• 제목/요약/키워드: pH treatment

검색결과 7,423건 처리시간 0.041초

Size Control and Dispersion Properties of Illite Clay by Physicochemical Treatment (물리화학적 처리에 의한 일라이트 점토광물의 입도조절 및 분산특성)

  • Lim, Jae Won;Jeong, Euigyung;Seo, Kyeong-won;Lee, Young-Seak
    • Applied Chemistry for Engineering
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    • 제22권2호
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    • pp.133-137
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    • 2011
  • In this study, illite was size-reduced using a wet-ball-milling treatment to improve its dispersion. Changes in illite particle size, size distribution, and dispersion characteristics after varying the treatment period were investigated. And the dispersion and dispersion stability of illite solution after 2 h wet ball milling treatment with different pH conditions were also evaluated. The illite particle size significantly decreased as the treatment time increased and the size reduction effect of wet ball milling deteriorated above 2 h treatment time. In addition, illite particle size was more evenly distributed as the treatment time increased. X-ray diffraction (XRD) analysis showed that no crystal structural changes of illite were induced, but the characteristic peak of illite the weaker due to the size reduction and exfoliation, as the treatment time increased. Zeta potential analysis showed that the illite dispersion improved, as the treatment time increased. The illite wet-ball-mill treated at pH 2 had the lowest dispersion stability. Illite dispersion and dispersion stability increased as pH increased, due to the increase in surface ionization. Hence, the results showed that as the treatment time increased, the illite particle size decreased, and dispersion and dispersion stability improved due to the increase in surface energy and repulsion force between particles.

Characteristics of the Water Soluble Browning Reaction of Korean Red Ginseng as Affected by Heating Treatment (열처리에 따른 고려홍삼의 수용성 갈변물질의 특성)

  • 이종원;이성계
    • Journal of Ginseng Research
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    • 제22권3호
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    • pp.193-199
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    • 1998
  • The purpose of this study was to Investigate characteristics of the water soluble browning reaction products (WS-BRPs) from Korean red ginseng by heat treatment. Absorbance of WS- BRPs was increased with increases of heating temperature and time, but pH value were decreased In Muter color value L and b value were decreased, while a value was increased. and absorbance at 280 nm in spectrum of the WS-BRPs was increased according to the increase of heating temperature. When the WS-BRPs were applied on Bio-Gel P-30 column after heating and pH treatment, two majors browning products increased according to the progress on time. And pH 3.0 increased in quantity of high molecular fractions and pH 8.0 increased in quantity of low molecular fractions.

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A study of the Emulsifying Properties of Kidney Bean Protein Isolate (분리 강남콩 단백질의 유화특성에 관한 연구)

  • 최희령;손경희;민성희
    • Korean journal of food and cookery science
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    • 제5권2호
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    • pp.9-17
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    • 1989
  • This study was carried out in order to study the emulsifying properties of kidney bean protein isolate. Kidney bean protein isolate was tested for the purpose of finding out the effect of pH, addition of NaCl, and heat treatment on the solbulity and emulsion capacity, emulsion stability, surface hydropobicity and emulsion viscosity. The results were summarized as follows. 1 The solubility of kidney bean protein isolate was affected by pH and showed the lowest value at pll 4.5 which is isoelectric point of kidney bean isolate. When the kidney bean protein isolate was heated, the highest value observed at pH 2 and pH 7 was 96.11%, 97.41% respectively. 2. The emulsion capacity of kidney bean protein isolate was not significantly different with each pH. With addition of NaCl, emulsion capacity decreased steadily. When heated thr highest value observed at pH 2 and pH 7 was 82.91 ml oil/100 mg protein ($60^{\circ}C$), 82.08 m1 oil/100 mg protein ($80^{\circ}C$) respectively. 3. The emulsion stability was significantly higher at pH 4.5 than that of pH 2 and pH 7 (p 0.05) When NaCl was added, emulsion stability was generally increased after 2hrs. When heated, the highest value observed at pH 2 and pH 7 was 21.25% ($80^{\circ}C$),23.7%($100^{\circ}C$) respectively after 2hrs. 4. Surface hydrophobicity increased sharply as 0.2 M NaCl was added to pH 4.5. When heated, the surface hydrophobicity increased as the temperature increased. 5. The highest value of emulsion viscosity was observed at pH 4.5 and pH 7 when 0.2 M NaCl was added. Under heat treatment, the highest value was 48,000 cps at pH 4.5 ($40^{\circ}C$). In the case of pH 7, the highest value was 105,000 cpa at $100^{\circ}C$.

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Boron doping with fiber laser and lamp furnace heat treatment for p-a-Si:H layer for n-type solar cells

  • Kim, S.C.;Yoon, K.C.;Yi, J.S.
    • Proceedings of the Korean Vacuum Society Conference
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    • 한국진공학회 2009년도 제38회 동계학술대회 초록집
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    • pp.322-322
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    • 2010
  • For boron doping on n-type silicon wafer, around $1,000^{\circ}C$ doping temperature is required, because of the relatively low solubility of boron in a crystalline silicon comparing to the phosphorus case. Boron doping by fiber laser annealing and lamp furnace heat treatment were carried out for the uniformly deposited p-a-Si:H layer. Since the uniformly deposited p-a-Si:H layer by cluster is highly needed to be doped with high temperature heat treatment. Amorphous silicon layer absorption range for fiber laser did not match well to be directly annealed. To improve the annealing effect, we introduce additional lamp furnace heat treatment. For p-a-Si:H layer with the ratio of $SiH_4:B_2H_6:H_2$=30:30:120, at $200^{\circ}C$, 50 W power, 0.2 Torr for 30 min. $20\;mm\;{\times}\;20\;mm$ size fiber laser cut wafers were activated by Q-switched fiber laser (1,064 nm) with different sets of power levels and periods, and for the lamp furnace annealing, $980^{\circ}C$ for 30 min heat treatment were implemented. To make the sheet resistance expectable and uniform as important processes for the $p^+$ layer on a polished n-type silicon wafer of (100) plane, the Q-switched fiber laser used. In consequence of comparing the results of lifetime measurement and sheet resistance relation, the fiber laser treatment showed the trade-offs between the lifetime and the sheet resistance as $100\;{\omega}/sq.$ and $11.8\;{\mu}s$ vs. $17\;{\omega}/sq.$ and $8.2\;{\mu}s$. Diode level device was made to confirm the electrical properties of these experimental results by measuring C-V(-F), I-V(-T) characteristics. Uniform and expectable boron heavy doped layers by fiber laser and lamp furnace are not only basic and essential conditions for the n-type crystalline silicon solar cell fabrication processes, but also the controllable doping concentration and depth can be established according to the deposition conditions of layers.

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Colorant Extracting and Its Storage Stability from Red bean and Black bean Seed Coat (팥 종피에서의 색소 추출과 저장 안정성)

  • Bae, Do Gyu;Jung, Yang Sook
    • Current Research on Agriculture and Life Sciences
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    • 제28권
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    • pp.31-38
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    • 2010
  • Extraction efficiency of colorants from red bean and black bean seed coat and its storage stability were examined according to the various extracting and storage conditions in this study. The obtained results were as follows ; The absorbance values of extracted colorants were increased with increasing extract time and temperature. pH 4 extracting was most efficient among the various pH conditions. The absorbance values of extracted colorant from red bean were increased with increasing extract time and temperature, when the extraction process was kept at $30^{\circ}C$ and $50^{\circ}C$, but it were decreased with increasing extract time at $70^{\circ}C$. In the case of black bean, it were also increased with increasing extract time and temperature. pH 5 extract was most efficient among the various pH conditions. In juice extractor system from red bean, the pH 5 of the pre-treatment was more efficient than the distilled water of pre-treatment. In black beans of the short-term pre-treatment with distilled water, the colorant was extracted better than at pH 5, but above 4 hours pre-treatment was decrease in pH 5. The Methionine added as a stabilizer gave the more effect to the stability of colorant from red bean the more Methionine addition. In the case of black bean 10mmol addition of methionine was more efficient than 20mmol.

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Changes in chemical stability and biological activities of sinapinic acid by heat treatment under different pH conditions (다양한 pH조건에서 가열처리에 의한 시나핀산의 화학 안정성 및 생리활성 변화)

  • Heo, Yunseon;Hong, Jungil
    • Korean Journal of Food Science and Technology
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    • 제52권6호
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    • pp.616-621
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    • 2020
  • Sinapinic acid is a widely-distributed phenolic acid in various edible plants. In this study, changes in chemical stability and biological activities of sinapinic acid by heat treatment were evaluated at different pH values. The decomposition of sinapinic acid with heating at 95℃ was accelerated at higher pH; the residual levels after 10 min of heating were 80, 45 and 24% at pH 6, 7 and 8, respectively. Levels of reactive oxygen species derived from sinapinic acid also increased after heating at pH 7 and 8. ABTS radical scavenging activities and ferric reducing antioxidant power of sinapinic acid were reduced significantly after heating at pH 7 and 8. The cytotoxic activity of sinapinic acid against HCT116 cells was significantly enhanced after heating at pH 8 with decreased glutathione levels. The results suggest that heat treatment causes changes in the chemical stability and biological activities of sinapinic acid, and such changes are more prominent at higher pH.

A Study on the Foaming Properties of Small red bean Protein Isolates at Various Conditions (분리 팥 단백질의 기포 특성에 영향을 주는 제 요인에 관한 연구)

  • 김현정
    • Journal of the Korean Home Economics Association
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    • 제28권2호
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    • pp.37-45
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    • 1990
  • The purpose of this study was to determine the foaming properties of two small red bean protein isolates at various conditions. Data concerning the effects of pH, temperature, MaCl concentration, sugar concentration and protein concentration on the properties such as solubility, foam expansion, foam stability were presented. The results were summarized as follows : 1. The crude protein contents of two small red beans were 26.14% and 22.71%. The percentage of nonpolar amino acid group was the highest and that of sulfur containing amino acid group was the lowest. 2. Protein solubility showed the minimum at pH 4.5 which is isoelectric point of small red bean protein isolate adn heat treatment lowered solubility(P<0.05). At pH 4.5, solubility increased sighificantly as 0.4M NaCl was added. However, the effect of sugar concentration in the solubility was not significant. 3. Foam expansion of two small red bean protein isolates was high at pH 4.5 and heat treatment at 10$0^{\circ}C$ lowered foam expansion(P<0.05). While addition of NaCl, sugar did not affect the foma expansion, gradual increment of the protein isolates concentration up to 9% decreased the foma expansion slightly. 4. Foam stability was significantly high at pH 4.5 and heat treatment at 10$0^{\circ}C$ lowered foam stability. Addition of sugar caused slight decrease in foam stability. From 1% to 9% suspension, foma stability increased significantly as protein concentration increased(P<0.05)

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The Effects of S-solution and A-solution on Oral Health in Preschool Children (S-solution과 A-solution을 이용한 구강함수가 미취학 아동의 구강건강에 미치는 효과)

  • Son, Hee Jung;Hong, Hae Sook
    • Journal of Korean Biological Nursing Science
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    • 제17권2호
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    • pp.150-158
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    • 2015
  • Purpose: This study aimed to evaluate the effects of gargling with S-solution and gargling with A-solution on salivary pH, coated tongue, and dental plaque index in preschool children. Methods: Non-equivalent control group pretest-posttest design was used to select the participants. 99 preschool children were divided into three groups. Dependent variables were recorded at baseline, 30 minutes, and 7 days after the first treatment was given. The data were analyzed using $X^2$-test, ANOVA, and repeated measures of ANOVA. Results: There were no significant differences in dependent variables in pre-test. However, the salivary pH in the S-solution group had significantly increased after 30 minutes (p<.05) and then again 7 days (p<.01) after the first treatment. Also, the S-solution and A-solution groups had greater decrease in dental plaque index after 30 minutes and again 7 days after the first treatment (p<.001) than the control group. With respect to coated tongue, there were no significant differences among the three groups. Conclusion: The results of this study indicate that essential oil gargling after brushing is helpful in improving oral health due to auxiliary oral hygiene effects with natural products. Specifically, gargling with S-solution is more effective than A-solution on oral health in preschool children by neutralizing salivary pH and reducing dental plaque index.

Changes in Ammonia Fluxes, pH and Total Nitrogen in Liquid Ferrous Sulfate-treated Litter (액상 황산철(liquid ferrous sulfate)을 육계 깔짚에 처리시 암모니아 발생량, pH및 총 질소 함량 변화)

  • Chung, Tae-Ho
    • Journal of Environmental Science International
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    • 제28권2호
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    • pp.287-290
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    • 2019
  • This study investigates the changes in ammonia fluxes, pH and total nitrogen of liquid ferrous sulfate-treated litter over 5 weeks. A total of 200 broiler chicks (Arbor Acres, 1 d old) was separated into two treatment groups (0 g and 100 g liquid ferrous sulfate/kg litter) with four replications of 25 birds in each group. Liquid ferrous sulfate was sprayed on the litter by using a small sprayer. There was no difference (p>0.05) in the ammonia fluxes observed between the control and liquid ferrous sulfate treatment groups at 0, 1, and 5 weeks, except for 2, 3 and 4 weeks. At 5 weeks, the litter pH and total nitrogen content did not show any difference (p>0.05) between the control and liquid ferrous sulfate treatment groups. In conclusion, the use of liquid ferrous sulfate is not a suitable for use in poultry litter to reduce ammonia and pH or improve the total nitrogen content.

Seasonal Changes in pH and Content of Phosphate, Organic Matter and Exchangeable Cations in Soil Profile of Urea-Fertilized Grassland (요소시용(尿素施用) 초지(草地)의 토양단면(土壤斷面)에서 pH 및 인산(燐酸), 유기물(有機物)과 치환성(置換性) 양(陽)이온 함량의 계절적 변화)

  • Yun, Sun-Gang;Yoo, Sun-Ho
    • Korean Journal of Soil Science and Fertilizer
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    • 제24권4호
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    • pp.254-259
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    • 1991
  • The present study was carried out to investigate the effect of nitrogen(urea) application on the seasonal change in pH content of Bray No.1-P, organic matter, and exchangeable cations along the grassland soil profile and further to provide the fundamental information for optimizing the rate of fertilizer application to grassland. Soil samples were taken 20cm intervals upto 100cm soil depth in spring(May 26), summer(July 27), and autumn (October 18) of 1990. The obtained results are summerized as follow 1. In spring and summer, soil pH at 0-20cm soil depth of 28kg N/10a treatment was lowered by 0.7 and 1.0 in comparison with those the same soil depth of 0 kg N/10a treatment and the tendency in pH decrease during all season at the soil depth below 20cm was in the order of summer>spring>autumn. 2. Although Bray No.1-P content at the soil depth 0-20cm of 28kg N/10a treatment was lowered by 20ppm compared to 0 kg N/10a treatment in summer, there was no great difference in its content between 0kg N/10a and 28kg N/10a treatment at all soil depth in spring and summer. In autumn, its content at soil depth below 20cm of 28kg N/10a treatment was higher than that of in summer. 3. Organic matter content at 0-20cm soil depth of 0 and 28kg N/10a treatment in autumn was slightly lowered and on the whole there was very little change in it by soil depth and nitrogen application. 4. The calcium content of 0 and 28kg N/10a treatment was also slightly lowered by increase in soil depth and Mg and K contents were below 0.4 and 0.2 me/100g during all seasons, respectively. 5. Positive correlations were shown among the $NH_4-N$ content and pH, organic matter, Ca and Mg of 0 kg N/10a treatment, however, there was negative correlation ($r=-0.534^{*}$) between $NO_3-N$ content and pH of 28kg N/10a treatment in summer.

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