• 제목/요약/키워드: pore volume test

검색결과 116건 처리시간 0.024초

Consolidation Test Method Considering Sample Deformation Due to Stress Release by Sampling (시료채취에 의한 응력해방시 시료변형을 고려한 압밀시험)

  • Kim Jae-Young;Takada Naotoshi
    • Journal of the Korean Geotechnical Society
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    • 제20권7호
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    • pp.99-105
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    • 2004
  • When a saturated clay is sampled from a borehole in an undisturbed manner, the exerted negative pore water pressure restricts the volume expansion. The vertical and horizontal stresses to which the clay was subjected in the ground are smaller and larger than this isotropically confining stress equivalent to the mean principal stress in the ground, respectively. Therefore the sample expands vertically and shrinks laterally under an undrained condition. In the ordinary consolidation test, the sample thus deformed is trimmed to fit the inside of the consolidometer ring. Thus, the specimen generates larger consolidation displacement due to confining larger horizontal stress when in-situ effective pressure is loaded. The specimen does not reproduce the in-situ consolidation behavior, In this paper, considering sample deformation, the test specimen is made to expand laterally to fit the inside of the ring in the undrained manner when the in-situ effective pressure is loaded. And applicability of this proposed test procedure was verified; results from the conventional consolidation test procedure are also discussed.

Hot Water Resistance of Polymer Mortar Composites Depending on Unsaturated Polyester Resin Types (불포화폴리에스테르 수지의 형태에 따른 폴리머 모르타르 복합재료의 내열수성)

  • Hwang, Eui-Hwan;Song, Min-Kyu;Kim, Yong-Yeon
    • Applied Chemistry for Engineering
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    • 제29권2호
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    • pp.201-208
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    • 2018
  • The ortho- and iso- type unsaturated polyester resins were synthesized and used as a polymer binder of the polymer mortar composite. Styrene monomer and acrylonitrile were used as a diluent for the unsaturated polyester resin. Methyl ethyl ketone peroxide (MEKPO) and cobalt octoate (CoOc) were used as a curing agent and an accelerator, respectively. Four kinds of unsaturated polyester resins were prepared according to types of the resin and diluent, and used as a polymer binder in the preparation of the specimen. A total of 16 polymer mortar specimens were prepared according to the added amount of the polymer binder and subjected to a hot water resistance test, followed by compressive and flexural strength tests, and pore and SEM analyses. As a result, it was found that the strength of the specimen using the iso-type unsaturated polyester resin as the polymer binder was better than that of using the ortho-type unsaturated polyester resin. The total pore volume and diameter measured after the hot water resistance test were reduced compared to the values before the test. In the micrographs observed before the hot water resistance test, the polymer binder, filler and fine aggregate were firmly combined to the co-matrix, but the polymer binder was mostly decomposed in the micrographs observed after the test.

Effect of Pore Structures of a Ti-49.5Ni (at%) Alloy on Bone Cell Adhesion (Ti-49.5Ni (at%)합금의 다공성 구조가 뼈 세포 흡착에 미치는 영향)

  • Im, Yeon-Min;Choi, Jung-Il;Khang, Dong-Woo;Nam, Tae-Hyun
    • Korean Journal of Materials Research
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    • 제22권2호
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    • pp.66-70
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    • 2012
  • Ti-Ni alloys are widely used in numerous biomedical applications (e.g., orthodontics, cardiovascular science, orthopaedics) due to their distinctive thermomechanical and mechanical properties, such as the shape memory effect, superelasticity and low elastic modulus. In order to increase the biocompatibility of Ti-Ni alloys, many surface modification techniques, such as the sol-gel technique, plasma immersion ion implantation (PIII), laser surface melting, plasma spraying, and chemical vapor deposition, have been employed. In this study, a Ti-49.5Ni (at%) alloy was electrochemically etched in 1M $H_2SO_4$+ X (1.5, 2.0, 2.5) wt% HF electrolytes to modify the surface morphology. The morphology, element distribution, crystal structure, roughness and energy of the surface were investigated by scanning electron microscopy (SEM), energy-dispersive Xray spectrometry (EDS), X-ray diffractometry (XRD), atomic force microscopy (AFM) and contact angle analysis. Micro-sized pores were formed on the Ti-49.5Ni (at%) alloy surface by electrochemical etching with 1M $H_2SO_4$+ X (1.5, 2.0, 2.5) wt% HF. The volume fractions of the pores were increased by increasing the concentration of the HF electrolytes. Depending on the HF concentration, different pore sizes, heights, surface roughness levels, and surface energy levels were obtained. To investigate the osteoblast adhesion of the electrochemically etched Ti-49.5Ni (at%) alloy, a MTT test was performed. The degree of osteoblast adhesion was increased at a high concentration of HF-treated surface structures.

Characteristics of EVA-Polymer Modified Mortars Recycling Rapid-chilled Steel Slag Fine Aggregate (급냉 제강슬래그를 재활용한 EVA-폴리머 시멘트 모르타르의 특성)

  • Hwang, Eui-Hwan;Kim, Jin-Man
    • Applied Chemistry for Engineering
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    • 제19권6호
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    • pp.652-660
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    • 2008
  • For the recycling of rapid-chilled steel slag, the mechanical strengths and physical properties of EVA-polymer modified mortars with the various replacement ratios of rapid-chilled steel slag were investigated. Twenty five specimens of polymer modified mortars were prepared with the five different amounts of EVA-polymer modifier (0, 5, 10, 15, 20 wt%) and rapid-chilled steel slag (0, 25, 50, 75, 100 wt%). For the investigation of the characteristics of polymer modified mortars, the measurements such as water-cement ratio, unit volume weight, air content for fresh mortar and compressive strength, flexural strength, water absorption, hot water resistance, porosity and SEM investigation for curing specimens were conducted. As a results, with an increase in the replacement ratio of rapid-chilled steel slag, water-cement ratios decreased but unit volume weight increased remarkably. With increasing EVA-polymer modifier and the replacement ratio of rapid-chilled steel slag, percent of water absorption decreased but compressive and flexural strengths increased remarkably. By the hot water resistance test, mechanical strengths decreased but total pore volume and porosity increased remarkably. In the SEM observation, the components of specimen were shown to stick to each other in the form of co-matrix phase before hot water resistance test, but polymer modifier of co-matrix phase was decomposed or deteriorated after hot water resistance test.

Evaluation for Contents of Contaminants and Leaching Characteristics of Bottom Ash (바텀애쉬의 유해물질 함량 측정 및 용출특성 평가연구)

  • Koh, Taehoon;Lee, Sungjin;Shin, Minho;Kim, Byongsuk;Lee, Jeakeun;Lee, Taeyoon
    • Journal of the Korean GEO-environmental Society
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    • 제11권6호
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    • pp.77-83
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    • 2010
  • In this study, we tried to determine any detrimental effects on water quality when bottom ash obtained from a coal-fired power plant intended to be used as a fill material in construction sites. Physical-chemical properties of bottom ash were determined using proximate analysis, elemental analysis, XRD, and XRF. Classification of bottom ash as a waste material and soil contamination due to the use of bottom ash were performed by Korea waste standard leaching test and soil toxicity test, respectively. Results of leaching tests were compared to the regulations for water quality and groundwater quality and no harmful effects on water quality were found. Most of heavy metals in leachate were below detection limits but trace amount of $Cr^{6+}$ was found. However, concentration of $Cr^{6+}$ was below the regulation criteria. Column leaching tests indicated that concentrations of Pb and Zn were slightly higher than regulations but below regulations within 1 PVE, but concentrations of sulfate were 10 times higher than regulation and thus, the required time to reach regulation was almost 8 PVE.

Classification of Alkali Activated GGBS Mortar According to the Most Suitable Usage at the Construction Site

  • Thamara, Tofeti Lima;Ann, Ki Yong
    • Journal of the Korean Recycled Construction Resources Institute
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    • 제8권1호
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    • pp.56-63
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    • 2020
  • The usage of OPC-free alkali activated ground granulated blast furnace slag(GGBS) mortar has been widely studied on the previous years, due to its advantages on sustainability, durability and workability. This paper brings a new view, aiming to classify the best application in situ for each mortar, according to the type and activator content. By this practical implication, more efficiency is achieved on the construction site and consequently less waste of materials. In order to compare the different activators, the following experiments were performed: analysis of compressive strength at 28 days, setting time measured by needles penetration resistance, analysis of total pore volume performed by MIP and permeability assessment by RCPT test. In general, activated GGBS had acceptable performance in all cases compared to OPC, and remarkable improved durability. Following the experimental results, it was confirmed that each activator and different concentrations impose distinct outcome performance to the mortar which allows the classification. It was observed that the activator Ca(OH)2 is the most versatile among the others, even though it has limited compressive strength, being suitable for laying mortar, coating/plaster, adhesive and grouting mortar. Samples activated with NaOH, in turn, presented in general the most similar results compared to OPC.

Fracture Analysis of Porous Titanium for Dental Implant Fabricated by Space Holder Process (Space holder 공정으로 제조된 치과 임플란트용 타이타늄 다공체의 파손 분석)

  • Lee, Seung-Mi;Jang, Jin-Man;Lee, Won-Sik;Byeon, Jai-Won
    • Journal of Applied Reliability
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    • 제16권2호
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    • pp.104-109
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    • 2016
  • Purpose: The purpose of this study is to analyze fracture behavior and failure mechanism of porous titanium for dental implant fabricated by space holder process. Method: Three porous titanium specimens with a specific volume fraction of open pore were test by 3 point bending and compression stress condition, respectively. Fracture appearance was observed by scanning electron microscope and discussed in relation with oxygen content. Results: For compression-tested specimens, two specimen showed brittle failure, while the other one showed normal failure after deformation. High oxygen content was detected in the brittle-fractured specimen. Several micro-cracks initiated at the struts propagated down to the bottom of the specimen resulting in normal failure. Conclusion: Oxygen contamination during the fabrication process can leads brittle premature failure, and hence quality problem of the porous titanium for dental implant.

Effects of cow manure compost on anion elution patterns and hydraulic conductivity (우분퇴비 처리에 따른 토양내 음이온의 용출특성과 투수특성 변화)

  • 정덕영;김필주;박무언;이병렬;김건엽
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 한국지하수토양환경학회 1996년도 경북지부 결성 및 추계학술발표회 논문집
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    • pp.131-139
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    • 1996
  • To quantitatively investigate the effects of manure compost on the soil and water environment including ground water the elution patterns of anions and hydraulic conductivity wore estimated with four different depth(15, 30, 45 60cm) and four variable ratio of compost treatment(0, 2, 4, 6%) through soil column test. 1. There were over 95% of elution of chloride and nitrate within 0.1 pore volume(PV), and sulfate within 0.2 PV. With 2 ton/10a of cow manure compost treatment recommended total 40 kg/10a of anions added was recovered as effluent at the amount of 17kg chloride, 5.4kg nitrate, and 13.2kg sulfate, respectively However, phosphate rarely recovered in the effluent due to the strong affinity for sorption sites in soils. 2. In multi-layered soil column the maximum peaks of each anion eluted were retardated with increasing soil depth and the amount of organic matter(OM) treatment. 3. With increasing OM up to 2% the saturated hydraulic conductivity(SHC) was greatly decreased, but the slight decrease in SHC was found by addition of OM greater than 4%. In multi-layered soil column SHC was more effected by the lower SHV layer than by that of the higher.

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Investigation of Demixing Phenomena of a Polymer Solution During the Phase Inversion Process

  • Han, Myeong-Jin;D. Bhattacharyya
    • Proceedings of the Membrane Society of Korea Conference
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    • 한국막학회 1995년도 춘계 총회 및 학술발표회
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    • pp.11-15
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    • 1995
  • Polysulfone (PS) membranes were prepared by the phase inversion process using water or isopropanol as nonsolvent. The Flory-Huggins theory for a ternary system nonsolvent/solvent/polymer is applied to describe the thermodynamic equilibria of the components. The calculated ternary phase equilibria show that demixing of a PS binary solution with n-methylpyrrolidone (NMP) will be fast in a water coagulation bath and will be delayed in an isopropanol bath. The prepared membranes were characterized by SEM, gas adsorption-desorption measurement, and permeability test. The membrane, which is precipitated by fast demixing in a water bath, has nodular structures in the skin region and includes finger-like cavities in the sublayer. The membrane coagulated by isopropanol has a very dense and thick skin structure, which is formed by delayed demixing. The membrane coagulated by isopropanol showed considerably lower pore volume and surface area compared to that observed with water coagulation method. With dimethylformamide (DMF) as solvent and 2-3 wt% of water, the solution can show the liquid-liquid phase separation due to agglomation of the polymer-lean phase from the homogeneous solution. The membranes, which were coagulated near an equilibrium state, show the large (micron size) round pores in the whole membranes. The pores do not contribute the permeation characteristics.

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Properties of Sponge Cake with Added Saltwort (Salicorniaherbacea L.) (함초 분말을 첨가한 스폰지 케이크의 품질특성)

  • An, Ho-Ki;Hong, Geum-Ju;Lee, Eun-Jun
    • Journal of the Korean Society of Food Culture
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    • 제25권1호
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    • pp.47-53
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    • 2010
  • This study was conducted to investigate the effects of saltwort, on the quality characteristics of sponge cake. In addition, we examined the commercialization potential of sponge cake containing saltwort. To accomplish this, saltwort was added to sponge cakes at concentrations of 0%, 3%, 5% and 7% and quality and sensory tests were then conducted. The 7% group had the highest water and ash content. There was no difference in the fat content between samples. The control group showed the highest protein content and the lowest specific gravity. As the content of saltwort increased, the specific gravity of the sponge cake increased. Additionally, the dough yield and loss during baking were highest, in the control group, and these values decreased as the saltwort content increased. Similarly, the volume and specific volume were highest in the control group, and these values decreased as the content of saltwort powder increased. Color measurements of the samples, revealed that the L-value decreased as the content of saltwort powder increased. Furthermore, the a-value of the saltwort powder groups was higher than that of the control group and the b-value was highest in the 7% group. There were no differences in elasticity and cohesion between samples, but chewiness and brittleness increased the content of saltwort powder increased. The results of the sensory test revealed that the color, flavor and taste scores were the highest in the 5% group. The pore size was greatest in the control group, while hardness was greatest in the 7% group, chewiness was highest in the 5% group and moistness was highest in the 5% group. Finally, the overall preference was for the 5% group.