• 제목/요약/키워드: physical characterization

검색결과 628건 처리시간 0.03초

CHARACTERISTICS OF RESIDUAL CARBON DERIVED FROM THE COMBUSTION OF VACUUM RESIDUE IN A TEST FURNACE

  • Park, Ho-Young;Seo, Sang-Il
    • Environmental Engineering Research
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    • 제12권3호
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    • pp.109-117
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    • 2007
  • The characteristics of carbonaceous particles collected from the combustion of Vacuum Residue (VR) in a test furnace have been investigated. The physical and chemical characterization includes particle size, scanning electron microscopy of the surface structure, measurement of porosity, surface area and density, EDX/XRD analyses and measurement of chemical composition. The studies show that the carbonaceous VR particles are very porous and spheroidal, and have many blow-holes on the surface. The particles become smaller and more sponge-like as the reaction proceeds. The present porosity of VR particles is similar to that of cenospheres from the combustion of heavy oil, and the majority of pores are distributed in macro-pores above $0.03\;{\mu}m$ in diameter. Measurements of pore distribution and surface area showed that the macro-pores contributed most to total pore volume, whereas the micro-pores contributed to total surface area.

Characterization of Graphite Oxide Reduced by Thermal and/or Chemical Treatments

  • Kim, Jungsoo;Nam, Dae-Geun;Yeum, Jeong Hyun;Suh, Sungbu;Oh, Weontae
    • Transactions on Electrical and Electronic Materials
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    • 제16권5호
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    • pp.274-279
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    • 2015
  • Reduced graphite oxides (rGOs) were prepared by the common graphite oxidation method and the subsequent reductions. The reduction of graphite oxides (GOs) was conducted chemically and/or thermally. To further reduce the as-prepared rGOs, GOs were treated with chemical/thermal reductions or thermal/chemical reductions, in which the reduction sequence was also considered. The structural changes of as-prepared rGOs, depending on reduction methods, were investigated by X-ray diffraction analyses, Raman spectroscopy, X-ray photoelectron spectroscopy, and scanning electron microscopy. In addition, we discuss the structural change of the rGOs and their closely related physical and electrical properties, such as thermogravimetry, nitrogen adsorption isotherm, and sheet resistance.

트리브로모 변성폴리에스테르를 함유한 PU 난연도료의 합성과 도막 특성화 (Synthesis and Characterization of PU Flame-Retardant Coatings Using Tribromo Modified Polyesters)

  • 박은경;양인모;김대원;황규현;박홍수
    • 폴리머
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    • 제25권3호
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    • pp.391-398
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    • 2001
  • 난연성분인 트리브로모아세트산의 함량을 10, 20, 30wt%로 변화시키면서 1,4-부탄디올, 아디프산 및 트리메틸올프로판과 축합중합을 하여 트리브로모 변성폴리에스테르(TBAO)를 합성한 후에, TBAO류와 이소시아네이트를 블렌드하여 2성분계 폴리우레탄(PU) 난연도료를 제조하였다. 제조된 난연도료의 도막물성을 측정한 결과, 결코 비난연도료보다 물성이 저하되지는 않았다. 또한 난연도료의 난연성 시험결과, 수직법에서 트리브로모아세트산 20 wt%에서 불꽃에 타지 않아서 양호한 난연도료임을 알 수 있었다.

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신서란 섬유를 이용한 종이 제조와 그 특성 (Manufacture and Characterization of Papers Made from New-Zealand Hemp Fibers)

  • 이현철;김봉용
    • 펄프종이기술
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    • 제36권1호
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    • pp.67-74
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    • 2004
  • This study was carried out to investigate the characteristics of handsheets made from nonwoody New-Zealand hemp (Phormium tenax) fibers that was not used before in Korea. The results were as follows : 1. Physical properties of bleached phormium fiber were satisfactory for handsheet forming. Specially, tensile strength was improved by adding bleached phormium fiber. 2. Opacity of handsheet with phormium pulp was fine, therefore it can be useful fiber to improve opacity of light-weight printing paper. 3. Filler retention rate was improved when phormium pulp was added, while drainage time was increased. 4. Phormium fiber has good characteristics as pulp for paper manufacture. So it can be valuable non-wood fiber resource if drainage problem is solved.

측정 기반 BRDF 데이터를 이용한 실감재질표현 연구 (Realistic representation based on measured BRDF data)

  • 유현진;김강연;김회민;서명국;고광희;이관행
    • 한국HCI학회:학술대회논문집
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    • 한국HCI학회 2007년도 학술대회 1부
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    • pp.1019-1024
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    • 2007
  • 그래픽스 분야에서 다양한 재질을 사실감 있게 표현하려는 연구가 활발히 진행되고 있는 가운데, 다양한 재질의 반사특성을 측정하는 방법들이 시도되고 있다. 본 연구에서는 디지털 카메라를 이용하여 영상 기반 양방향 반사 분포함수(BRDF: Bidirectional Reflectance Distribution Function)를 획득할 수 있는 측정 시스템을 구축하였다, 이를 통한 BRDF 모델은 경험적(empirical)혹은 물리(physical)기반의 모델에 비해 보다 사실성 높은 표현이 가능하다. 영상 기반으로 양방향 반사 분포함수를 생성하는 과정에서 노출시간을 달리한 여러 장의 영상을 가지고 HDR(High Dynamic Range) 영상을 생성하였다. 또한 원색재현을 위해 표준광원을 사용하고 컬러차트와 회귀분석을 통해 컬러 보정을 수행하였다. 본 연구에서는 플라스틱이나 금속재질같이 불투명한 등방성(isotropic) 재질을 사용하였고, 이러한 재질의 BRDF데이터를 통해 산업제품에서 많이 사용되는 재질의 모델을 보다 실감나게 렌더링(rendering)할 수 있다.

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Growth and characterization of lead bromide: application to mercurous bromide

  • Kim, Geug-Tae
    • 한국결정성장학회지
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    • 제14권2호
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    • pp.50-57
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    • 2004
  • Mercurous Bromide ($Hg_2Br_2$) crystals hold promise for many acousto-optic and opto-electronic applications. This material is prepared in closed ampoules by the physical vapor transport (PVT) growth method. We investigate the effects of solutal convection on the crystal growth rate in a horizontal configuration for diffusive-convection conditions and purely diffusion conditions achievable in a low gravity environment. Our results show that the growth rate is decreased by a factor of one-fourth with a ten reduction of gravitational acceleration near y = 2.0 cm. For 0.1 $g_O$ the growth rate pattern exhibits relatively flat which is intimately related to diffusion-dominated processes. The growth rate nonuniformity is regardless of aspect ratio across the interfacial positions from 0 to 1.5. Also, the effect of a factor of the ten reduction in the gravitational acceleration is same to both Ar = 5 and 2. The enlargement in the molecular weight of B from 50 to 500 by a factor 4 causes a decrease in the maximum growth rate by the same factor, indicative of the effect of solutal gradients.

Wall Voltage Characteristics Simulated Using an Equivalent Circuit Model for AC POPs

  • Kim, Joon-Yub;Lim, Jong-Sik
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2003년도 International Meeting on Information Display
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    • pp.317-320
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    • 2003
  • As a convenient means for the characterization of the wall voltage and wall charge of AC PDPs during the sustain period, an equivalent circuit model for AC PDPs is presented. The equivalent circuit model for AC PDPs consists of capacitors and thyristors. The equivalent circuit model is based on the physical structure of the AC PDP and the I-V characteristic of the discharge space. This equivalent circuit model can be easily implemented in the standard simulators such as SPICE and can easily simulate the variation of the current, charge and voltage involved in AC PDPs as the supply voltage varies.

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주사형 맥스웰응력 현미경에 의한 표면의 전기적 이미지 (Electrical Imaging of Thin Film Surface by Scanning Maxwell-stress Microscopy)

  • 신훈규;권영수
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1998년도 하계학술대회 논문집 D
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    • pp.1508-1510
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    • 1998
  • Recent development of scanning probe microscope techniques has made it possible to investigate, not only microscopic surface topography, but also physical and chemical properties on the nanometer-scale. The scanning Maxwell-stress microscopy (SMM) is surface characterization tool capable of mapping both the surface topography and electrical properties, such as surface potential, surface charge dielectric constant of thin films with a nanometer-scale resolution by means of the AC voltage driven oscillation of metal coated cantilever. In this study, we observed the surface potential distribution and molecular ordering in thin films. We have demonstrated that the SMM can be used for imaging surface potential distribution over the film surface and also be used for detecting surface changes in thin films. This is first step towards the understanding of electrical phenomena in organic and inorganic materials, biological system with SMM.

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카바졸을 포함하는 청색 OLED 재료의 합성 (Synthesis and Characterization of Carbazole Derivate for Blue light Emitting Material)

  • 신민기;박현태;장상훈;고혜진;장재완;김윤희;권순기
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2010년도 하계학술대회 논문집
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    • pp.58-58
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    • 2010
  • We designed and synthesized DFPCE blue emitting materials by Mc Murry coupling reaction in order to improve the device efficiency and stability. The structure was confirmed by $^1H$-NMR. The physical properties were characterized by differential scanning calorimetry, thermogravimetric analysis, UV-vis, photoluminescence spectrum and cyclic voltammetry. The decomposition temperature of the material, which correspond to a 5% weight loss upon heating, is $513.58^{\circ}C$. The photoluminescence (PL) spectrum of DFPCE exhibited blue emission at 425 nm in chloroform solution and 462 nm in film.

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Te이 과량 포함된 $Sb_xTe_{1-x}$ 나노와이어 및 나노튜브의 합성 및 분석 (Synthesis and Characterization of Te-rich $Sb_xTe_{1-x}$ Nanowires and Nanotubes)

  • 이준석;노광수;정순원;윤성민;유병곤
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2008년도 추계학술대회 논문집 Vol.21
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    • pp.423-423
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    • 2008
  • One dimensional (1D) nanostructures, including nanowires, nanorods, nanobelts, and nanotubes, have been the focus of current research on nanotechnology because of their fundamental significance in chemistry, physics, materials science and engineering, and potential applications in nanoelectronics. We have synthesized Te-rich $Sb_xTe_{1-x}$ nanowires and nanotubes via thermal evaporation method under vapor-solid mechanism. The physical morphology and chemical composition of the fabricated nanowires and nanotubes were investigated by scanning electron microscopy (SEM), transmission electron microscopy (TEM), and energy dispersive X-ray spectroscopy (EDX).

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