• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.782-783
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• 2006

Titinium carbide $(TiC_x)$ was produced by self-propagating high temperature synthesis (SHS) method. The morphology and non-stoichiometric number of the SHS product were observed by scanning electron microscopy and neutron diffractometry, respectively. Tubular titanium carbide with hole inside was formed with different non-stoichiometric number (x), which value increased with combustion temperature.

• 한국세라믹학회지
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• 제31권10호
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• pp.1231-1239
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• 1994

In this study, gel powder which had relatively high hydration reactivity in CaO and P2O5 rich composition of CaO-P2O5-SiO2-H2O system was prepared by sol-gel process and its hydrated specimen was manufactured. The it was investigated to appropriate calcination temperature in sol-gel process which hydrated specimen of gel powder have proven to strength and the effect of factors influenced strength in hydration process. The major product of before and after hydration reaction was hydroxyapatite, and crystalline phase of C-S-H was already formed during gelation process. After hydration reaction of pressed specimen, crystalline phase of C-S-P-H was formed. It was hydrated product of silicocarnotite (5CaO.P2O5.SiO2). Gel phases of C-S-H and C-S-P-H occured as a result of partial substitution of amorphous silica by P2O5 was formed. The strength of hydrated hardened body is developed by strong bonding and bridging between the gel phases of C-S-H or C-S-P-H and the crystalline products such as hydroxyapatite, Ca(OH)2 C-S-H and C-S-P-H. In addition, the ultrafine gel powder have an great effect on increase of hydration reaction.

• 한국세라믹학회지
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• 제29권12호
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• pp.942-948
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• 1992

Ultrafine iron oxide powder, {{{{ gamma }}-Fe2O3 and $\alpha$-Fe2O3, were prepared by the thermal decomposition of organometallic compounds. The formation process of powder includes the thermal decomposition and oxidation of the organometallic precursors, Fe(N2H3COO)2(N2H4)2 (A) and N2H5Fe(N2H3COO)3.H2O (B). The organometallic precursors, A and B, were synthesized by the reaction of ferrous ion with hydrazinocarboxylic acid, and characterized by quantitative analysis and infrared spectroscopy. The mechanistic study for the thermal decomposition was performed by DAT-TG. The iron oxide powder was obtained by the heat treatment of the precursors at 20$0^{\circ}C$ and $600^{\circ}C$ for half an hour in air. The phases of the resulting product were proved {{{{ gamma }}-Fe2O3 and $\alpha$-Fe2O3 respectively. The particle shape was equiaxial and the particle size was less than 0.1 ${\mu}{\textrm}{m}$. Magnetic properties of the {{{{ gamma }}-Fe2O3 powder obtained from A and B was 234 Oe of coercivity, 64.26 emu/g of saturation magnetization, 23.59 emu/g of remanent magnetization and 24.1 Oe, 47.27 emu/g, 3.118 emu/g respectively. The value of $\alpha$-Fe2O3 powder was 1.494 Oe, 0.4862 emu/g, 0.1832 emu/g and 1,276 Oe, 0.4854 emu/g, 0.1856 emu/g respectively.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.773-774
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• 2006

Gas surface treatment is considered to be effective for titanium because of its high reactivity. In this study, we investigated the gas nitriding mechanism in titanium sintered parts produced by metal powder injection molding (MIM) process. The microstructure and nitrogen content of sintered MIM parts were greatly affected by nitriding conditions. Nitriding process strongly depended on the specimen size, for example, the size of micro metal injection molding (${\mu}-MIM$) product is so small and the specific surface is so large that the mechanical and functional properties can be modified by nitriding.

• 한국식품과학회지
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• 제26권3호
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• pp.305-309
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• 1994

이축압출성형기를 사용하여 붉은 통팥과 옥수수전분을 원료로 하여 압축성형하고 이를 건조, 분쇄, 배합하여 즉석팥죽 분말을 제조하였으며 이때의 제조공정과 제품의 품질을 검토하였다. 원료의 수분함량 $24{\sim}26%$, 압출성형온도 $150{\sim}155^{\circ}C$, 스크류의 회전속도 350 rpm 및 원료투입량 60 kg/hr의 압출성형조건으로 제품을 생산하였을 경우 팥죽 고유의 냄새와 색상을 유지하는 제품을 얻을 수 있었다. 압출성형중 분말원료에 가해지는 가수량이 6 kg/hr에서 2 kg/hr로 감소됨에 따라서 압출성형온도는 $150^{\circ}C$에서 $198^{\circ}C$로, 기계적소모에너지는 134 kwh/ton에서 144 kwh/ton으로 증가하였다. 건조분말상태에서 caking이 형성이 되지 않는 수분함량인 4% 이하로 건조되는 열풍건조 조건은 건조온도 $80^{\circ}C$ 에서는 4시간, $100^{\circ}C$ 에서는 1.5시간 이었다. 압출물의 분쇄후 분말의 입도분석은 체목이 0.5 mm인 것을 사용하였을 경우 약 80%가 65 mesh 체를 통과하였고, 1 mm인 체목인 경우는 약 65%가 65 mesh 체를 통과하였다. 최종배합제품의 수분흡수속도는 설탕배합구가 100% RH하에서 13시간이 경과된 후 caking이 형성되었다. 팥압출물분말, 옥수수전분 및 설탕의 배합비를 달리한 제품의 기호도 검사에서 팥의 함량이 줄어듬에 따라 팥죽냄새가 감소하여 기호성이 저하되었다.

• 유기물자원화
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• 제19권2호
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• pp.33-40
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• 2011

본 연구는 지렁이 분말을 이용하여 음식물쓰레기 처리 후 발생되는 부산물과 혼합하여 해수류 어류 사료로 활용하여, 음식물쓰레기 염분문제, 영양소 문제 및 수입사료 대체 효과를 통하여 음식물쓰레기의 안정적 처리와 부산물의 다각도 활용도 가능성을 목적으로 행한 실험결과 음식물쓰레기 부산물 및 지렁이 분말의 조단백질(25.93%,69.72%), 조지방(16.91%,6.39%) 및 조회분(15.38%, 5.30%) 등이 각각 국내 제조어분의 함량보다 높게 나타났으며 C18:1n9c, 1n9t 및 c16:0등의 함유로 지방산 공급원으로 좋은 원료로 사용 가능 할 것으로 나타났다. 사료원료의 안정성은 검정항목의 기준치 이하로 사료원료 활용시 안정성이 높은 것으로 나타났으며 음식물쓰레기 부산물과 지렁이 분말을 각각 S1=5:5, S2=6:4, S3=9:1, S4=8:2및 S5=7:3의 비율과 음식물쓰레기:지렁이 분말:분변토의 혼합비를 각각7:1:2로 하였을때 부산물 혼합비율에 대한 성분의 함량 변화는 크지 않았으나 조회분, 조섬유 및 조지방 등의 항목에서는 분변토 혼합시료(S6)가 높게 나타나 향 후 분변토 활용도 가능성이 높은 것으로 나타났다. 또한 전체적으로 등록성분의 조단백질, 조지방, 조회분 및 조섬유의 함량이 국내 제조 타 시료원료 보다 성분 함량이 높아 해수 사료 제조시 어분 대체 물질로 가능 한 것으로 나타나 향 후 경제성 분석 및 제조 가능 기술 등 다양한 연구가 필요한 것으로 판단된다.

• 한국결정성장학회지
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• 제27권5호
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• pp.223-228
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• 2017

Aluminum nitride (AlN) powder was successfully synthesized at low temperature via carbothermal reduction and nitridation (CRN) assisted by microwave heating. The synthesis processes of AlN powder were investigated with X-ray diffraction, FE-SEM, FT-IR and TGA/DSC. Aluminum nitrate was used as an oxidizer and aluminum source, urea as fuel, and glucose as carbon source. These starting materials were mixed with D.I water and reacted in a flask at $100^{\circ}C$ for 20 minutes. After the reaction was finished, black foamy intermediate product was formed, which was considered to be an amorphous $Al_2O_3$ particles through intermediate product obtained by solution combustion synthesis (SCS) at the results of X-ray diffraction patterns and FT-IR. This intermediate product was nitridated at temperatures of $1300^{\circ}C$ and $1400^{\circ}C$ in $N_2$ atmosphere by a microwave heating furnace and then decarbonated at $600^{\circ}C$ for 2 hours in air. It should be noticed from FE-SEM images that as nitridated particles, identified as AlN from X-ray diffraction patterns, are covered with carbon residues. After decarbonating the nitridated powders, the spherical pure AlN powders were obtained without alumina and their particle sizes were dependent on the nitridating temperature with high temperature of $1400^{\circ}C$ giving large particles of around 70~100 nm.

• Bulletin of the Korean Chemical Society
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• 제21권7호
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• pp.715-719
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• 2000

A ceramic powder of destructive adsorbent was synthesized by impregnating copper and manganese on the surface of silica aerosil@. In-site FTIR measurements on pulses of malodorant tert-butylmercaptan injected over the powder showed that rert-butylmercaptan dimerized into di-tert-hutyldisulfide on the surface of the adsorbent in an ambient condition. GC/MS measurement on the gas over the adsorbent showed no tert-butylmercaptan remaining, and showed only the dimerization product of di-tert-butyldisulfide. Most of the dimerization product, di-tert-butyldisulfide,remained on the surface of the adsorbent as physisorbed condense, and apparently Iowered the destruction efficiency by blocking the surface from the access by tert-butylmercaptan. Upon being heated above $100^{\circ}C$ it was observed that the physisorbed di-tert-butyldisulfide dissociated back into tert-butylmercaptan. tert-butylmercaptan physisorbed on the activated carbon, thereby no dimerization was occurring on the surface of the activated carbon. In an argn environment, the dimerization reaction was practically not occurring even on the surface of the adsorbent, indicating the free oxygen in air was also participating in the dimerization reaction. Water was identified as a by-product of the dimerization reaction. Possible reactions on the surface of the adsorbent were proposed.

• Animal Bioscience
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• 제34권12호
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• pp.1963-1973
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• 2021

Objective: The present study aimed to evaluate the influence of including L-glutamine along with glutamic acid as a supplement in weaned piglets' diets with and without whey powder. Methods: Two assays were carried out. A total of 40 piglets ([Landrace×Large White]×Pietrain) weaned at 24 days of age with an initial body weight of 6.6±0.6 kg were used in the first assay, and the following parameters were evaluated: growth performance, the incidence of diarrhea, morphometry, intestinal integrity, and hepatic glycogen index. The animals were then blocked into four groups according to different diets: diet all-grain feeding (G); diet all-grain feeding with whey powder (GW); and with vs without 1% supplementation of the commercial product containing L-glutamine and glutamic acid (A or NA). Whey powder was added according to the stage of life, corresponding to 17%, 10%, and 5%, respectively, in order to meet the need for lactose. The animals were evaluated at 24 to 42 days and at 24 to 55 days of age. The nutrient digestibility for the second assay was carried out by using 24 animals with an average weight of 11.49±1.6 kg, and the same diets were tested. Results: The supplementation of L-glutamine + glutamic acid or the addition of whey powder in diets for weaned piglets provided (p<0.05) greater feed intake, greater weight gain and improved feed conversion in the initial period (24 to 42 days age). However, in the whole period (24 to 55 days age) only amino acid supplementation affected (p<0.05) growth performance. There was a positive interaction (p<0.05) between the type of diet and L-glutamine + glutamic acid supplementation on villus height, crypt depth and the villus:crypt ratio in the duodenum. In addition, L-glutamine + glutamic acid supplementation reduced (p<0.05) the crypt depth and improved the villus:crypt ratio in the jejunum. The inclusion of whey powder affected (p<0.05) positively the digestibility coefficients analyzed except mineral matter digestibility coeficients. The supplementation of 1% the commercial product composed of L-glutamine and glutamic acid improved (p<0.05) only the digestibility coefficient of crude protein. Conclusion: These results indicate that supplementation of 1% commercial product containing L-glutamine + glutamic acid in diets for piglets from 24 to 55 days of age, dispenses with the use of whey powder when evaluating growth performance. Amino acid supplementation alone or associated with whey powder affects (p<0.05) positively the indicators of the intestinal integrity.

• Asian-Australasian Journal of Animal Sciences
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• 제26권6호
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• pp.886-895
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• 2013

This study was conducted to explore the antioxidant potential and functional value of guava (Psidium guajava L.) powder in muscle foods. Guava powder was used as a source of antioxidant dietary fibre in sheep meat nuggets at two different levels i.e., 0.5% (Treatment I) and 1.0% (Treatment II) and its effect was evaluated against control. Guava powder is rich in dietary fibre (43.21%), phenolics (44.04 mg GAE/g) and possesses good radical scavenging activity as well as reducing power. Incorporation of guava powder resulted in significant decrease (p<0.05) in pH of emulsion and nuggets, emulsion stability, cooking yield and moisture content of nuggets while ash and moisture content of emulsion were increased. Total phenolics, total dietary fibre (TDF) and ash content significantly increased (p<0.05) in nuggets with added guava powder. Product redness value was significantly improved (p<0.05) due to guava powder. Textural properties did not differ significantly except, springiness and shear force values. Guava powder was found to retard lipid peroxidation of cooked sheep meat nuggets as measured by TBARS number during refrigerated storage. Guava powder did not affect sensory characteristics of the products and can be used as source of antioxidant dietary fibre in meat foods.