• Title/Summary/Keyword: nickel-iron

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Regeneration Methods for Iron Powers in the Treatment of the Waste FeCl3 Etching Solution (엣칭용 염화철폐액의 처리에서 미반응철의 재생방법)

  • Park, Chan-Woo;Jeung, Woo-Won;Lee, Man-Ho
    • Applied Chemistry for Engineering
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    • v.8 no.4
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    • pp.595-601
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    • 1997
  • The regeneration of the iron powders in the treatment of $FeCl_3$ etching solution containing nickel by ball-mill and ultrasonic treatments has been studied. When the unreacted iron powders were treated twice, the removal efficiency of nickel was 94.0% for the ball-mill treatment and 82.1% for the ultrasonic treatment. But the removal efficiency of nickel was 40.0% for the untreated iron powders. As the treatment time was increased, the particle size of iron powders was decreased for ball-mill treatment and almost not changed for ultrasonic treatment.

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Research of Electrochemical Properties with Metal Sulfide Electrode for Lithium Batteries (리튬전지용 금속황화물 전극의 전기화학적 특성에 관한 연구)

  • RYU, HO SUK;KIM, IN SOO
    • Transactions of the Korean hydrogen and new energy society
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    • v.31 no.1
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    • pp.138-143
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    • 2020
  • Metal sulfides are good candidates for cathode materials. Especially, iron sulfides and nickel sulfides have been demonstrated to be potential electrode materials among metal sulfides due to nontoxicity and high theoretical specific capacities. Electrochemical properties (capacity, cycle life, stability etc.) of Li/iron sulfides or nickel sulfides cell were improved by methode such as coating, doping of material, and nanoization of materials etc.

The Effects of Silicon and Nickel Additions on the Mechanical Properties of Heavy Section Ductile Irons for Wind Mill (풍력발전용 후육 구상흑연주철의 기계적 성질에 미치는 Si 및 Ni 첨가의 영향)

  • Park, Heung-Il;Kim, Woo-Yeol;Ahn, Won-Young
    • Journal of Korea Foundry Society
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    • v.26 no.6
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    • pp.258-266
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    • 2006
  • The purpose of this study was to investigate the effects of silicon and nickel additions that influenced the impact and tensile properties of heavy section as-cast ductile irons for wind mill. Based on the results of the metallographic analysis and the mechanical testing on the 2.0 wt.%Si (LS group) and 2.4 wt.%Si (HS group) ductile irons, which contains 0.0, 0.3, 0.6 and 0.9 wt.%Ni, respectively, the following conclusions could be obtained. The nickel additions increased the tensile properties, the microhardness of pearlite, and the pearlite fraction of matrix for the specimen with the same silicon content. The mechanical properties of LS group specimen were in the range of the specification for the ductile iron wind mill castings. The LS group specimens showed higher absorbed impact energy at room temperature and $-20^{\circ}C$ than that of the HS group specimens. However, the absorbed impact energy at $-20^{\circ}C$ for the HS group specimens was observed to be sharply decreased under 10 J by addition of the nickel.

Recovery of nickel from the spent nickel-cadmium battery (폐 Ni-Cd 전지로부터 니켈의 회수)

  • 박제신;박경호;전호석;손정수;김병규
    • Resources Recycling
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    • v.8 no.5
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    • pp.28-33
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    • 1999
  • Trus paper presenls a hydrometallurgical process Tor recovcnng ~uckcals mckcl sulfate fiom the spent nickel-cadrnlum bauery in whch c:,dmi~lm war re~novcdb y vapowing m e h d in vacuum. F ~ s ts,e lcct~vcc rushing and classification mell~odw ere performed to separate iron physically and the nickel-rich sample (over 80% nickel) was obtained. Ths sarnple was dissolved in sulf~ uiuica cid to obtain a luckcl sulfatc soluho~d~o se to its seluradon painl. TIE Cree acid in the unpurificd nickcl solut~onw as neutl-dized and iron war ve~novedk om the solulmn Thc mckel sulhte solution was c~yst~llizeadt around 45'C to obtain ruckel sulfate henahyril-ate.

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Effect of Nickel Content on Corrosion Resistance and Machinability of Fe-23Cr-2.5C-1.2Si-1.08Mn-0.48Mo-0.3V-xNi Cast Iron (Fe-23Cr-2.5C-1.2Si-1.08Mn-0.48Mo-0.3V-xNi 주철의 내식성 및 피삭성에 미치는 Ni의 영향)

  • Kim, Ki-Bin;Jung, Sung-Sik;Baek, Min-Sook;Yoon, Dong Joo
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.3
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    • pp.576-584
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    • 2020
  • The extruder screw material is mainly SKD11, but the recent development of synthetic resins have increased the occurrence of chemical corrosion and wear. To solve this issue, high chromium cast iron is needed because of its good abrasion resistance and corrosion resistance, but its use is avoided because of its poor machinability. In this study, to improve the machinability of high chrome cast iron, 0, 0.5, 1.0, 1.5% of nickel, which has excellent workability, was added to high chromium cast iron with a composition of Fe-23Cr-2.5C-1.2Si-1.08Mn-0.48Mo-0.3V, and annealed after casting. Subsequently, the effect of nickel on the machinability and corrosion resistance was analyzed using a turning test and coin polarization test, and compared with SKD11. After casting using a high-frequency vacuum induction furnace, the annealing treatment was performed at 750 ℃ for five hours and then reheated at 1100 ℃ for five hours. A turning test after annealing at 750 ℃ showed that the machinability was improved remarkably when the nickel content was over 1.0%. In the potentiodynamic polarization test in a 5% NaCl solution, the corrosion resistance decreased with increasing nickel content in the as-cast and annealing treatment. On the other hand, after reheating, the corrosion resistance was best with a 1.5% nickel content.

Comparison of Pretreatment Methods for Determination of 55Fe and 63Ni Activity in Nuclear Wastes Sample (원자력 시설 해체 폐기물 내 55Fe 와 63Ni 방사능 분석을 위한 전처리 방법 비교 연구)

  • Lee, Hoon;Lim, Jong-Myoung;Ji, Young-Yong;Jung, Kun-Ho;Kang, Mun-Ja;Choi, Geun-Sik;Lee, Jin-Hong
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.13 no.2
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    • pp.113-122
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    • 2015
  • 55Fe and 63Ni are key factors in deciding the proper handling of the decommissioning of radioactive waste from nuclear facilities. For determining beta emitting radionuclides, the dismantled waste samples should be completely decomposed and separated from the sample matrix. This study reports the comparison results of the recovering efficiencies of Iron and Nickel with wet digestion methods that use various acids and alkali-fusion methods. Various matrices of NIST SRMs (1646a, 1944, 8704, 2709a, and 1633c), the recovering efficiencies of using alkali-fusion methods ranged from 95.3 to 98.3% for Iron, and from 86.6 to 88.1% for Nickel within about 2% of relative standard deviation. On the other hand, those using one of the three wet digestion methods ranged from 77.9 to 105.3% for Iron and from 40.1 to 78.5% for Nickel with over 10% of relative standard deviation. Therefore, one may draw the conclusion that the analytical results derived from Iron and Nickel using alkali-fusion methods are fairly reliable due to the recovering efficiencies observed.

Microstructure and Properties of High Nitrogen Sintered Stainless Steel

  • Pieczonka, Tadeusz;Stoytchev, Marin
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.568-569
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    • 2006
  • The use of the nickel free, high nitrogen stainless steel powder and nitriding during sintering of iron based materials have been shown as an alternative way to the conventional PM stainless steels containing nickel. Nitrogen as an alloying element for iron improves in an effective way the properties of sintered alloyed steels. The powder metallurgy route is a suitable way to introduce nitrogen into these alloys and, in particular, to produce high nitrogen (close to the solubility limit) stainless steels. The paper presents and discusses the nitriding behavior of nickel-free stainless steels produced by powder metallurgy method. Alloyed melt was atomized by nitrogen and in this way nitrogen was introduced into the powder. Further nitriding occurred during sintering in a nitrogen atmosphere. For comparison, compacts having the same composition as an alloyed powder were produced from elemental powders mixture. Sintering-nitriding behaviour of investigated materials has been controlled by dilatometry, chemical and X-Ray phase analysis and metallography. Mechanical properties of sintered compacts were also measured.

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Removal of Nickel from the Etching Waste Solution of Ferric Chloride (엣칭용 염화제2철 폐액중의 니켈제거)

  • Doh, Yong-Il;Jeung, Woo-Won;Lee, Man-Ho
    • Applied Chemistry for Engineering
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    • v.7 no.4
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    • pp.614-622
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    • 1996
  • Efficient removal of nickel from the ferric chloride etching solution has been studied. At first, $Fe^{3+}$ was reduced to $Fe^{2+}$ by the electrolytic iron flake or the waste shadow mask iron plate. And then, $Ni^{2+}$ was removed from the solution by electrolytic iron powder. Under the optimum conditions the reduced rates of nickel were 99 % and 98%, respectively at the initial $Ni^{2+}$ concentrations of 1.0% and 0.1%. Sludge formed during reduction of $Fe^{3+}$ in the solution were analyzed by XRD and SEM.

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