• Title/Summary/Keyword: powder mixture

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Synthesis of size-controlled ZnO tetrapods sizes using atmospheric microwave plasma system and evaluation of its photocatalytic property (대기압 마이크로웨이브 플라즈마를 이용한 다양한 크기의 ZnO tetrapod 합성 및 광촉매 특성 평가)

  • Heo, Sung-Gyu;Jeong, Goo-Hwan
    • Journal of the Korean institute of surface engineering
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    • v.54 no.6
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    • pp.340-347
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    • 2021
  • Among various metal oxide semiconductors, ZnO has an excellent electrical, optical properties with a wide bandgap of 3.3 eV. It can be applied as a photocatalytic material due to its high absorption rate along with physical and chemical stability to UV light. In addition, it is important to control the morphology of ZnO because the size and shape of the ZnO make difference in physical properties. In this paper, we demonstrate synthesis of size-controlled ZnO tetrapods using an atmospheric pressure plasma system. A micro-sized Zn spherical powder was continuously introduced in the plume of the atmospheric plasma jet ignited with mixture of oxygen and nitrogen. The effect of plasma power and collection sites on ZnO nanostructure was investigated. After the plasma discharge for 10 min, the produced materials deposited inside the 60-cm-long quartz tube were obtained with respect to the distance from the plume. According to the SEM analysis, all the synthesized nanoparticles were found to be ZnO tetrapods ranging from 100 to 600-nm-diameter depending on both applied power and collection site. The photocatalytic efficiency was evaluated by color change of methylene blue solution using UV-Vis spectroscopy. The photocatalytic activity increased with the increase of (101) and (100) plane in ZnO tetrapods, which is caused by enhanced chemical effects of plasma process.

Experimental Study on Low-pH, Anti-washing Grouts Incorporating Gypsum for Reinforcement of Underwater Cavities (수중 공동보강용 석고 활용 저 pH형 수중불분리 그라우트에 대한 실험적 연구)

  • Kim, Young-sang;Baek, Jeong Jin;Kim, Hyeong-Ki
    • Resources Recycling
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    • v.27 no.6
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    • pp.30-37
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    • 2018
  • A series of experiment was conducted to evaluate basic performances of low-pH, anti-washing grouts incorporating gypsum which applied for reinforcing underwater cavities in limestone- grounds. Various types of mix proportions were designed and the fluidity, strength and environmental impact of these mixtures were evaluated. The flowability was evaluated under two conditions, i.e., flows without and with pressing, respectively. Strength was measured for the hardened mixtures fabricated under conditions of air and water injections. The environmental impacts including the pH of the suspension and the suspended solids concentration for the mixtures were evaluated. The low pH of fresh mixture suspension, below than 10, was achieved by incorporation of gypsum. The mix proportions of cement-quartz powder-gypsum binders and chemical agents resulted in mortar natural flow 7-10 cm and uniaxial compressive strength 4 MPa were derived.

A Study on Anti-oxidization Coating for Staged Combustion Cycle Rocket Engines (다단연소 사이클 엔진 적용을 위한 내산화 코팅에 관한 연구)

  • Kim, Young-June;Rhee, Byong-ho;Noh, Yong-Oh;Bae, Byung-Hyun;Hyun, Seong-Yoon;Cho, Hwang-Rae;Bang, Jeong-Suk;Byon, Eung-Sun;Han, Yeoung-Min
    • Journal of the Korean Society of Propulsion Engineers
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    • v.22 no.5
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    • pp.125-131
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    • 2018
  • Some propellants in a liquid rocket engine are burned in the pre-burner of a staged combustion cycle engine, resulting hot gas drives the turbine. The burned gas passing through the turbine is supplied to the combustor at high temperature and pressure. The form of the gas can be fuel rich or oxidizer rich dependent upon the mixture ratio or the engine scheme. When the cycle works at oxidizer-rich condition, the metal pipes composing the engine can be ignited or even exploded by an impact of very a small particle. In this study, we developed the powder combination and processes for an anti-oxidation coating through the analysis of various coating materials.

Evaluation of Mechanical and Durability Performance of Mortar Shotcrete (모르타르 숏크리트의 역학성능 및 내구성능 평가)

  • Park, Byoungsun;Jang, Kun Young;Choi, Young Cheol
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.23 no.5
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    • pp.68-74
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    • 2019
  • In this study, the mechanical property and durability of improved bond performance mortar shotcrete was investigated. Mortar shotcrete was prepared by replacing coarse aggregate with 100% fine aggregate in the shotcrete mixture proportion proposed in the road construction standard specification. OPC, GGBFS and anhydrite were used as binders, and polymer powder was substituted for 1% and 2% of binder for improving bond property. From the experimental results, it was found that the compressive strength decreased with increasing polymer addition, but the bond strength increased. The addition of polymer to mortar shotcrete also reduced the drying shrinkage and improved the resistance to carbonation. Initial hydration heat of mortar shotcrete decreased with the addition of polymer, and it was judged that the initial compressive strength decreased.

A Study on the Application of Non-glutinous rice in Shanghanlun (『상한론(傷寒論)』의 갱미(粳米) 입약법(入藥法)에 대한 고찰)

  • Ahn, Jin-hee
    • Journal of Korean Medical classics
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    • v.32 no.2
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    • pp.71-92
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    • 2019
  • Objectives : To examine various ways non-glutinous rice has been applied in different formulas of "Shanghanlun" and the relationship between non-glutinous rice and the formulas' effects. Methods : First, texts that included non-glutinous rice were selected from the "Shanghanlun". Then, they were categorized according to the application of non-glutinous rice, followed by analysis of its relationship with each formula. Results : Most formulas that used non-glutinous rice in raw form when decocting with other ingredients included Shigao. Non-glutinous rice alleviates coldness of Shigao as in the case with Taohuatang where it stops diarrhea. Non-glutinous rice used in Wumeiwan warms the center and boosts Qi and helps the medicinal ingredients to bind when made into pellets. In Guizhitang and Lizhongwan, non-glutinous rice assists Stomach Qi. In Shizaotang, porridge is taken after diarrhea to help quick recovery. To prevent damage of Zheng Qi, Baisan can be mixed with rice water for administration. The level of cathartic effect can be managed through giving cold or hot porridge to the patient according to his/her response to the medicine. Mazirenwan, Mulizexiesan, Banxiasan, Sinisan, Wulingsan are mixed in rice water for administration. It makes it easier to swallow than when mixed with plain water. The application of rice flour is either internal or external. In Zhufutang, where rice flour is parched, it harmonizes the center and stops diarrhea. In Daqinglongtang when there is too much perspiration, warm powder is sprinkled on the skin to stop sweating. Clear porridge in Jiuziyisifang and rice flour in Shechuangzisan were exclusive to "Jinguiyaolue", while Baisan and rice water mixture could only be found in "Shanghanlun". Conclusions : The excavation and research on various ways non-glutinous rice was applied in treatment holds certain meaning in contemporary practice of Korean Medicine where treatment leans heavily on medicinal treatment rather than food, and all ingredients are boiled together in large quantities for most decoctions.

Influence of Various Replacing Ratios of SCMs on Properties of High Fluidity Concrete (광물질 혼화재의 치환율 변화가 고유동 콘크리트의 특성에 미치는 영향)

  • Han, In-Deok
    • Journal of the Architectural Institute of Korea Structure & Construction
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    • v.35 no.12
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    • pp.165-172
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    • 2019
  • The aim of the research is to evaluate the influence of various replacing ratios of supplementary cementitious materials(SCMs) such as fly ash(FA), blast furnace slag(BS), and both FA and BS on general properties including segregation resistance as a powder based high fluidity concrete of normal strength grade with water-to-cement ratio 0.40. Specifically, by replacing the SCMs with low density powders, it was assessed that the decreased segregation resistance due to the decreased viscosity by J-ring test. As a result of the experiment, from the general test, the mixtures with SCMs showed increased segregation resistance by increased viscosity as the references, while some segregation was shown from J-ring test due to the decreased density of fresh state mixture related with the capacity of delivering coarse aggregate.

Effect of dietary supplementation of a phytogenic blend containing Schisandra chinensis, Pinus densiflora, and Allium tuberosum on productivity, egg quality, and health parameters in laying hens

  • Moon, Seung-Gyu;Lee, Sung-Kwang;Lee, Woo-Do;Niu, Kai-Min;Hwang, Won-Uk;Oh, Jong-Seok;Kothari, Damini;Kim, Soo-Ki
    • Animal Bioscience
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    • v.34 no.2
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    • pp.285-294
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    • 2021
  • Objective: This study was conducted to investigate the supplementary effect of a phytogenic blend (SPA: a mixture containing fermented Schisandra chinensis pomace, fermented Pinus densiflora needle extract, and Allium tuberosum powder in the ratio of 2:2:1) on egg production, egg quality, blood constituents, and visceral organs in laying hens. Methods: A total of 135 Hy-line brown laying hens (48-wk-old) were randomly allocated to three dietary treatments with 5 replicates of 9 hens. The control group (CON) was fed a basal diet (no exogenous SPA addition) and the experimental groups were fed the basal diet containing SPA at the level of 0.1% and 0.3% for 6 weeks. Results: The feed intake was significantly improved in SPA supplemented groups as compared with the control (p<0.05). However, egg production, daily egg mass, and feed conversion ratio were not different among the dietary treatments (p>0.05). For egg quality traits, only Haugh unit (HU) was significantly improved in SPA (0.3%) (p<0.05) as compared with other groups. However, HU was not affected during 4-wk of storage at 18℃ among the dietary treatments (p>0.05). Furthermore, SPA supplementation did not affect the blood biochemical constituents except for the phosphate content, which was significantly higher in SPA groups than the CON group (p<0.05). There were no significant differences in visceral organ characteristics and immune indicators (immunoglobulin A [IgA], IgG, and IgM) in SPA or CON groups. Conclusion: This study suggested that the supplementation of SPA may have beneficial effects on feed intake and egg quality in laying hens.

Extractives from the needles of Juniperus rigida Siebold et Zucearin and Antioxidant activity (노간주나무(Juniperus rigida Siebold et Zucearini) 잎의 추출성분 및 항산화 활성)

  • Lee, Sang-Keug;Kim, Jin-Kyu;Ham, Yeon-Ho;Bae, Young-Soo
    • Journal of the Korean Wood Science and Technology
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    • v.32 no.1
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    • pp.59-66
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    • 2004
  • The dried neeldes(1.5 kg) of Juniperus rigida were ground, extracted with acetone-H2O(7:3, v/v), concentrated, and fractionated with a series of hexane, CH2Cl2, EtOAc and water on a separatory funnel. Each fraction was freeze dried to give dark-brown powder and EtOAc and water soluble fractions were chromatographed on a Sephadex LH-20 column using a series of aqueous methanol and ethanol-hexane mixture as eluent. Spectrometric analysis such as NMR and FAB or EI-MS including TLC were performed to characterize the structures of the isolated compounds. The needles of Juniperus rigida contained a large amount of (+)-catechin, quercetin-3-O-α-L-rhamnopyranoside and isoconiferin, in addition to a small amount of umbelliferone and quercetin-3-O-β-D-rutinoside. The antioxidative activities of each fraction and isolated compounds were tested by DPPH radical scavenging method, and EtOAc soluble fraction, (+)-catechin and quercetin-3-O-α-L-rhamnopyranoside were effective.

Fundamental Study on the Strength and Heat Transferring Charcteristic of Cement Composite with Waste CNT (폐CNT를 혼입한 시멘트 복합체의 강도 및 열전달 특성에 대한 기초적 연구)

  • Koo, Hounchul;Kim, Woon-Hak;Oh, Hongseob
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.10 no.1
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    • pp.66-73
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    • 2022
  • The purpose of this study was to develop self-heating concrete by utilizing the conduction resistance of concrete in order to reduce the risk of occurrence of black ice in the concrete pavement in winter and to prevent damage caused by freez-thawing effect. For this purpose, it was attempted to evaluate the strength and temperature exothermic characteristics using powder and liquid waste CNTs and a waste cathode agent as a conduction promotion. It was analyzed that liquid waste CNT had an effective dispersion degree in the mortar and a small decrease in strength occurred. In addition, DC 24 V was supplied by applying steel mesh, copper foil and copper wire to the mortar as electrodes, and the temperature change characteristics according to the mixing ratio of spent CNTs, anodes and carbon fibers were evaluated. In addition, by evaluating the temperature characteristics according to the electrode spacing from the selected optimal mixture, it was confirmed that it had sufficient heating characteristics up to an electrode spacing of 100 mm up to AC 50 V.

Flvonoids and Their Glycosides from the Bark of Salix rorida (분버들(Salix rorida) 수피의 후라보노이드 및 배당체 화합물)

  • Ham, Yeon-Ho;Bae, Young-Soo
    • Journal of the Korean Wood Science and Technology
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    • v.30 no.1
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    • pp.56-62
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    • 2002
  • The air-dried bark of Salix rorida was extracted with acetone-water(7:3, v/v) and its extractives were concentrated with a vacuum evaporator. The extractives were fractionated with a series of n-hexane, chloroform, ethylacetate(EtOAc) and water on a separatory funnel. Each fraction was freeze-dried to give some dark brown powder. The EtOAc and water soluble fractions were chromatographed on a Sephadex LH-20 column using a series of aqueous methanol and ethanol-hexane mixture as eluents. The isolated compounds were tested with a cellulose TLC developed with TBA and 6% acetic acid and then visualized on UV lamp or sprayed with vanillin-HCl-EtOH. The purified compounds were flavonoids and their glycosides as follows:(+)-catechin, naringenin, salipurposide, aromadendrin, isosalipurposide, aromadendrin-7-O-𝛽-D-glucopy- ranoside and taxifolin-7-O-𝛽-D-glucopyranoside. The structures of each compounds were confirmed by 1H-NMR, 13C-NMR and mass spectra.