• Journal of the Korean Ceramic Society
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• v.40 no.12
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• pp.1224-1228
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• 2003

The crystallization behavior of a luster glaze containing ceria has been investigated. When glazed specimens were sintered at 110$0^{\circ}C$, crystalline ceria particles were preferentially precipitated with (100) planes parallel to the specimen surface with the size of around 200 nm. The particle population in the surface region was much higher than inside glaze, covering over 60% of the specimen surface area. Crystallization of the particles with preferred orientation was promoted, after the removal of internal interface through complete melting of the fit particles. The luster effect seems to result from CeO$_2$ particles of high refractive index, their strong light scattering at visible rage due to fine crystalline size 200 nm and their planar arrangement in the surface region.

• Bulletin of the Korean Chemical Society
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• v.14 no.1
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• pp.137-143
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• 1993

The tetranuclear heterometallic complex CpMo$Os_3(CO)_{10}({\mu]-H)2[{\mu}3-{\eta}^2-C(O)CH_2Tol]\;(1,\;Cp={\eta}^5-C_5H_5,\;Tol=p-C_6H_4Me)$ has been examined by variable-temperature $^{13}$C-NMR spectroscopy and by a full three-dimensional X-ray structual analysis. Complex 1 crystallizes in the orthorhombic space group Pna2$_1$ with a = 12.960(1) ${\AA}$, b = 11.255(l) ${\AA}$, c = 38.569(10)${\AA}$, V = 5626(2) ${\AA}^3$ and ${\rho}$(calcd) = 2.71 gcm$^{-3}$ for Z = 8 and molecular weight 1146.9. Diffraction data were collectedon a CAD4 diffractometer, and the structure was refined to $R_F$ = 9.7% and $R_{W^F}$ = 9.9% for 2530 data (MoK${\alpha}$ radiation). There are two essentially equivalent molecules in the crystallographic asymmetric unit. The tetranuclear molecule contains a triangulated rhomboidal arrangement of metal atoms with Os(2) and Mo at the two bridgehead positions. The metal framework is planar; the dihedral angle between Os(l)-Os(2)-Mo and Os(3)-Os(2)-Mo planes is 180$^{\circ}$. A triply bridging (${\mu}_3,\;{\eta}^2$) acyl ligand lies above the Os(l)-Os(2)-Mo plane; the oxygen atom spans the two bridgehead positions, while the carbon atom spans one bridgehead position and an acute apical position. The molecular architecture is completed by an ${\eta}^5$-cyclopentadienyl ligand and a semi-triply bridging carbonyl ligand on the molybdenum atom, and nine terminal carbonyl ligands-four on Os(3), three on Os(l), and two on Os(2). The two hydride ligands are inferred to occupy the Os(l)-Os(2) and Mo-Os(3) edges from structural and NMR data.

• Journal of the Korean Society of Industry Convergence
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• v.25 no.6_2
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• pp.1119-1125
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• 2022

The depletion of resources and waste disposal caused by the continuous development of industry have emphasized the need to reduce consumption and production, recycle and reuse, and the importance of remanufacturing has increased in recent years. The spindle part of the aging planner miller, which is currently being remanufactured, is one of the factors that has the greatest impact on the performance of the machine tool. When designing the spindle part of the spindle shaft, there are considerations such as the configuration size bearing performance of the main shaft, but the diameter of the main shaft, the dangerous speed bearing, and the arrangement that affect the machining accuracy should be basically considered. As such, various studies have been conducted on the design of machine tool spindle spindles, but research on the reverse engineering of existing aging machine tool spindle spindles is poor. Reverse engineering is designing in the direction of improving performance by extracting specifications from already finished products, and first scanning the reverse engineered object through a 3D scanner, 3D modeling is performed based on the collected data, and then the process of deriving improvement plans by reverberating to improve performance by identifying wear and damage conditions is followed. Therefore, in this study, the purpose of this study is to provide data on reverse engineering by deriving improvement plans through optimal design for the bearing position of the aging planar Miller spindle spindle using central composite programming.

• The Journal of the Convergence on Culture Technology
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• v.9 no.6
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• pp.113-122
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• 2023

This study was conducted on the premise of the development of cultural products using relic assets of traditional culture in a knowledge and information society led by culture and soft power. It was conducted in the context of exploring the possibility of cultural content products of Wa-Dang relics excavated from traditional architecture in the Unified Silla Period and expanding the scalability of commercialization motifs that are highly useful in jewelry design. First, the original form, material, use, size, meaning, and formative aesthetics of Wa-Dang were identified through literature and media research. Among the considered Wa-Dang, 10 types of Wa-Dang which represent the category and have values in modules and patterns were selected, and, then, circular images were extracted and modularized with a "formal simplification technique." Based on the "mathematical symmetry analysis technique," which is a method of systematizing pattern composition arrangement format. we derived a planar formative element that can be used in the development of the cultural content industry and jewelry design. In order to expand its usability in the jewelry industry in the future, it was presented as a 2D digital image. In the future, we hope more studies on the various cultural content industry utilizing the traditional culture will be carried out.

• Journal of the Korean Society for Precision Engineering
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• v.31 no.10
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• pp.881-887
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• 2014

Micro-sized Peltier coolers are generally employed for uniformly distributing heat generated in the multi-chip packages. These coolers are commonly classified into vertical and planar devices, depending on the heat flow direction and the arrangement of thermoelectric materials on the used substrate. Owing to the strong need for evaluation of performance of thermoelectric modules, at present an establishment of proper theoretical model has been highly required. The design theory for micro-sized thermoelectric cooler should be considered with contact resistance. Cooling performance of these modules was significantly affected by their contact resistance such as electrical and thermal junction. In this paper, we introduce the useful and optimal design model of small dimension thermoelectric module.