The dissolved or powdered silk was applied to the surface of fabric with addition of the binder (a urethane resin). The moisture content of polyester and nylon fabrics treated with the silk solution was improved due to hygroscopic property of silk. The fine fibroin powder mixed with the binder ws coated on the surface of synthetic film by use of the air pressed sprayer. It was revealed that the hygroscopicity as well as the softness of fibroin powder coated film was much improved. Therefore, it is thought that the fine silk fibroin powder is applicable as an coating agent for the surface modification of plastic and synthetic leather.

• 한국세라믹학회지
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• 제46권5호
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• pp.528-533
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• 2009

High purity $\beta$-SiC powders were synthesized using sol-gel processing. TEOS and phenol resin were used as the starting material for the silicon source and carbon source, respectively. The process turned out to be capable of producing high purity SiC powder purity degree with 99.98 %. However, it was difficult to control the shape and size of $\beta$-SiC powders synthesized by sol-gel process. In this study, $\beta$-SiC powder with size of $1{\sim}5$ um an 30 nm were used as the seeds for $\beta$-SiC to control the $\beta$-SiC powder morphology. It was found that $\beta$-SiC powder seeds was effective to increase the powder average size of synthesized $\beta$-SiC using sol-gel process by acting as the preferred growing sites for $\beta$-SiC.

• 한국세라믹학회지
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• 제56권6호
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• pp.521-525
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• 2019

A study was conducted to investigate the possibility of a composite material containing a composite resin as a matrix and hydroxyapatite (HAp) powder as a substitute material for tooth repair. As the content of HAp increased, hardness value (111.9 HV at 9%) increased and flexural strength (73.3 MPa at 9%) decreased. Observation of the microstructure after immersion in a simulated body fluid (SBF) solution confirmed a dense structure due to mutual coagulation and curing. It was thought that fine HAp recrystals were formed with the lapse of time, and they were entangled to form a condensation structure and had a dense structure. In addition, since the activity was shown by the ion migration on the surface of a tooth, it was highly likely that a biocompatible bond occurred during tooth contact. Therefore, it could be used as a substitute material for tooth repair.

• Restorative Dentistry and Endodontics
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• 제39권4호
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• pp.310-318
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• 2014

Objectives: This study examined the influence of the resin thickness on the polymerization of silorane- and methacrylate-based composites. Materials and Methods: One silorane-based (Filtek P90, 3M ESPE) and two methacrylate-based (Filtek Z250 and Z350, 3M ESPE) composite resins were used. The number of photons were detected using a photodiode detector at the different thicknesses (thickness, 1, 2 and 3 mm) specimens. The microhardness of the top and bottom surfaces was measured (n = 15) using a Vickers hardness with 200 gf load and 15 sec dwell time conditions. The degree of conversion (DC) of the specimens was determined using Fourier transform infrared spectroscopy (FTIR). Scratched powder of each top and bottom surface of the specimen dissolved in ethanol for transmission FTIR spectroscopy. The refractive index was measured using a Abbe-type refractometer. To measure the polymerization shrinkage, a linometer was used. The results were analyzed using two-way ANOVA and Tukey's test at p < 0.05 level. Results: The silorane-based resin composite showed the lowest filler content and light attenuation among the specimens. P90 showed the highest values in the DC and the lowest microhardness at all depth. In the polymerization shrinkage, P90 showed a significantly lower shrinkage than the rest two resin products (p < 0.05). P90 showed a significantly lower refractive index than the remaining two resin products (p < 0.05). Conclusions: DC, microhardness, polymerization rate and refractive index linearly decreased as specimen thickness linearly increased. P90 showed much less polymerization shrinkage compared to other specimens. P90, even though achieved the highest DC, showed the lowest microhardness and refractive index.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1999년도 추계학술대회 논문집
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• pp.629-632
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• 1999

For replacing Li metal ai Lithium ton Bakery(LIB) system. we used carbon powder material which prepared by pyrolysis of phenol resin as starting material. It became amorphous carbon by pyrolysis through it\`s self condensation by thermal treatment. Amorphous carbon can be doped with Li intercalation and deintercalation because it has wide interlayer. however it has a problem with structural destroy causing weak carbon-carbon bond. So. we used ZnCl$_2$ as the pore-forming agent. This inorganic salt used together with the resin serves not only as the pore-forming agent to form open pores, which grow Into a three-dimensional network structure in the cured material, foul also as the microstructure-controlling agent to form a loose structure dope with bulky dopants. We analyzed SEM in order to find to different of structure. and can calculate distance of interlayer. CV test showed oxidation and reduction

• 대한소아치과학회지
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• 제30권1호
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• pp.69-79
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• 2003

자가중합형 아크릴릭 레진에 polyp를 혼합하지 않은 대조군, 그리고 레진 분말에 대한 polyP(사슬길이 13과 18의 혼합물인 Calgon)의 무게비를 1%로 혼합한 polyP 1%군, 2% 혼합한 polyP 2%군 및 3% 혼합한 polyP 3%군으로 분류하여 경화시킨 후, 경화된 각각의 레진과 실험균주 S. mutans GS5, S. sobrinus 6715, S. gordonii G9B및 Challis, 그리고 P. gingivalis 2561과 Candida albicans ATCC90027을 대상으로 레진표면에 대한 미생물들의 부착의 정도, 성장 억제효과 및 접촉각의 변화를 관찰하여 그 결과로 미루어 아크릴릭 레진에 포함된 polyP는 구강 미생물에 대해 직접적으로 강한 항균 효과를 나타내지는 않는 것으로 판단되나 미생물의 부착 특히 우식원인균인 mutans streptococci의 부착을 방해하는 것으로 가늠되며, 이는 polyP의 첨가에 의한 아크릴릭 레진 표면에서 일어난 소수성의 변화가 일부 관여하는 것으로 여겨진다. PolyP가 혼합된 아크릴릭 레진의 장착은 일반적인 아크릴릭 레진으로 제작된 가철성 장치를 장착한 후 나타날 수 있는 우식 이환의 가능성을 감소시킬 수 있는 임상적 적용 가능성을 제시하였다고 여겨진다.

• 대한금속재료학회지
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• 제49권1호
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• pp.85-91
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• 2011

Alnico magnets can be used as magnetic bearings for the precise electric power measuring instruments such as watt-hour meters because they have high remanence ($B_r$), relatively high maximum energy product ($(BH)_{max}$), and excellent temperature stability. In this study, Alnico composite magnets were fabricated by appropriately mixing alnico alloy powders with epoxy resin and binder. The Alnico powders mixed with epoxy resin and a hardening agent with a mixing ratio of 96:4 were pressed and then cured to be a toroid-type ring magnet with an outer diameter (${\Phi}_{out}$) of 15 mm, an inner diameter (${\Phi}_{in}$) of 6.5 mm and a thickness (t) of 2.5 mm, respectively. The magnetic properties of the Alnico ring magnets were varied with the mixing ratio of Alnico powders that possess different average particle sizes. The Alnico ring magnet prepared by mixing 5 wt% of $50{\mu}m$ (small size) powder, 15~20 wt% of $150{\mu}m$ (medium size) powder, and 75~80 wt% of $300{\mu}m$ (large size) powder showed the best magnetic properties (remanent induction, coercive force, maximum energy product, and surface flux density). In addition, measurements of temperature and moisture characteristics for the Alnico ring magnets showed that the surface flux densities of the N and S poles decreased little and the repulsive distance between the magnets decreased as small as 0.05 mm after 10 days.

• Journal of the Korean Wood Science and Technology
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• 제36권6호
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• pp.49-58
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• 2008

본 연구는 내구성이 우수하며 포름알데히드방출이 적은 페놀수지 사용 메란티합판을 마루판용 대판으로 사용하고 북미산 벚나무 단판을 표면재료로 사용한 마루판의 제조과정에서 접착제 및 도료에 녹차잎 분말을 첨가하였을 때 마루판으로부터 방출하는 총휘발성유기화합물(TVOC)과 포름알데히드의 감소효과와 녹차잎 분말의 적정 첨가량을 구명하였다. 1) 녹차잎 분말의 폴리페놀화합물량은 9.85%였다. 2) 녹차잎 분말은 FT-IR 결과 벤즈알데히드와 에틸헥사알콜과 반응하여 화학결합을 하는 것으로 나타났다. 3) 페놀수지메란티대판에 벚나무단판오버레이 마루판 제조를 위한 접착제와 UV도료에 전건중량기준으로 2.5%의 녹차잎 분말을 각각 첨가하는 것이 총휘발성유기화합물과 포름알데히드의 방산제거 효과가 매우 적절한 것으로 나타났다. 4) 20L 소형챔버법에 의한 녹차잎 분말 2.5%를 접착제와 도료에 각각 첨가한 온돌용 마루판의 7일째 TVOC는 $0.089mg/m^2hr$이고 포름알데히드는 $0.001mg/m^2hr$를 나타내 최우수등급으로 나타났다.

• 한국자기학회지
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• 제4권3호
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• pp.219-225
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• 1994

이방성 Sr-페라이트/레진본드 영구자석에서 외부자장과 성형체의 유동성이 Sr-페라이트 자성분말의 방향성에 어떤 영향을 미치는지 조사하였다. 이방성 Sr-페라이트 자성분말의 방향성은 외부자장의 세기와 충전율과 성형온도의 함수인 유동성에 따라 변화하였다. 자성분말의 방향성은, 자성분말의 충전율이 56vol%이고 $1000sec^{-1}$의 전단속도에서 성형체의 겉보기점도가 약 3000 poise 이하인 성형온도에서 5 kOe 이상의 자장을 가해주었을때, 본 실험에서 얻을 수 있는 최대값을 나타내었다. 이러한 조건에서 직류자기이력곡선으로부터 측정된 Sr-페라이트 자성분말의 방향성은 배향도가 84~85%(0.84~0.85)이었다. 이 결과는 ${23~40}^0$ 범위의 $2{\theta}$에서 X-선 회절분석 결과인 0.85의 방향계수와 일치하였다. 이러한 Sr-페라이트 자성분말의 방향성에서 이방성 레진본드 영구자석은 잔류자 속밀도가 2.2kG, 최대자기에너지적이 2.2 MGOe인 자기특성을 나타내었다.

• 구강회복응용과학지
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• 제37권3호
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• pp.101-110
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• 2021

목적: 본 연구에서는 3D 프린팅 레진과 임시 수복용 레진의 열순환 처리에 따른 전단결합강도의 변화를 연구하고자 하였다. 연구 재료 및 방법: DLP 방식을 이용하여 3D 프린팅 레진으로 표본을 제작하였다. 표본은 상부에 부착한 임시 수복용 레진(PMMA, bis-acryl resin) 및 열순환 처리 횟수(대조군, 2,000, 3,000, 5,000회)에 따라 8개의 군으로 분류하였다. 만능 재료시험기 상에서 결합된 표본들의 전단결합강도를 측정하였다. 결과: 열순환 처리의 횟수가 증가함에 따라 3D 프린팅 레진에 대한 PMMA와 bis-acryl resin의 전단결합강도는 PMMA에서 3,000회와 5,000회 간을 제외하고 모두 감소하였다. PMMA 그룹에서는 3,000회 미만의 열순환 처리 횟수 간에서 유의한 전단결합강도의 차이를 보였으며(P < 0.05), 3,000회 이상의 열순환 처리 횟수 간에는 유의한 차이를 보이지 않았다(P > 0.05). Bis-acryl resin 그룹에서는 대조군과 2,000회 간, 대조군과 3,000회 간, 대조군과 5,000회 간의 열순환 처리에는 유의한 전단결합강도의 차이가 있었으며(P < 0.05), 2,000회와 3,000회 간, 3,000회와 5,000회 간에는 유의한 차이가 없었다(P > 0.05). 결론: 3D 프린팅 레진에 대한 임시 수복용 레진의 전단결합강도는 열순환 처리를 한 경우 결합강도가 낮아지는 경향을 보였다.