• 제목/요약/키워드: porous layered structure

검색결과 23건 처리시간 0.047초

이중 기공구조를 갖는 다공질체의 제조 (Fabrication of Double-layered Porous Materials)

  • 윤중열;김해두;박천홍
    • 한국세라믹학회지
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    • 제39권10호
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    • pp.919-927
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    • 2002
  • 표면층과 내부간의 기공구조가 다른 다공질체를 제조하기 위해 입자크기가 다른 두 종류의 분체를 이용하여 다공질 성형체를 제조하였다. 두 층간의 소결 수축율을 동일하게 제어하기 위해 성형밀도 변화에 따른 소결밀도 변화를 예측할 수 있는 Ford's equation을 도입하여 소결 수축율을 동일한 조건을 구하였다. 제조된 다공질체는 미세구조와 통기도를 조사함으로서 기공의 이중 구조화 여부를 평가하였다. SEM 관찰결과 기공크기가 다른 두 층으로 구성되어 있는 것을 확인하였다. 각 층의 통기도는 출발 입자크기와 기공율이 클수록 증가하였으며, 이중 기공구조를 갖는 시편의 통기도는 기공크기가 작은 층의 특성에 의존하였다.

다공성 세라믹스와 다공질층을 포함하는 적층체의 제조에 관한 연구;I. 기공구조 (Fabrication of Porous Ceramics and Multi-layered Ceramics Containing Porous Layers; I. Pore Structure)

  • 이해원;윤복규;송휴섭
    • 한국세라믹학회지
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    • 제31권9호
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    • pp.1044-1052
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    • 1994
  • Tape casting technique was successfully applied to produce porous ceramics and multi-layered ceramics containing porous layers, where spherical hollow polymer particles were introduced as pore precursors. In the presence of extreme differences in density and size between Al2O3 and pore precursor particles, hindered settling was effective in preventing segregation of component particles and packing behavior of mixed powders was improved through bimodal packing. There were two transitions in packing behavior of mixed powders. The first transition took place at 40~50 vol% pore precursor addition, where majority of pores changed from close to open pore state. The other transition occured at 60~70 vol% pore precursor addition, where pore precursor particles formed a continuous network structure.

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경계요소법과 유한요소법에 의한 흡음판의 소음저감에 관한 다영역 연성해석 (Multi-Region Structural-Acoustic Coupling Analysis on Noise Reduction of Layered Structures using Finite Element and Boundary Element Technique)

  • 주현돈;서원진;이시복
    • 한국소음진동공학회:학술대회논문집
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    • 한국소음진동공학회 2000년도 춘계학술대회논문집
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    • pp.309-313
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    • 2000
  • A structural-acoustic coupling problem involving fluid in a cavity divided with flexible walls and porous materials is investigated in this paper. In many practical problems, the use of finite elements to discretize the fluid region leads to large stiffness and mass matrices. But, since the acoustic boundary element discretization requires to put elements only on the surface of structure, the size of matrices is reduced considerably. Here, we developed a numerical analysis program for the structural-acoustic coupling problems of the multi-region cavity, using boundary elements for the fluid regions and finite elements for the structure. By considering sound transmission through layered systems placed in a cavity, the accuracy of the coupled acoustical-structural finite element model has been verified by comparing its transmission loss predictions with analytical sloutions. Example problems are included to investigate the characteristics of the multi-region structural-acoustic coupling system with porous material.

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혼합가스 분위기 중에서 공업용 순 타이타늄의 고온산화 거동 (High-Temperature Oxidation Behavior of Commercial Pure Titanium in Mixed Gases)

  • 박성호;안용식
    • 동력기계공학회지
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    • 제11권2호
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    • pp.44-50
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    • 2007
  • The oxidation behavior of commercial pure titanium is investigated in the temperature range of $727^{\circ}C{\sim}950^{\circ}C$ in mixed gases. The weight change is measured by TGA during oxidation in mixed gases. The oxidation behavior indicated by weight gain or the growth of oxide layer is based on the linear rate law at high temperatures. The structure of the oxide scale formed during oxidation is analysed by optical microscopy, electron probe microanalyzer, scanning electron microscope and x-ray diffraction. Oxide scales have a $TiO_2$ structure, and are constituted with multi-layered or two layered porous external one and a dense internal one. Ti-O solid solution region is formed at the interface of metal and scale layer. The formation of oxide scale is influenced by the oxidation temperature, time, crystal structure and the condition of atmosphere.

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A New Nanohybrid Photocatalyst between Anatase (TiO2) and Layered Titanate

  • Lee, Hyun-Cheol;Jeong, Hyun;Oh, Jae-Min;Choy, Jin-Ho
    • Bulletin of the Korean Chemical Society
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    • 제23권3호
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    • pp.477-480
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    • 2002
  • A new microporous TiO2-pillared layered titanate has been successfully prepared by hybridizing the exfoliated titanate with the anatase TiO2 nano-sol. According to the X-ray diffraction analysis and N2 adsorption-desorption isotherms, the TiO2-pillared layered titanate showed a pillar height of ~2 nm with a high surface area of ~460 m2/g and a pore size of ~0.95 nm, indicating that a microporous pillar structure is formed. Its photocatalytic activity was evaluated by measuring the photodegradation rate of 4-chlorophenol during irradiation of catalyst suspensions in an aqueous solution. An enhancement in activity of ca. 170% was obtained for TiO2-pillared layered titanate compared to that of the pristine compound such as layered cesium titanate.

Co, Ni 마가다이트 주형을 이용한 다공성 흑연의 합성 (Preparation of Porous Graphite by Using Template of Co- and Ni-Magadiite)

  • 정순용
    • 한국분말재료학회지
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    • 제12권2호
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    • pp.151-158
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    • 2005
  • Porous graphite was synthesized by removal of template in HF after pyrolysis of pyrolyzed fuel oil (PFO) at $900^{\circ}C$ using the template of Co or Ni intercalated magadiite. Porous graphite had a plate structure like template, and d-spacing value of about 0.7 nm. The extent of crystallization of porous graphite was dependent on the contents of Co or Ni intercalated in interlayer. It can be explained that the metal such as Co and Ni acts as a promotion catalyst for graphite formation. Porous graphite shows the surface area of $328\sim477 m^2/g$.

Scattering of torsional surface waves in a three layered model structure

  • Gupta, Shishir;Pati, Prasenjit;Mandi, Anand;Kundu, Santimoy
    • Structural Engineering and Mechanics
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    • 제68권4호
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    • pp.443-457
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    • 2018
  • In this article, a comparative study has been made to investigate the scattering behaviour of three layered structure model on torsional surface wave. For such model intermediate layer is taken as fiber reinforced composite, resting over a dry sandy Gibson substratum and underlying by different anelastic media. We consider two distinct mediums for topmost layer. In the first case, topmost layer has been taken as fluid saturated homogeneous porous layer, while in the second case the fluid saturated porous layer has been replaced by a transversely isotropic layer. Simple form expression for the secular equation of torsional surface wave has been worked out in both the cases by executing specific boundary conditions, which comprises Whittaker's function and its derivative, for imminent result that have been elaborated asymptotically. Some special cases have been constituted which are in excellent compliance with recorded literatures. For the sake of comparative study, numerical estimation and graphical illustration have been accomplished to identify the effects of the width ratio of the layers, Biot's gravity parameter, sandy parameter, porosity parameter and other heterogeneity parameters corresponding to the layers and half spaces, horizontal compressive and tensile initial stress on the phase velocity of torsional surface wave.

Size-dependent magneto-electro-elastic vibration analysis of FG saturated porous annular/ circular micro sandwich plates embedded with nano-composite face sheets subjected to multi-physical pre loads

  • Amir, Saeed;Arshid, Ehsan;Arani, Mohammad Reza Ghorbanpour
    • Smart Structures and Systems
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    • 제23권5호
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    • pp.429-447
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    • 2019
  • The present study analyzed free vibration of the three-layered micro annular/circular plate which its core and face sheets are made of saturated porous materials and FG-CNTRCs, respectively. The structure is subjected to magneto-electric fields and magneto-electro-mechanical pre loads. Mechanical properties of the porous core and also FG-CNTRC face sheets are varied through the thickness direction. Using dynamic Hamilton's principle, the motion equations based on MCS and FSD theories are derived and solved via GDQ as an efficient numerical method. Effect of different parameters such as pores distributions, porosity coefficient, pores compressibility, CNTs distribution, elastic foundation, multi-physical pre loads, small scale parameter and aspect ratio of the plate are investigated. The findings of this study can be useful for designing smart structures such as sensor and actuator.

다층 기공구조를 갖는 다공성 반응소결 탄화규소 다공체 제조 (Fabrication of Porous Reaction Bonded Silicon Carbide with Multi-Layered Pore Structures)

  • 조경선;김규미;박상환
    • 한국세라믹학회지
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    • 제46권5호
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    • pp.534-539
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    • 2009
  • Reaction Bonded Silicon Carbide(RBSC) has been used for engineering ceramics due to low-temperature fabrication and near-net shape products with excellent structural properties such as thermal shock resistance, corrosion resistance and mechanical strength. Recently, attempts have been made to develop hot gas filter with gradient pore structure by RBSC to overcome weakness of commercial clay-bonded SiC filter such as low fracture toughness and low reliability. In this study a fabrication process of porous RBSC with multi-layer pore structure with gradient pore size was developed. The support layer of the RBSC with multi-layer pore structure was fabricated by conventional Si infiltration process. The intermediate and filter layers consisted of phenolic resin and fine SiC powder were prepared by dip-coating of the support RBSC in slurry of SiC and phenol resin. The temperature of $1550^{\circ}C$ to make Si left in RBSC support layer infiltrate into dip-coated layer to produce SiC by reacting with pyro-carbon from phenol resin.