• 제목/요약/키워드: particle size analyzer

검색결과 359건 처리시간 0.027초

Morphological, Physical Characterization of Poly(acrylic acid) Nanogel Prepared by Electron Beam Irradiation

  • Park, Jong-Seok;Choi, Jong-Bae;Gwon, Hui-Jeong;Lim, Youn-Mook;Jeong, Sung-In;Shin, Young-Min;Kang, Phil-Hyun;Nho, Young-Chang
    • 방사선산업학회지
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    • 제8권1호
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    • pp.29-34
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    • 2014
  • Nanogels are internally cross-linked particles of sub-micrometer size made of hydrophilic polymers and are considered a distinct type of macromolecules, compared with linear and branched polymers or macroscopic gels. In this study, we studied a method of radiation induced synthesis of nanogels, which allows us to obtain tailored intra-molecularly crosslinked macromolecules of independently chosen molecular weight and dimensions. Thus, we report the possibility of applying the prepared nanogels using poly(acrylic acid) through electron beam irradiation for potential application as biomaterials. The nanogels were characterized by scanning electron microscopy (SEM). In addition, the size and zeta-potential of nanogels were measured by a particle size analyzer (PSA). The nanogels were prepared at an approximate size of 180 nm at 100 kGy and were spherical in shapes. The size of the nanogels decreased with increasing irradiation doses, and the absolute value of zeta potential increased with increasing irradiation doses.

Characterization of the PAC Modified Cationic Rosin Size and its Sizing Effect

  • Yan, Yong-Xiang;Chandranupap, Fu-Shan;Wang, Gao-Sheng
    • 한국펄프종이공학회:학술대회논문집
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    • 한국펄프종이공학회 2006년도 PAN PACIFIC CONFERENCE vol.2
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    • pp.387-390
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    • 2006
  • Cationic rosin sizes are prepared by premixing extremely pure ployaluminum chloride (PAC) and dispersed rosin size (DRS). It turned out that zeta potential and particle size of the sizing agents took a big change by Plus90 analyzer's and FTIR analyzer's analysis. It turned out that -C=O and -COOH of the DRS have both chemical reaction with PAC to form the muti-hydroxyl aluminum rosin acid and that the cationic rosin sizes modified by PAC has dissymmetric and symmetric flexible vibration two absorbing peaks of the groups (its absorbing peaks $at1596cm^{-1}\;and\;1425cm^{-1}$). By DRS reacting with PAC, zeta potential of the resin size varied from negative to cationic. $Al_{2}O_{3}/rosin=1:0.3$, zeta potential of premixed admixture is tiptop28.8mv, When joined continuously PAC, zeta potential of cationic rosin sizes descend on the contrary.

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이중응집이 응집공정에 미치는 영향 (Effects of Dual-Coagulant Performance)

  • 김희근;문병현;김승현
    • 상하수도학회지
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    • 제19권1호
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    • pp.92-97
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    • 2005
  • This research is to investigate the effect of the dual coagulant using inorganic coagulants($AICl3{\cdot}6H2O$) and polymer on the coagulant process. Jar-test was conducted by using Kaolin injected raw water. PDA(Photometric Dispersion Analyzer) equipment in order to analyze the size of the particles and the characteristics of the shapes. The change in the rate of sample ores' residual deposited after coagulants were also compared. According to the result derived from this experiment, the concentration of inorganic coagulant reduced 50% and the residual was lower by using dual coagulants compared to using single coagulant. However the dual coagulant required sufficient mixing time, and affected particle characteristics, with the effect of the injection order of coagulants, the simultaneous injection of inorganic coagulant and polymer showed the most effective in the particle removal.

기능성 마이크로스피어의 개발 (I) - 열유도 상분리에 의한 Poly(ethylene-co-vinyl acetate) 마이크로스피어의 제조와 특성 - (Development of functional microsphere (I) - Formation and characteristics of poly(ethylene-co-vinyl acetate) microspheres via thermally induced phase separation -)

  • 이신희;김효정;박수민
    • 한국염색가공학회지
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    • 제15권4호
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    • pp.57-64
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    • 2003
  • Poly(ethylene-co-vinyl acetate)(EVA) microspheres were prepared by a thermally induced phase separation. The microsphere formation occurred by the nucleation and growth mechanism in the metastable region. The diluent used was toluene. The microsphere formation and growth was followed by the cloud point of the optical microscope measurement. The microsphere size distribution, which was obtained by SEM observation and particle size analyzer, became broader when the polymer concentration was higher, the content of vinyl acetate in EVA copolymer was higher, and the cooling rate of EVA copolymer solution was lower.

석산골재광산에서 발생한 잔토의 콘크리트 유효이용에 대한 연구 (Studies of concrete utilization of waste sludge by-producted in aggregate mines)

  • 엄태선;백상현;백원준;김창수
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1998년도 가을 학술발표회 논문집(I)
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    • pp.7-12
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    • 1998
  • The waste sludge is by-produced about 20-30% of total production and arised to the severe problems of this mine's surrounding environmnet. This study was invested the composition of component, particle of size of the waste sludge by Chemical Analysis, X, R, D, Particle Size Analyzer and the physical properties (air content, slump, strength, etc) of concrete when the waste sludge is added into concrete. so, It's recomended the proper content of the waste sludge to be added into concrete. and then, is verified to be applied at batch plant in field. Above the results, the recomeded content of the waste sludge is about 2-4% (about 4-8% in cement) in aggregates and when it's added the recomended content, they are detected to be more or less changed the physical properties of concrete, ( equally strength and durability, little less air con tent, little increased shinkage, etc). but the application of the recomended content don't arise the problem of the basic quality control of concrete and physical properties.

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기능성 마이크로스피어의 개발(II) - 안료를 함유한 에틸렌-비닐아세테이트 공중합체의 마이크로스피어 제조와 특성 - (Development of functional microsphere(II) - Formation and Characteristics of Poly(ethylene-co-vinylacetate) Microsphere with Pigment -)

  • 이신희;박수민
    • 한국염색가공학회지
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    • 제17권4호
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    • pp.15-20
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    • 2005
  • Poly(ethylene-co-vinylacetate)(EVA) microspheres were prepared by thermally induced phase separation in toluene. The microsphere formation occurred by the nucleation and growth mechanism in metastable region. The effects of the polymer or pigment weight percentage and cooling rate on microsphere formation were investigated. The microsphere formation and growth were followed by the cloud point of the optical microscope measurement. The microsphere size distribution, which was obtained by particle size analyzer, became broader when the polymer concentration was higher, the pigment concentration and the cooling rate of EVA copolymer solution were lower.

회전연료 분사시스템의 분무특성 (Spray Characteristics of the Rotating Fuel Injection System)

  • 이동훈;박정배;최성만
    • 한국분무공학회지
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    • 제11권2호
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    • pp.81-88
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    • 2006
  • The spray characteristics of the rotating fuel injection system were investigated. The special test rig was devised to get the spatial and momentary droplet information. This experimental apparatus consists of a high-speed motor, a shaft, a rotating fuel nozzle and an acrylic case. Spray droplet size and velocity were measured by PDPA(Phase Doppler Particle Analyzer) and instantaneous velocity field was measured by 1'IV (Particle Image Velocimetry) system. At the same time, spray visualization was performed by using ND-YAG laser-based flash photography. From these two different laser diagnostic techniques, we could get spatial and instantaneous spray information fur rotating fuel injection system. The results presented in this paper indicate that spray characteristics such as droplet size, velocity and spray pattern were strongly influenced by rotational speed.

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포트 분사 연료 인젝터의 분무 구조에 관한 연구 (An Study on the Spray Structure of Fuel Port Injectors)

  • 이창식;이기형;전문수;손강호;박종순
    • 한국분무공학회지
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    • 제3권3호
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    • pp.42-48
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    • 1998
  • This study describes the spray structure of gasoline port injectors by using phase Doppler particle analyzer(PDPA) and particle motion analysis system(PMAS). The characteristics of fuel spray such as the spray penetration, spray angle and breakup processes were obtained by PMAS and the droplet size and mean velocity were measured by PDPA system. Pintle type and two-hole type injectors were used as gasoline port fuel injectors under various injection pressures. The effect of injection pressure on the droplet mean diameter and axial mean velocity of droplet were investigated under the various injection conditions. In addition the comparison of breakup processes for the two types of injectors was also conducted. It Is shown that pintle type injector has smaller droplet size than that of two-hole type injector.

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Atomization Characteristics of a Double Impinging F-0-0-F Type Injector with Four Streams for Liquid Rockets

  • Kang, Shin-Jae;Rho, Byung-Joon;Oh, Je-Ha;Kwon, Ki-Chul
    • Journal of Mechanical Science and Technology
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    • 제14권4호
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    • pp.466-476
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    • 2000
  • This paper presents atomization characteristics of a double impinging F -0-0- F type injector with four streams. A phase Doppler particle analyzer was employed to measure the droplet-size and water was used as the inert simulant liquid instead of reactive propellant liquids. The droplet mean diameter (SMD) and size distribution were measured to investigate the effects of the momentum ratio and pressure drop variations. This experimental results can be used during the preliminary design stage of a impinging stream type injector for liquid rockets.

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헤드-디스크 인터페이스에 주입되는 입자의 영향에 대한 연구 (Study on the Effect of Particles Injected Into the Head/Disk Interface)

  • 한제희;이래준;김대은;강태식;조긍연
    • 정보저장시스템학회:학술대회논문집
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    • 정보저장시스템학회 2005년도 추계학술대회 논문집
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    • pp.179-183
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    • 2005
  • Particles in the HDD can cause serious damages such as scratches and thermal asperity(TA) at the head/disk interface(HDI). Accordingly, particles cause data loss including physical and electrical damages. To improve the reliability of head-disk interface, understanding the damage characteristics at the HDI due to particle interactions is required. The materials such as $A1_2O_3$, TiC and aluminum were used in this experiment. The size and hardness of particles injected into the HDI are closely relevant to surface damage caused the data loss on the disk and head. In this paper, a variety of scratches were analyzed using scanning electron microscope(SEM) and atomic force microscope(AFM). In order to analyze defects of very small size on the disk, optical surface analyzer(OSA) was also used.

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