• Title/Summary/Keyword: pore size measurement

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Prediction of Intrinsic Pore Properties of Ultrafiltration Membrane by Solute Rejection Curves (용질배제 곡선에 의한 한외여과 막의 세공특성 예측)

  • 염경호
    • Proceedings of the Membrane Society of Korea Conference
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    • 1991.10a
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    • pp.4-8
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    • 1991
  • The characterization of pore properties (mean pore size and pore size distribution) of the active layer in a UF membrane is important not only in order to obtain information about the factors affecting pore formation during membrane manufacturing but also to understand deeply the mechanism of solute and solvent transport through pores. Many methods of characterizing quantitatively the pore properties of UF membranes have been suggested in the literature: solvent and gas flow measurement, bubble point determination, electron microscopy, gas adsorption/desorption measurement, rejection measurement etc. But most of these methods involve time-consuming procedures and involve some wellknown problems and uncertainties.

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Fabrication of nanohoneycomb structures and measurement of pore sizes (나노허니컴 구조물의 제작 및 홀 사이즈 측정)

  • Choi, Duk-Kyun;Lee, Pyung-Soo;Hwang, Woon-Bong;Lee, Kun-Hong
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2005.04a
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    • pp.265-268
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    • 2005
  • A new method for measurement of the pore size in a nanohoneycomb structure using atomic force microscopy (AFM) was proposed. Porous type anodic aluminum oxide (AAO) was fabricated as a nanohoneycomb structure to measure the pore size. For measuring pore sizes from AFM images, a criterion was set in porous type AAO. The pore sizes from AFM images were compared with those from SEM images, and the results showed good agreement. The relationship between the pore size and widening time was found to be linear in the range of this study. It was understood as the synchronized effects of the impurity gradient in outer oxide of AAO, mechanical packing and mass transfer increase.

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A progressive study of the sausage mode wave on the pore: the pore-selection technique

  • Cho, Il-Hyun;Kim, Yeon-Han;Cho, Kyung-Suk;Bong, Su-Chan;Park, Young-Deuk
    • The Bulletin of The Korean Astronomical Society
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    • v.38 no.1
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    • pp.66.2-66.2
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    • 2013
  • In this study, we present a pore-selection technique to estimate the size of pore. The estimation of the size of pore is important to examine the temporal evolution of size itself and corresponding intensity. The size of pore is typically estimated by applying the intensity threshold technique to the fixed box which contains the entire pore. The typical method has disadvantages in the following circumstances; there are small features near the pore or the image has low spatial resolution. In the former, it is difficult to define a box containing the pore only, excluding the small features near the pore. In the latter, the background and threshold intensity are insignificant due to the insufficient number of pixel in the box. To avoid these difficulties, we use a pore-selection technique which is simply based on the measurement of distances from the pore center. In addition, we will discuss the advantage of the technique for the imaging spectrograph data like the NST FISS.

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A Novel Technoque for Characterization of Membranes

  • Webber, Ronald;Jena, Akshaya;Gupta, Krishna
    • Proceedings of the Membrane Society of Korea Conference
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    • 2001.10a
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    • pp.39-50
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    • 2001
  • The performance of membranes is governed their pore struture. Pore structures of porous materials can be determined by a number of techniques. However, The novel technique, capillary folw porometry has a number of advantages. In this technique, the sample is brought in contact with a liquid that fills the pores in the membrane spontaneously. Gas under pressure is used to force the liquid from the pores and increase gas flow. Gas flow rate measured as a function of gas pressure in wet and dry samples yield data on the largest pore size, the mean flow pore size, flow distribution and permeability. Pore characteristics of a number of membranes were measured using this technique. This technique did not require the use of any toxic material and the pressure employed was low. Capillary flow porometry is a suitable technique for measurement of the pore structure of many membranes.

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Pore Characteristics of Porous Alumina Ceramics Fabricated from Boehmite Hydrosol and Alumina Particles (Boehmite 수화졸의 알루미나로 제조한 다공성 알루미나 세라믹스의 기공특성)

  • 오경영
    • Journal of the Korean Ceramic Society
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    • v.33 no.5
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    • pp.547-555
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    • 1996
  • Porous alumina ceramics were fabricated by pseudo-boehmite phydosol-gel process within/without commercial $\alpha$-alumina particles average 1 and 40 micron respectively. The pore characteristics of fired specimens were studied by the measurement of bulk density total porosity thyermal analysis pore volume pore distribution BET area XRD and SEM. with increasing of firing temperature pore volume and BET surface area were decreased and the average pore size was increased to approximately 146$\AA$ upto 80$0^{\circ}C$ by de-watering of [OH] and formation of $\alpha$-alumina. The fired relative density of the alumina-dispersed specimen with average 1 micron particle was increased with the amounts of dispersed particle by bimodal packing theory which is compared to the ones of specimen including of average 40 micron particle. It was confirmed that the percola-tion threshold in porous ceramics with coarser particle (40 micron) has formed between the transformed-alumina from hydrogel and dispersed-alumina of above 50 vol% particle and the total porosity was increased at the threshold point above.

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Analysis of Pore Structure for Porous Body with Coal Fly ash and Clay (석탄회-점토계 다공체의 기공구조 분석)

  • 이기강;박천주
    • Korean Journal of Crystallography
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    • v.9 no.1
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    • pp.64-70
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    • 1998
  • Porous body was prepared from coal fly ash 70 wt%0clay 30 wt% slip using DCC(Direct Coagulated Casting) method. Effect of the specific gravity of the slip on the pore size and distribution of the sintered body was examined by the SEM observation of microstructure and mercury porosimetry measurement of the pore size distribution. Average pore size of the porous sintered body was about 2.5μm for all slips with specific gravity of 1.55, 1.60 and 1.65g/cm3, respectively. Sintered body prepared from the slip of specific gravity of 1.60g/cm3 have the narrowest pore size distribution. slip of specific gravity of 1.55g/cm3 shows broader pore size distribution due to slow gellation process. Slip of specific gravity of 1.65g/cm3 required large amount of deflocculant and showed large variation of the viscosity with addition of coagulant which resulted in very unstable slip properties.

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Studies on the Pore of Coating Layer and Printability (IV) -Effects of Blending Ratio of Pigments- (도공층의 공극과 인쇄적성에 관한 연구(제4보) -안료 배합 비율이 미치는 영향-)

  • 김창근;이용규
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.33 no.3
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    • pp.29-36
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    • 2001
  • This paper was made to evaluate the effect of the blending ration of GCC and No. 1 clay on the printability by investigating the structure of pore such as the pore rate, the number of pores, pore size and distribution of coated paper. The coated structure is mainly depended on the results of correlation between pigment and binder. It means that the structure of the pore occurred is chiefly affected by the blending ratio of GCC and No. 1 clay. This physical properties of the pore have a close relation with ink set-off associated with the drying rate and the penetration in ink into base paper and with printing gloss. Therefore it was needed to find out how the pore structure and the printability will be changed by modifying the blending ratio of GCC and No. 1 clay to vary the pore structure of coated paper. Below are the results of measurement: As the blending ratio of clay going up, water retention, sedimentation volume. smoothness, and paper gloss were increased, but relatively brightness and opacity were decreased. Pore rate was the highest at the blending ratio of No. 1 clay to GCC, 70:30. In this case, average pore radius was also increased. Ink receptivity and K&N ink receptivity were improved with the increase of the blending ratio of GCC, where was, ink setting was vice versa. No difference was observed in the weight of ink, but ink repellance decrease with the decrease of blending ratio of GCC.

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Indentation Damage of Porous Alumina Ceramice

  • Ha, Jang-Hoon;Lee, Chul-Seung;Kim, Jong-Ho;Kim, Do-Kyung
    • Journal of the Korean Ceramic Society
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    • v.41 no.1
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    • pp.19-23
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    • 2004
  • The Hertzian indentation contact damage behavior of porous alumina with controlled pore shape was investigated by experiments. Porous alumina ceramics containing well-defined pore shape, size and distribution were prepared by incorporation of fugitive spherical starch. Porous alumina with isolated pore structure was prepared with porosity range up to 30%. The indentation stress-strain curves of porous alumina were constructed. Elastic modulus and yield stress can be obtained from the stress-strain relationship. Impulse excitation method for the measurement of elastic modulus was also conducted as well as Hertzian indentation and was confirmed as a useful tool to evaluate the elasticity of highly porous ceramics. Elastic modulus of the inter-connected pore structure is more sensitive to porosity than that of the isolated pore structure. When the specimen had isolated pore structure, higher yield point was obtained than it had inter-connected pore structure. This study proposed that the elastic modiulus of porous ceramics is strongly related to not only porosity, but also the structure of pore.

STUDIES FOR THE CHARACTER OF THE POROUS SILICA CONTAINING THE NANO-SIZED TIO$_2$, PARTICLE IN THE PORE.

  • Jhun, Hyun-pyo;Kong, Woo-sik;Lee, Kyoung-chul
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.24 no.3
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    • pp.59-64
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    • 1998
  • In order to lower porosity of the porous silica, titanium alkoxide solution was filled in the pore of silica in the heating-vacuum condition. The specific surface area of modified samples was decreased effectively from 900 m$^2$/g to 100 m$^2$/g. (The aggregation phenomena in modified samples were improved fairly.) Samples were heated at 600 , and then the titanium alkoxide in the pore was decomposed completely to titanium oxide from TGA-DTA measurement. From SEM result, it was evident that titanium oxide did not coat the surface of the silica. The modified samples were analyzed using SEM, DTA-TGA, BET, and UV-visible spectrometer.

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CHARACTERISTICS OF RESIDUAL CARBON DERIVED FROM THE COMBUSTION OF VACUUM RESIDUE IN A TEST FURNACE

  • Park, Ho-Young;Seo, Sang-Il
    • Environmental Engineering Research
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    • v.12 no.3
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    • pp.109-117
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    • 2007
  • The characteristics of carbonaceous particles collected from the combustion of Vacuum Residue (VR) in a test furnace have been investigated. The physical and chemical characterization includes particle size, scanning electron microscopy of the surface structure, measurement of porosity, surface area and density, EDX/XRD analyses and measurement of chemical composition. The studies show that the carbonaceous VR particles are very porous and spheroidal, and have many blow-holes on the surface. The particles become smaller and more sponge-like as the reaction proceeds. The present porosity of VR particles is similar to that of cenospheres from the combustion of heavy oil, and the majority of pores are distributed in macro-pores above $0.03\;{\mu}m$ in diameter. Measurements of pore distribution and surface area showed that the macro-pores contributed most to total pore volume, whereas the micro-pores contributed to total surface area.