• Preventive Nutrition and Food Science
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• 제15권2호
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• pp.147-151
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• 2010

The volatile aroma constituents of Atractylodes japonica rhizome were separated by steam distillation extraction method using a Clevenger-type apparatus, and analyzed by gas chromatography-mass spectrometry (GC/MS). The yield of the essential oil from Atractylodes japonica was 1.0% (v/w), and its color was pale yellow. Forty-five volatile flavor compounds, which make up 93.86% of the total peak area, were tentatively identified in the rhizome oil. The oil contained 32 hydrocarbons (79.19%) with sesquiterpene hydrocarbon predominating, 3 esters (12.46%), 4 alcohols (0.11%), 1 ketone (0.01%), 2 aldehydes (0.02%), and 3 miscellaneous compounds (2.07%).

• Plant Resources
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• 제7권2호
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• pp.104-109
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• 2004

This study was conducted to investigate the possibility that oil seed rape could be used as a forage fodder crop and to select the most suitable variety of forage rape at the southern area of Korea, Two varieties of oil seed rape currently grown for oil production and six introduced varieties of forage rape with relatively high yield and high nutritional value were grown at the same condition and their nutritional value were observed in Spring. Generally, rape was considered as a useful forage fodder crop with high content of crude protein and low contents of NDF, ADF, hemicellulose, cellulose and lignin. Differences in mean values of the above characters between two groups of rape were not statistically significant. Velox showed significantly higher content of crude protein and significantly lower contents of NDF, ADF, hemicellulose, cellulose and lignin compared with other varieties of forage rape in spring. Rape was relatively high in IVDMD compared with other forage fodder crops, and forage rape was more or less in IVDMD and DDMW than oil seed rape. Velox was the highest in IVDMD and DDMW among the varieties of forage rape in Spring, in this experiment.

• Preventive Nutrition and Food Science
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• 제13권2호
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• pp.122-127
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• 2008

The aroma constituents of Chrysanthemum indicum L. were separated by the hydro distillation extraction method using a Clevenger-type apparatus, and were analyzed by gas chromatography-mass spectrometry (GC/MS). The yield of Chrysanthemum indicum L. flower oil was 2.0% (w/w) and the color was light golden yellow. Sixty-three volatile flavor components, which make up 89.28% of the total aroma composition of the flower oil, were tentatively characterized. This essential oil contained 35 hydrocarbons (48.75%), 12 alcohols (19.92%), 6 ketones (15.31%), 3 esters (4.61%), 5 aldehydes (0.43%), 1 oxide (0.22%), and 1 miscellaneous component (0.04%). ${\alpha}$-Pinene (14.63%), 1,8-cineol (10.71%) and chrysanthenone (10.01%) were the predominant volatile components in Chrysanthemum indicum L., an aromatic medicinal herbaceous plant.

• Natural Product Sciences
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• 제25권2호
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• pp.150-156
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• 2019

Conventional extraction of oil and azadirachtin, a botanical insecticide, from Azadirachta indica involves defatting the seeds and leaves using hexane followed by azadirachtin extraction with a polar solvent. In order to simplify the process while maintaining the yield we explored a binary extraction approach using Soxhlet extraction device and hexane and ethanol as non-polar and polar solvents at various ratios and extraction times. The highest oil and azadirachtin yields were obtained at 6 h extraction time using a 50:50 solvent mixture for both neem leaves (44.7 wt%, $720mg_{Aza}/kg_{leaves}$) and seeds (53.5 wt%, $1045mg_{Aza}/kg_{leaves}$), respectively.

• 공업화학
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• 제19권2호
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• pp.214-221
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• 2008

산성도와 세공구조가 다른 제올라이트 촉매에서 폐식용유의 전이에스터화 반응에 의해 바이오디젤을 제조하였다. $H^+$ 이온 교환한 MOR, MFI, BEA, FAU 제올라이트와 산점이 거의 없는 실리카라이트 촉매의 반응 수율을 조사하였다. 산세기가 가장 강하고 산점이 많은 $H^+$ 이온 교환한 MOR(10) 제올라이트에서 메틸에스터 수율이 약 95%로 가장 높았다. 제올라이트 골격에서 알루미늄을 제거하면 산점의 수가 줄어들고 산세기도 약해지면서 메틸에스터 수율도 감소하였다. 폐식용유의 전이에스터화 반응에서 메틸에스터의 수율은 제올라이트 촉매의 산세기와 산량에 따라 비례하는 것으로 나타났다. 메틸에스터의 수율은 제올라이트의 세공구조에는 영향을 받지 않는 것으로 조사되었다.

• 한국작물학회지
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• 제42권6호
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• pp.647-651
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• 1997

무피복 재배조건에서 생육특성 및 수량성 그리고 종실의 단백질과 지방함량, 지방산 조성을 조사하여 무피복 재배법 확립을 위한 기초자료를 얻고자 대광땅콩, 대풍땅콩을 공시하고 흑색 비닐 피복재배와 비교하여 시험한 결과는 다음과 같다. 1. 출현기는 대광땅콩, 대풍땅콩 모두 피복재배보다 6일정도 지연되었으며 개화기는 각각 9일, 6일 지연되었고 입모율도 각각 3.7％, 16％감소되었다. 2. 분지장은 피복재배보다 대광땅콩 24％(11.2cm), 대풍땅콩 17％(6.9cm) 감소되었으나 분지수는 감소되지 않았다. 3. 성숙협수,100립중, 협실비율, 주당 종실수량등은 피복재배보다 현저히 감소되었으나 밀식재배로 인한 재식밀도의 증가로 1ha당 종실수량은 대광땅콩의 경우 피복재배와 비슷하였고 대풍땅콩의 경우는 26％ 증수되었다. 4. 단백질함량은 대광땅콩의 경우, 피복재배보다 4％ 증가하였으나 대풍땅콩은 3％ 감소하였으며 지방함량은 두 품종 모두 각각 7％, 9％ 감소되었다. 5. 지방산 조성에서 oleic acid는 대광, 대풍땅콩 모두 피복재배보다 증가하였으나 linolelc acid는 감소하였으며 O/L비율도 작아졌다.

• 신재생에너지
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• 제9권3호
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• pp.36-42
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• 2013

To secure raw materials of biodiesel production, the possibility of camellia (C. japonica L.) and tea (C. sinensis L.) seed oil was studied to produce biodiesel. In this research, crude oil contents and fatty acid compositions of seeds were analyzed by Solxlet and Gas chromatography (GC). The oil contents in the seeds of camellia were 69.8%~73.8%, and tea were 26.3%~29.4%. Among the fatty acids of camellia and tea oil, oleic acid was dominant. The unsaturated fatty acids accounted for 88.4% and 80.2% of the whole fatty acids of camellia and tea seed oil. Total seed oil content and fatty acid composition of tea seed were influenced by collecting date. Across maturation period, oil content of tea seed averaged 18.3% on $6^{th}$ September increasing to 27.9% by $11^{th}$ October. For largest seed yield and oil content, the optimum time to harvest tea is in middle october, and camellia is late september and thereafter. The extraction efficiency of oil from seeds by extraction methods was determined. Biodiesel were synthesized in 92.1~92.8% yields from camellia and tea oils by transesterification. The biodiesel was characterized by its physical and fuel properties including oxidation stability, iodine value and cold filter plugging point (CFPP). Oxidation stability of camellia was 8.6~8.8 hours and tea was 2.9~3.6 at $110^{\circ}C$. Camellia oil had considerably better oxidation stability and CFPP than tea oil.

• 수산해양교육연구
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• 제27권5호
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• pp.1334-1342
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• 2015

본 연구에서는 연어 오일의 미세캡슐화를 위해 다양한 피복물질을 사용해 보았다. 피복물질의 종류가 미세캡슐화 수율에 큰 영향을 미쳤으며, 피복물질로 사용한 MD/SC/WPI 혼합 처리구에서 수율이 82.55%로 가장 우수한 성능을 보였다. SEM 분석 결과 입자의 분포가 균일하고 섬유 표면의 질감이 매끄럽게 나타났으며, 저장성 실험결과 pH, 산가, 과산화물가에서 안정한 수치를 나타내었기에 제품화 시 유통기한 30일까지는 실온저장에서 안전할 것으로 사료된다. 또한 MD/SC/WPI를 이용하여 분말화 한 연어 오일은 유화안정성이 높고, 제품의 취급이 쉽게 이용 될 수 있을 것이다. 이에 본 연구에서의 캡슐화 방법이 연어 오일과 유사한 특성을 지닌 물질의 캡슐화에 응용 될 수 있을 것이다.

• KSBB Journal
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• 제24권1호
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• pp.89-95
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• 2009

Biodiesel (fatty acid alkyl esters), which is produced from sustainable resources such as vegetable oil, animal fat and waste oils, have used to as substitutes for petro-diesel. In this study, we investigate the performance of 30 L and 300 L pilot-scale biodiesel production system using alkali-catalyst transesterification from soybean oil and rapeseed oil produced at Jeju island in Korea. The 30 L-scale biodiesel production was performed to in the condition of reaction temperature $65^{\circ}C$, catalyst amount 1% (w/w) and oil to methanol molar ratio 1 : 8. At that reaction condition, the fatty acid methyl ester contents of product are above 98% within reaction time 30 min. Also, the conversion yield of over 98% was obtained in 300 L-scale biodiesel production system using rapeseed oil and soybean oil. The quality of biodiesel produced from reaction system was satisfied to recommended quality standard of Korea. Our results may provide useful information with regard to the scale-up of more economic and efficient biodiesel production process.

• 한국연초학회지
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• 제14권1호
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• pp.66-78
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• 1992

The essential oil of Korean valerian root ( Valeriana fauriei roar. dasycarpa Hara) was isolated by simultaneous distillation Sl extraction. The oil content of fresh root was 0.7% (wb) and that of dried root was 2.1 5 (db) and sensory analysis of the oil indicated sweet-balsamic, woody and floral characteristic aroma notes. The oil was fractionated into one hydrocarbon fraction and three oxygenated hydrocarbon fractions by using silica gel column chromatograpy. Each fraction was analyzed by capillary GC and GC-MS. Out of 81 characterized compounds, the major compounds were a-pinene, camphene, $\beta$-pinene, bornyl acetate, borneol , bornyl iso-valerate and sesquiphellandrene and the characteristic floral and woody aroma of neutral fraction of Korean valerian root could be due to be the presence of oxygenated compounds such as borneol, bornyl acetate, bornyl iso-valerate, p-ionone ana $\beta$-ionone epoxide. Comparing the yield of Korean valerian root with those from other origins reported, oil content of Korean valerian root was higher than those of European and Indian origins.