• Title/Summary/Keyword: particle reduction

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Effects of Sintering Temperature on Fabrication Properties of LPS-SiC Ceramics (LPS-SiC 세라믹스 제조특성에 미치는 소결온도의 영향)

  • Park, Yi-Hyun;Jung, Hun-Chae;Kim, Dong-Hyun;Yoon, Han-Ki;Kohyam, Akira
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.204-209
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    • 2004
  • SiC materials have been extensively studied for high temperature components in advanced energy system and advanced gas turbine. However, the brittle characteristics of SiC such as low fracture toughness and low strain-to fracture still impose a severe limitation on practical applications of SiC materials. For these reasons, $SiC_f/SiC$ composites can be considered as a promising for various structural materials, because of their good fracture toughness compared with monolithic SiC ceramics. But, high temperature and pressure lead to the degradation of the reinforcing fiber during the hot pressing. Therefore, reduction of sintering temperature and pressure is key requirements for the fabrication of $SiC_f/SiC$ composites by hot pressing method. In the present work, Monolithic LPS-SiC was fabricated by hot pressing method in Ar atmosphere at 1760 $^{\circ}C$, 1780 $^{\circ}C$, 1800 $^{\circ}C$ and 1820 $^{\circ}C$ under 20 MPa using $Al_2O_3-Y_2O_3$ system as sintering additives in order to low sintering temperature. The starting powder was high purity ${\beta}-SiC$ nano-powder with an average particle size of 30 nm. Monolithic LPS-SiC was evaluated in terms of sintering density, micro-structure, flexural strength, elastic modulus and so on. Sintered density, flexural strength and elastic modulus of fabricated LPS-SiC increased with increasing the sintering temperature. In the micro-structure of this specimen, it was found that grain of sintered body was grown from 30 nm to 200 nm.

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Fabrication of 13Cr-1.5Nb-Fe Alloy Powder and AC Magnetic Properties of the Sintered Magnetic Core (소결 13Cr-1.5Nb-Fe 합금의 교류 자기 특성)

  • 오환수;김택기;조용수
    • Journal of the Korean Magnetics Society
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    • v.10 no.1
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    • pp.11-15
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    • 2000
  • 13Cr-1.5Nb-Fe alloy powder prepared by water atomizing method is reduced with flowing hydrogen gas. The characteristics of a reduced alloy powder is investigated and magnetic cores formed by using the reduction power sintered in the vacuum of ∼10$\^$-5/ Torr. In order to study on the magnetic cores permeability and power loss in alternating magnetic field are also measured. The result of particle size distribution shows the paticle size is 70 ㎛ at volume fraction of 50 %. The saturation magnetization of the reduced alloy powder is 160 emu/g. The relative peak permeability (H$\_$a/=5Oe) of a magnetic core is 400 and the power loss (B$\_$m/=80G) 0.12 mW/cc at sintering temperature of 1,200 $\^{C}$, 10 ton/㎠ forming pressure, and 1 kHz.

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Microstructure and Giant Magnetoresistance of AgCo Nano-granular Alloy Films (Ag-Co합금박막의 두께에 따르는 미세구조 변화 및 자기저항 거동)

  • 이성래;김세휘
    • Journal of the Korean Magnetics Society
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    • v.8 no.3
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    • pp.131-137
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    • 1998
  • The thickness dependence of the microstructure and the giant magnetoresistance behavior of co-evaporated Co-Ag granular alloy films were investigated. The maximum magnetoresistance ratio of 24% was observed in the the as-deposited state of the 40 at. % Co alloy having 200 nm thickness. The surface scattering contributed about 20% to the total resistivity in the 20 nm thick films. The MR ratio dropped sharply when the film thickness was below 50 nm. The reduction in the Co particle size and the increase in solid solubility of Ag in fcc Co when the film thickness decreased were observed using a high resolution TEM. The aspect ratio of the Co particles was also affected by the film thickness. Those microstructural changes as well as the surface induced spin flipping play a significant role in the $\Delta$p change.

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Synthesis of Silica Membranes on a Porous Stainless Steel by Sol-Gel Method and Effect of Preparation Conditions on Their Permselectivity

  • Lee, Dong-Wook;Nam, Seung-Eun;Sea, Bong-Kuk;Ihm, Son-Ki;Lee, Kew-Ho
    • Bulletin of the Korean Chemical Society
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    • v.25 no.9
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    • pp.1371-1378
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    • 2004
  • A porous stainless steel (SUS) as a substrate of silica composite membranes for hydrogen purification was used to improve mechanical strength of the membranes for industrial application. The SUS support was successfully modified by using submicron Ni powder, $SiO_2$ sols with particle size of 500 nm and 150 nm in turns. Silica top layer was coated on the modified supports under various preparation conditions such as calcination temperature, dipping time and repeating number of dipping-drying process. The calcination temperature for proper sintering was between H ttig temperature and Tamman temperature of the coating materials. Maximum hydrogen selectivity was investigated by changing dipping time. As repeating number of dipping-drying process increased, permeances of nitrogen and hydrogen were decreased and $H_2/N_2$ selectivity was increased due to the reduction of non-selective pinholes and mesopores. For the silica membrane prepared under optimized conditions, permeance of hydrogen was about $3\;{\times}\;10^{-5}\;cm^3{\cdot}cm^{-2}{\cdot}s^{-1}{\cdot}cmHg^{-1}$ combined with $H_2/N_2$ seletivity of about 20.

Permeation Characteristics of the Microfiltration Tubular Module using the Discharged Rod (배출봉을 이용한 정밀여과용 관형 모듈의 투과특성)

  • Chung, Kun-Yong;Choi, Jeong-Gyu
    • Membrane Journal
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    • v.19 no.4
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    • pp.285-290
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    • 2009
  • The permeation experiments were carried out for the nominal pore size $0.1\;{\mu}m$ and 5 mm inner diameter microfiltration tubular membrane equipped with self-designed discharging rod in order to determine the effect of fouling reduction. Dioctyl tinoxide (DOTO) latex particle was used to prepare up to 0.5 wt% concentration of feed solution, and the experiments were operated within 1.6 bar. The permeation flux effect on the discharged rod was measured as a result of flux comparison between the cases of equipped and non-equipped discharge rod modules for every experiment. The permeation flux for the case using the discharged rod was enhanced to 20% at 1.6 bar operating pressure. The improvement on permeation flux for using the discharged rod was greater as the concentration of feed increased, and reached up to 43% under 0.5 wt% concentration of feed solution.

Application of Copper Slag as a Substitute for Sand in Sand Compaction Pile (모래다짐말뚝의 모래대체재로서 동슬래그의 활용)

  • 천병식;정헌철
    • Journal of the Korean Geotechnical Society
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    • v.18 no.5
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    • pp.195-207
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    • 2002
  • The domestic, quantity of copper slag as a by-product at copper smelting process reaches 700,000 tons annually while its application is limited. Therefore, the secure disposal plan of copper slag is urgently required. For this reason, in this study, copper slag was used as a substitute for sand in Sand Compaction Pile that is one of the improvement methods of soft ground because the particle size distribution of copper slag ranges from 0.15mm to 5m(coarse state) and it maintains stable glassy state environmentally. The geotechnical characteristics of copper slag were evaluated through laboratory model tests and the field application of copper slag was compared with generally used sand by pilot tests. From these experimental results, copper slag's material characteristics, bearing capacity, settlement reduction and improvement effects of surrounding ground were found to be superior to generally used sand. The copper slag can be used as a substitute far sand in the Sand Compaction Pile method and as recycling material of industrial by-product with high econonical and environmental value when natural resources are being exhausted.

A Study on the Effects of Hydrogen Addition and Swirl Intensity in CH4-Air Premixed Swriling Flames (메탄-공기 예혼합 선회화염에서 수소첨가와 선회강도 영향에 관한 연구)

  • KIM, HAN SEOK;CHO, JU HYEONG;KIM, MIN KUK;HWANG, JEONGJAE;LEE, WON JUNE
    • Journal of Hydrogen and New Energy
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    • v.30 no.6
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    • pp.593-600
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    • 2019
  • The combustion characteristics of methane/hydrogen pre-mixed flame have been investigated with swirl stabilized flame in a laboratory-scale pre-mixed combustor with constant heat load of 5.81 kW. Hydrogen/methane fuel and air were mixed in a pre-mixer and introduced to the combustor through a burner nozzle with different degrees of swirl angle. The effects of hydrogen addition and swirl intensity on the combustion characteristics of pre-mixed methane flames were examined using particle image velocimetry (PIV), micro-thermocouples, various optical interference filters and gas analyzers to provide information about flow velocity, temperature distributions, and species concentrations of the reaction field. The results show that higher swirl intensity creates more recirculation flow, which reduces the temperature of the reaction zone and, consequently, reduces the thermal NO production. The distributions of flame radicals (OH, CH, C2) are dependent more on the swirl intensity than the percentage of hydrogen added to methane fuel. The NO concentration at the upper part of the reaction zone is increased with an increase in hydrogen content in the fuel mixture because higher combustibility of hydrogen assists to promote faster chemical reaction, enabling more expansion of the gases at the upper part of the reaction zone, which reduces the recirculation flow. The CO concentration in the reaction zone is reduced with an increase in hydrogen content because the amount of C content is relatively decreased.

Effects of Free Surface Fluctuation on the Response of Submerged Structure (파낭에 의한 해수면의 변화가 해양구조물의 동적거동에 미치는 영향)

  • Cho, Yong-Jun;Yoo, Keung-Hwan
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.5 no.1
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    • pp.1-10
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    • 1993
  • In this paper, the effects of free surface fluctuation on the dynamic response of offshore structure is studied. In order to make the mathematical treatment of problem more tractable, only a single degree of freedom system subjected a long crested, stationary, Gaussian, non-breaking random waves of arbitrary bandwidth is considered. Wave force is computed based on the Morison equation in which wave induced fluid particle velocity and acceleration are modified to account for the effect of intermittent submergence of structural members near the free surface. It is shown that the response spectrum is reduced and higher harmonic response component appears when the intermittent submergence of structural member is considered. Furthermore, it is also found that the amount of reduction in the response spectrum is getting smaller as frequency is increased which might be attributed to the higher harmonic component caused by intermittent submergence and these effects are getting profound as water depth is decreased.

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The Multi-layer Fabrication and Characteristic Performance for Dark Current Reduction of Mercury Iodide (Hgl2의 누설전류 저감을 위한 다층구조 제작 및 특성 평가)

  • Kim, Kyung-Jin;Park, Ji-Koon;Kang, Sang-Sik;Cha, Byung-Youl;Cho, Sung-Ho;Kim, Jin-Yung;Mun, Chi-Ung;Nam, Sang-Hee
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.07a
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    • pp.388-389
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    • 2005
  • In this paper, the electric properties of mercury Iodide multi-layer samples has been investigated. We measured and analyzed their performance parameters such as the X-ray sensitivity and dark-current for a mercury Iodide multi-layer X-ray detector with a dielectric layer. The digital X-ray image detector can be constructed by integrating photoconduction multi-layer that dielectric layer has characteristics of low dark-current, high X-ray sensitivity. However this process has found to have complexity on the performance of the sample. We have investigate dielectric layer that it substitute dielectric layer for HgO(Mercury Oxide). We have employed two approaches for producing the mercury Iodide sample : 1) Physical Vapor Deposition(PVD) and 2) Particle-In-Binder(PIB). In this paper fabricated by PIB Method with thicknesses ranging from approximately 180um to 240um and we could produce high-quality samples for each technique particular application. As results, the dielectric materials such as HgO between the dielectric layer and the top electrode may reduce the dark-current of the samples. Mercury Iodide multi-layer having HgO has characteristics of low dark-current, high X-ray sensitivity and simple processing. So we can acquired a enhanced signal to noise ratio. In this paper offer the method can reduce the dark-current in the X-ray detector.

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Detection of foot-and-mouth disease virus (FMDV) and avian influenza virus (AIV) from animal carcass disposal sites using real-time RT-PCR

  • Miguel, Michelle;Kim, Seon-Ho;Lee, Sang-Suk;Cho, Yong-Il
    • Korean Journal of Veterinary Service
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    • v.43 no.2
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    • pp.107-112
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    • 2020
  • Foot-and-mouth disease (FMD) and avian influenza (AI) are highly pathogenic viral disease which affects the livestock industry worldwide. Outbreak of these viruses causes great impact in the livestock industry; thus, disease infected animals were immediately disposed. Burial is the commonly used disposal method for deceased animals. However, there is potential for secondary environmental contamination, as well as the risk that infectious agents persisting in the environment due to the limited environmental controls in livestock burial sites during the decomposition of the carcasses. Therefore, this study aimed to investigate the detection of FMD and AI viruses from animal carcass disposal sites using real-time reverse transcription PCR. Soil samples of more than three years post-burial from livestock carcass disposal sites were collected and processed RNA isolation using a commercial extraction kit. The isolated RNA of the samples was used for the detection of FMDV and AIV using qRT-PCR. Based on the qPCR assay result, no viral particle was detected in the soil samples collected from the animal disposal sites. This indicates that 3 years of burial and their carcass disposal method is efficient for the control or at least reduction of spread infections in the surrounding environment.