• Title/Summary/Keyword: paticle size

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Specification and Testing Method of WHW ex. for Chronic Renal Failure (만성신부전 치료제 개발을 위한 WHW 엑스의 기준 및 시험방법 설정)

  • So, Jae-Woo;Kang, Hee-Chul;Seo, Chang-Gyo;Lim, Ji-Ho;Park, Yong-Ki;Lee, Young-Jae;Kim, Young-Ho;Kang, Jong-Seung;Cho, Cheong-Weon
    • Journal of Pharmaceutical Investigation
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    • v.39 no.3
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    • pp.161-166
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    • 2009
  • This study is to specify the criteria and testing methods of WHW extract which has a potency as a therapeutic agent for chronic renal failure. The determination of specifications of WHW extract is mostly important because of the quality assurance. Three batches of WHW extract were obtained by the extraction at $98^{\circ}$C for 3 hr using water from mixture of 15 herbal medicines including Codonopsis Pilosulae Radix, Salviae Radix, Pinelliae Rhizoma, Coptidis Rhizoma, Evodiae Fructus, Epimedii Herba, Rhei Rhizoma, Perillae Herba, Glycyrrhizae Radix, Artemixiae capillaris Herba, Alimatis Rhizoma, Hoelen, Atractylodies Rhizoma alba, Polyporus and Cinnamomi Ramulus, subsequently, vaccum-dried for 15 hr. The yield of WHW extracts was 24.53% on the average. The identification of each herbal medicine of WHW extract was performed by modification of Korean Pharmacopeia IX (KP IX). The assay of WHW extract was performed using standard such as berberine, icariin, glycyrrhizin, and cinnamic acid of indicative herbal medicines by modification of KP IX, too. As well as, paticle size classification test was carried out to indicate the boundary of particle size of WHW extract and the particle size of WHW extract more than 50% showed the 140 ${\mu}$m. Taken together, WHW extract could be prepared reproducibly and assurable if follows the presented extraction and drying steps and its specifications were satisfied with the indicated criteria.

Characteristics of Spray from Pressure-Swirl Nozzle with Different Liquid Properties and Nozzle Geometries (액체의 물성치와 노즐의 형상 변화에 따른 압력스월 노즐의 분무 특성)

  • Choe, Yun-Cheol;Jeong, Ji-Won;Kim, Deok-Jul
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.25 no.12
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    • pp.1813-1820
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    • 2001
  • The purpose of this study was to investigate the significant characteristics in atomization process of industrial etching spray fur the design or Precise pressure-swirl nozzles. The experiment was carried out with different viscosities and densities of the liquid. The macro characteristics of liquid spray, such as the spray angle and breakup process were captured by PMAS and the micro characteristics of liquid spray. such as droplet size and velocity measurements were obtained by PDA. The droplet axial and radial velocity and SMD were measured along axial and radial direction. The RMS of two velocities was measured along radial direction. It was found that the fluid with higher kinematic viscosity resulted in the larger SMD and the lower mean droplet velocity. And we could divide breakup processes into three regions that is atomization, non-dilution and dilution one in spray of pressure-swirl nozzle. The radial as well as axial velocity of droplet played an important role in the atomization process of higher kinematic viscosity fluid.

KATSTIC SINKHOLE SEDIMENTS OF DOLOSTONE IN THE UPPER MIDWEST'S DRIFTLESS AREA, USA

  • Oh, Jong-woo
    • Journal of the Speleological Society of Korea
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    • v.34 no.35
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    • pp.78-104
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    • 1993
  • Analysis of one sinkhole, the Dodgeville sinkhole, developed in Ordovician dolostones in the Driftless Area of Wisconsin in the Upper Midwest'd Driftless Area reveals homogenous clayey sediment fills reflecting a range of dissolutional processes during the Quaternary or Pre-Quaternary. Granulometric analysis, graphical moments statistics, carbonate minerals, ana sand grain lithology were used to differentiate sinkhole sediment sources and modes of accumulation. Sediments in the dolostone sinkholes developed by dissolution. Sediments contain two major types of sediments : residual redish clay( autogenic sediments) and aeolian silt (allogenic sediments). The massive clay is generated from the weathered dolostone bedrocks as a in situ materials. The loessial silt is mostly derived from transportation of the surrounding surface materials, with some evidences of penetrated deposition. Unlike the collapsed sandstone sinkholes (Oh et al., 1993), dolostone sinkholes reveal homogenous, autogenic clay materials, and a geochemical composition indicative of in situ autogenic karstification. Dolostone sinkhole si1ts (26.9%) and sands (34.9%) are derived from weathered Plattevi1le-Galena dolostones, and contain high carbonate(37.5%), chert (57.2%) and lead ore (3%). Graphical moments statistics for sorting, skewness, and kurtosis indicate that sand grains from dolostones were derived entirely from local bedrock by in situ dissolution. Upper sinkhole sediments are pedagogically very young as carbonate is unleashed. Materials of the sinkhole sediment are definitely inherited from internal dolostones by dissolution and weathering, because not only a granulomatric comparison of dolostone and sandstone sediments demonstrates that they have heterogeneous paticle size distributions, but also 1ithologic analyses displays they differ completely.

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The Frost-Susceptibility of Compacted Coal Ash with Proper Mixing Ratio of Fly Ash to Bottom Ash (비회와 저회의 적정 혼합비로 다짐한 석탄회의 동상성)

  • Chun, Byung Sik;Gang, In Sung;Koh, Yong Il
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.13 no.1
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    • pp.173-178
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    • 1993
  • The most appropriate mixing ratio of fly ash to bottom ash obtained from compaction characteristics and CBR values is varying from 5:5 to 6:4. But these mixed ashes are frost-susceptible materials according to judging by the paticle-size distribution because of a lot of silty-size paticles. In this study, the frost-susceptibility of compacted coal ash with proper mixing ratio is examined experimentally for use of subgrade materials. And, the efforts have been made to find proper cement addition in making these mixed ashes frost-insusceptible. It was revealed that these mixed ashes are frost-susceptible, and 4% of cement content is required to be made frost-insusceptable. It was found that amount of frost heave of these mixed ashes decreases with the unconfined compressive strength, and increases with log k if the permeability coefficient k is as low as the water into the freezing front of these mixed ashes is restricted.

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Fabrication of 13Cr-1.5Nb-Fe Alloy Powder and AC Magnetic Properties of the Sintered Magnetic Core (소결 13Cr-1.5Nb-Fe 합금의 교류 자기 특성)

  • 오환수;김택기;조용수
    • Journal of the Korean Magnetics Society
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    • v.10 no.1
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    • pp.11-15
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    • 2000
  • 13Cr-1.5Nb-Fe alloy powder prepared by water atomizing method is reduced with flowing hydrogen gas. The characteristics of a reduced alloy powder is investigated and magnetic cores formed by using the reduction power sintered in the vacuum of ∼10$\^$-5/ Torr. In order to study on the magnetic cores permeability and power loss in alternating magnetic field are also measured. The result of particle size distribution shows the paticle size is 70 ㎛ at volume fraction of 50 %. The saturation magnetization of the reduced alloy powder is 160 emu/g. The relative peak permeability (H$\_$a/=5Oe) of a magnetic core is 400 and the power loss (B$\_$m/=80G) 0.12 mW/cc at sintering temperature of 1,200 $\^{C}$, 10 ton/㎠ forming pressure, and 1 kHz.

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Paticle Size Distribution, Pasting Pattern and Texture of Gel of Acorn, Mungbean, and Buckwheat Starches (도토리, 녹두 및 메밀전분의 입도분포, 호화패턴과 겔특성)

  • Cho, Sung-Ae;Kim, Sung-Kon
    • Korean Journal of Food Science and Technology
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    • v.32 no.6
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    • pp.1291-1297
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    • 2000
  • Particle size distribution, pasting properties by Rapid Visco Analyser, and textural properties of acorn, mungbean and buckwheat starches, which are the basic raw materials for mook, are compared. The major particle size of mungbean starch was $10{\sim}30$ micron, whereas acorn and buckwheat starches were $5{\sim}20$ micron. At the same starch concentration, mungbean starch had the highest peak viscosity, breakdown and setback. Acorn starch showed the lowest peak viscosity and breakdown. The peak viscosity of buckwheat starch was close to that of mungbean, however the trough and final viscosity were comparable to those of acorn starch. At the same peak viscosity, mungbean starch showed the lowest trough and final viscosity and the highest breakdown and setback. Acorn starch was differentiated from buckwheat starch in that the former had the higher value of setback. The textural properties of mungbean starch gel were significantly different from others. The texture of gels from acorn and buckwheat starches revealed that only the hardness and gumminess were different each other. The hardness of starch gels were negatively correlated with trough and final viscosity, and positively correlated with setback.

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Improvement of Wear Resistance and Formation of Si Alloyed Layer on Aluminum Alloy by PTA Process (PTA법에 의한 Al 합금표면의 Si 합금층 형성과 내마모성 개선)

  • ;;松田福久;中田一博
    • Journal of Welding and Joining
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    • v.15 no.5
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    • pp.134-143
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    • 1997
  • The formation of thick alloyed layer with high Si content have been investigated on the surface of Al alloy (A5083) plate by PTA process with Si powder. Hardening characteristics and wear resistance of alloyed layer was examined in relation to the microstructure of alloyed layer. Thick hardened layer in mm-order thickness on the surface of A5083 plate can be formed by PTA process with wide range of process condition by using Si powder as alloying element because of eutectic reaction of Al-Si binary alloy. High temperature and rapid solidification rate of molten pool, which are features of PTA process, enable the formation of high Si content alloyed layer with uniform distribution of fine primary Si paticle. High plasma arc current was beneficial to make the alloyed layer with smooth surface appearance in wide range of powder feeding rate, because enough volume of molten pool was necessary make alloyed layer. Uniform dispersion of fine primary Si particle with about 30${\mu}{\textrm}{m}$ in particle size can be obtained in layer with Si content ranging from 30 to 50 mass %. Hardness of alloyed layer increased with increasing Si content, but increasing rate of hardness differed with macrostructure of alloyed layer. Wear resistance of alloyed layer depended on $V_{si}$(volume fraction of primary Si) and was remarkably improved to two times of base metal at 20-30% $V_{si}$ without cracking, but no more improvement was obtained at larger $V_{si}$.

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