• 제목/요약/키워드: planetary ball

검색결과 105건 처리시간 0.025초

아연-공기전지용 페롭스카이트 산화물 촉매의 산소환원반응 특성 (Characterization of LaCoO3 Perovskite Catalyst for Oxygen Reduction Reaction in Zn-air Rechargeable Batteries)

  • 선호정;조명연;안정철;엄승욱;박경세;심중표
    • 한국수소및신에너지학회논문집
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    • 제25권4호
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    • pp.436-442
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    • 2014
  • $LaCoO_3$ powders synthesized by Pechini process were pulverized by planetary ball-milling to decrease particle size and characterized as a catalyst in alkaline solution for oxygen reduction and evolution reaction (ORR & OER). The changes of physical properties, such as particle size distribution, surface area and electric conductivity, were analyzed as a function of ball-milling time. Also, the variations of the crystal structure and surface morphology of ball-milled powders were examined by X-ray diffraction (XRD) and scanning electron microscopy (SEM), respectively. The electrochemically catalytic activities of the intrinsic $LaCoO_3$ powders decreased with increasing ball-milling time, but their electrochemical performance as an electrode improved by the increase of the surface area of the powder.

기계적 합금화 공정을 이용한 초미세 자성연마입자의 제조 및 특성 평가 (Fabrication of the Fine Magnetic Abrasives by using Mechanical Alloying Process and Its Polishing Characteristics)

  • 박성준;이상조
    • 한국정밀공학회지
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    • 제21권10호
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    • pp.34-41
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    • 2004
  • A new method to fabricate the fine magnetic abrasives by using mechanical alloying is proposed. The mechanical alloying process is a solid powder process where the powder particles are subjected to high energetic impact by the balls in a vial. As the powder particles in the vial are continuously impacted by the balls, cold welding between particles and fracturing of the particles take place repeatedly during the ball milling process using a planetary mill. After the manufacturing process, fine magnetic abrasives which the guest abrasive particles c lung to the base metal matrix without bonding material can be obtained. The shape of the newly fabricated fine magnetic abrasives was investigated using SEM and its polishing performance was verified by experiment. It is very helpful to finishing the injection mold steel in final polishing stage. The areal ms surface roughness of the workpiece after several polishing processes has decreased to a few nanometer scales.

Titanium hydride를 이용한 TiC분말의 제조 및 특성 (Characteristics of Titanium Carbide Fabricated by Fine Titanium Hydride Powder)

  • 성택경;안인섭;배승열;정우현;박동규;정광철;김유영
    • 한국분말재료학회지
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    • 제12권3호
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    • pp.174-178
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    • 2005
  • This paper deals with the fabrication of titanium carbide using fine titanium hydride. The ratio of $TiH_2$ and C (Activated carbon) was 1:1 (mol) and milled in a planetary ball mill at a ball-to-powder weight ratio of 20:1. Thereafter, TGA was performed at $1400^{\circ}C$ to observe change of weight with milling time. Titanium carbide was obtained by using tempering the milled powders at $1100-1500^{\circ}C$. The microstructures of titanium carbide as well as the change of the lattice parameters and particle size have been studied by X-ray diffraction (XRD) and scanning electron microscopy (SEM).

유한요소해석과 실험에 의한 유압 윈치 드럼의 응력 계산 및 수명 예측 (Life Prediction and Stress Evaluation of Hydraulic Winch Drum by Finite Element Analysis and Experiment)

  • 이기천;박제인;남태연;최종식;박종원;이용범;제영기;이재환
    • 대한조선학회논문집
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    • 제57권5호
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    • pp.254-261
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    • 2020
  • The structural safety of hydraulic winch drum and the gears are estimated by the Finite Element Analysis (FEA) and the winch operation experiment. The mesh convergence test is performed and the applied force is the pressure on the drum converted from the rope tension in working condition. The stress of the drum calculated from the strain values of the winch operation experiment shows the agreement with that from the FEA. Most stress values are under the yield strength except for the small hole made for the wire rope fixation. The life of bearings in the drum is calculated using the life prediction formula with the reaction forces from the operation load. One of the two ball bearings shows the short life for impact condition, yet the real prototype winch system shows more life than the numerical value.

기계적 밀링공정에 의해 제조된 Bi0.4Sb1.6Te3 소결체의 열전특성 (Thermoelectric Properties of Bi0.4Sb1.6Te3 Sintered Body Fabricated by Mechanical Grinding Process)

  • 이길근;신승철;김우열;하국현
    • 한국분말재료학회지
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    • 제13권5호
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    • pp.313-320
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    • 2006
  • The present study is to analyze the thermoelectric properties of $Bi_{0.4}Sb_{1.6}Te_3$ thermoelectric materials fabricated by the mechanical grinding process. The $Bi_{0.4}Sb_{1.6}Te_3$ powders were prepared by the combination of mechanical milling and reduction treating methods using simply crushed pre-alloyed $Bi_{0.4}Sb_{1.6}Te_3$ powder. The mechanical milling was carried out using the tumbler-ball mill and planetary ball mill. The tumbler-ball milling had an effect on the carrier mobility rather than the carrier concentration, whereas, the latter on the carrier concentration. The specific electric resistivity and Seebeck coefficient decreased with increasing the reduction-heat-treatment time. The thermal conductivity continuously increased with increasing the reduction-heat-treatment time. The figure of merit of the $Bi_{0.4}Sb_{1.6}Te_3$ sintered body prepared by the mechanical grinding process showed higher value than one of the sintered body of the simply crushed powder.

복합 밀링 공정으로 제조된 산화물 분산 강화 강의 미세조직 및 고온 기계적 특성 (Microstructure and High Temperature Mechanical Properties of Oxide Dispersion Strengthened Steels Manufactured by Combination Milling Process)

  • 이정욱;김영균;김정한;김휘준;이기안
    • 한국분말재료학회지
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    • 제28권5호
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    • pp.389-395
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    • 2021
  • Oxide dispersion-strengthened (ODS) steel has excellent high-temperature properties, corrosion resistance, and oxidation resistance, and is expected to be applicable in various fields. Recently, various studies on mechanical alloying (MA) have been conducted for the dispersion of oxide particles in ODS steel with a high number density. In this study, ODS steel is manufactured by introducing a complex milling process in which planetary ball milling, cryogenic ball milling, and drum ball milling are sequentially performed, and the microstructure and high-temperature mechanical properties of the ODS steel are investigated. The microstructure observation revealed that the structure is stretched in the extrusion direction, even after the heat treatment. In addition, transmission electron microscopy (TEM) analysis confirmed the presence of oxide particles in the range of 5 to 10 nm. As a result of the room-temperature and high-temperature compression tests, the yield strengths were measured as 1430, 1388, 418, and 163 MPa at 25, 500, 700, and 900℃, respectively. Based on these results, the correlation between the microstructure and mechanical properties of ODS steel manufactured using the composite milling process is also discussed.

Effect of Mixed Grinding on Superconductivity YBaCu Composite Oxide

  • Ryu, Ho-Jin
    • The Korean Journal of Ceramics
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    • 제2권4호
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    • pp.251-256
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    • 1996
  • Effect of mixed grinding with a planetary ball mill of starting materials before heat treatment on the crystal structure and superconduction properties in the YBaCu composite oxide was studied. The size reduction of powders too place in the early stage of grinding, followed by aggregation of the resultant fine particles. The uniformity of the composition in the mixture was improved with grinding, which later decreased in the crystal grain size and well distribution of twin phase in the sintered bodies. The critical current density of the sintered bodies obtained from the mixture ground for 60 minutes showed the maximum value about 150 A/$\textrm{cm}^2$, while critical temperatures were around 90K and were independent of the grinding time.

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Metal-Polymer Composites and their Characterization

  • Lebedev, S.M.;Gefle, O.S.;Semenikhin, M.V.
    • 한국분말재료학회지
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    • 제18권2호
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    • pp.181-187
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    • 2011
  • PVDF was used as a polymeric matrix material in this work. Nickel powders with average particles size of 200 nm or 72 nm were used as fillers. PVDF/metal submicro- and nanocomposites were prepared by means of a mixing in twin screw extruder and planetary ball mill, respectively. All samples were prepared by hot pressing method. Their electrical, thermal and morphological properties were examined by dielectric spectroscopy, DSC, FTIR, XRD, optical microscopy and scanning electron microscopy. It was found that all properties of composites were strongly modified depending on the content of metal powders and filler particles size. Particularly, specific volume resistivity of PVDF/Ni composite with 0.2 wt.% of Ni was increased by factor of 1.5~4.

항공기용 2단 차동 GRA 개발 (Development of Aircraft 2-Stage Differential GRA)

  • 이강희;임대진;이선홍;박슬기;최진호
    • 한국기계가공학회지
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    • 제15권6호
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    • pp.115-121
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    • 2016
  • The aircraft flight control system controls an aircraft's direction and flying attitude, and actuators are key components of control systems. Actuators can be classified as Geared Rotary Actuator (GRA) and Ball Screw Actuator (BSA). GRA is used in mid-sized aircraft, and BSA is used in larger aircraft. A two-stage differential GRA model was suggested in this paper, and structural analysis and performance tests were performed. According to the analysis and experiment, the stiffness of the two-stage differential GRA was 17.57% higher than that of the conventional GRA, and the structural safety was improved.

분쇄공정에서 변화된 입자크기 및 형상특성의 평가방법에 관한 새로운 제언 (New Evaluation Method for The Particle Size and Morphology Via Change of Ground Particle During a Grinding Process)

  • 최희규;이재현;최준우
    • 한국입자에어로졸학회지
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    • 제9권1호
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    • pp.1-6
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    • 2013
  • New evaluation method for the particle size and morphology via change of ground particle during a grinding process was investigated. The grinding experiments were carried by a planetary ball mill. The relationship between the particle outline of the scanning electron microscopy photograph and measurement line, the measurement contact number was evaluated. The value of contact number decreased with the increase in the particle size of the ground sample, and varied with the experimental conditions. The value of contact number, which is related to the particle size of the raw sample, changed at the various experimental conditions.